Breaking thermodynamic and kinetic barriers in superalloy homogenization process by electropulsing to improve mechanical properties

2021 ◽  
pp. 159854
Author(s):  
Jianqiao Hao ◽  
Shuyang Qin ◽  
Longge Yan ◽  
Xinfang Zhang
2015 ◽  
Vol 9 (2) ◽  
pp. 2431-2439
Author(s):  
Saad El Madani ◽  
S. ELHAMZI ◽  
J. KATTEN ◽  
A. IBNLFASSI

In order to master and improve the quality and properties of the final products, the major industrial challenge lies in the possibility of controlling the morphology, size of microstructures that reside within the molded pieces, as well as their defects; this is the fundamental reason according to which we are more and more interested in mastering the growth and germination of such alloys, as well as the developing structures, at the time of solidification process. The modeling reveals as a valuable aid in the mastery of the formation of such heterogeneousness: segregation cells that are incompatible with industrial requirements. The whole work focuses upon the modeling of the segregation phenomenon of the four hypoeutectic alloys, Al1%Sn, Al2%Sn, Al3%Sn and Al4%Sn, as well as the tin effect upon certain mechanical properties of aluminum. Usually, the microstructure and mechanical  behavior of such alloys as Al-Sn are directly influenced by some parameters such as composition, cooling velocity and homogenization process.


2015 ◽  
Vol 10 (2) ◽  
pp. 2753-2761
Author(s):  
Saad El Madani ◽  
S. ELHAMZI ◽  
A. IBNLFASSI ◽  
L. ZERROUK ◽  
O. BEN LENDA ◽  
...  

In order to master and improve the quality and properties of the final products, the major industrial challenge lies in the possibility of controlling the morphology, size of microstructures that reside within the molded pieces, as well as their defects; this is the fundamental reason according to which we are more and more interested in mastering the growth and germination of such alloys, as well as the developing structures, at the time of solidification process. The modeling reveals as a valuable aid in the mastery of the formation of such heterogeneousness: segregation cells that are incompatible with industrial requirements.   The whole work focuses upon the modeling of the segregation phenomenon of the four hypoeutectic alloys, Al1%Cu, Al2%Cu, Al3%Cu et Al4%Cu, as well as the copper effect upon certain mechanical properties of aluminum. Usually, the microstructure and mechanical behavior of such alloys as Al-Cu are directly influenced by some parameters such as composition, cooling velocity and homogenization process.


2016 ◽  
Vol 16 (1) ◽  
Author(s):  
Ayu Rizeki Ridhowati ◽  
Eka Febriyanti ◽  
Rini Riastuti

Warm rolling is one of the thermomechanical method has several advantages such as produces high mechanical properties, but does not decrease % elongation and toughness value because partial recrystallization phenomenon that produces micron-sized new grain. This paper reports the results of an investigation carried out on the effects of holding time annealing to mechanical properties Cu-Zn 70/30 alloy. These alloy after homogenization process and quenched in the air then heated to temperature of 300°C, later the heated copper samples are warm rolled at 25%, 30%, and 35% reduction, after that heated at temperature 300°C and held during 120 minutes. Then sample is experienced rewarm rolling with reduction 25%, 30%, and 35%. The results obtained showed that the ultimate tensile strength and yield strength are higher proportional with the increasing of % reduction, their values are 501,1 MPa; 599,3 MPa; later decrease to 546, 5 MPa and to yield strength are 441,8 MPa; 466,1 MPa; then decrease to 458,6 MPa. Moreover hardness value increase proportional with % reduction such as 154 HV; 162 HV; after that decrease to 160 HV While, % elongation decreases inversely proportional with % reduction namely 12,4%; 8,2%; later increase to 11,2 %. It is caused of the partial recrystallization phenomenon as evidenced by the presence micron-sized.AbstrakWarm rolling merupakan salah satu metode termomekanik yang mempunyai beberapa keuntungan yaitu salah satunya menghasilkan sifat mekanik yang tinggi, namun tidak mengurunkan nilai keuletan karena adanya fenomena rekristalisasi parsial yang menghasilkan butiran baru berbentuk micron. Paper ini menjelaskan tentang hasil penelitian berupa pengaruh persentase reduksi terhadap sifat mekanis paduan Cu-Zn 70/30. Paduan Cu-Zn 70/30 setelah dilakukan proses homogenisasi dan didinginkan di udara lalu dipanaskan ke suhu 300°C, kemudian masing-masing dilakukan warm rolling dengan persentase reduksi sebesar 25%, 30%, dan 35% kemudian ditahan di suhu 300°C dalam waktu 120 menit. Selanjutnya sampel dilakukan rewarm rolling dengan persentase reduksi sebesar 25%, 30%, dan 35%. Hasil penelitian yang dilakukan antara lain nilai kekuatan tarik (UTS dan YS) yang semakin tinggi sebanding dengan peningkatan % reduksi warm rolling yaitu masing-masing untuk nilai UTS sebesar 501,1 MPa; 599,3 MPa; lalu menurun menjadi 546,5 MPa serta untuk nilai kekuatan luluh sebesar 441,8 MPa; 466,1 MPa; lalu menurun menjadi 458,6 MPa. Selain itu, nilai kekerasan meningkat sebanding dengan peningkatan % reduksi warm rolling masing-masing sebesar 154 HV; 162 HV; lalu menurun menjadi 160 HV. Sedangkan persentase elongasi semakin menurun berbanding terbalik dengan peningkatan % reduksi masing-masing sebesar 12,4%; 8,2%; lalu meningkat menjadi 11,2%. Hal tersebut disebabkan karena adanya fenomena rekristalisasi parsial yang dibuktikan dengan kehadiran butir kecil berukuran mikron.Keywords : Cu-Zn 70/30 alloy, warm rolling, anneal, % reduction, mechanical properties


2019 ◽  
Vol 112 ◽  
pp. 03009
Author(s):  
Anişoara Păun ◽  
Gheorghe Stroescu ◽  
Dumitru Milea ◽  
Mihai Olan ◽  
Mariana Epure

Obtaining quality fodder that meets the requirements of fodder receipts makes necessary the use of components that have to respect certain dimensions. The milled products must respect the granulation imposed by the receipt because they are very well assimilated by animals and the homogenization process is also very good. The milling process is a complex one, influenced by a number of factors that depend on the technical and constructive solution of the milling chamber and on the physical and mechanical properties of the processed raw material (seeds). In the hammer mills with open chambers and sieve surface up to 180 degrees, the presence of concaves (grooved plates) within the milling chamber is a must because it will lead to the acceleration of the seed milling process and implicitly to increase the productivity and reduce electricity consumption. The paper follows the theoretical and experimental presentation of an open chamber mill that is provided with these grooved plates.


2019 ◽  
Vol 15 (2) ◽  
pp. 29
Author(s):  
Eka Febriyanti ◽  
Rini Riastuti

Abstract Warm rolling is one of the thermomechanical method has several advantages such as produces high mechanical properties, but does not decrease % elongation and toughness value because partial recrystallization phenomenon that produces micron-sized new grain. This paper reports the results of an investigation carried out on the effects of holding time annealing to mechanical properties Cu-Zn 70/30 alloy. These alloy after homogenization process and quenched in the air then heated to temperature of 300°C, later the heated copper samples are warm rolled at 25%, 30%, and 35% reduction, after that heated at temperature 300°C and held during 120 minutes. Then sample is experienced rewarm rolling with reduction 25%, 30%, and 35%. The results obtained showed that the ultimate tensile strength and yield strength are higher proportional with the increasing of % reduction, their values are 501,1 MPa; 599,3 MPa; later decrease to 546, 5 MPa and to yield strength are 441,8 MPa; 466,1 MPa; then decrease to 458,6 MPa. Moreover hardness value increase proportional with % reduction such as 154 HV; 162 HV; after that decrease to 160 HV While, % elongation decreases inversely proportional with % reduction namely 12,4%; 8,2%; later increase to 11,2 %. It is caused of the partial recrystallization phenomenon as evidenced by the presence micron-sized. Warm rolling merupakan salah satu metode termomekanik yang mempunyai beberapa keuntungan yaitu salah satunya menghasilkan sifat mekanik yang tinggi, namun tidak mengurunkan nilai keuletan karena adanya fenomena rekristalisasi parsial yang menghasilkan butiran baru berbentuk micron. Paper ini menjelaskan tentang hasil penelitian berupa pengaruh persentase reduksi terhadap sifat mekanis paduan Cu-Zn 70/30. Paduan Cu-Zn 70/30 setelah dilakukan proses homogenisasi dan didinginkan di udara lalu dipanaskan ke suhu 300°C, kemudian masing-masing dilakukan warm rolling dengan persentase reduksi sebesar 25%, 30%, dan 35% kemudian ditahan di suhu 300°C dalam waktu 120 menit. Selanjutnya sampel dilakukan rewarm rolling dengan persentase reduksi sebesar 25%, 30%, dan 35%. Hasil penelitian yang dilakukan antara lain nilai kekuatan tarik (UTS dan YS) yang semakin tinggi sebanding dengan peningkatan % reduksi warm rolling yaitu masing-masing untuk nilai UTS sebesar 501,1 MPa; 599,3 MPa; lalu menurun menjadi 546,5 MPa serta untuk nilai kekuatan luluh sebesar 441,8 MPa; 466,1 MPa; lalu menurun menjadi 458,6 MPa. Selain itu, nilai kekerasan meningkat sebanding dengan peningkatan % reduksi warm rolling masing-masing sebesar 154 HV; 162 HV; lalu menurun menjadi 160 HV. Sedangkan persentase elongasi semakin menurun berbanding terbalik dengan peningkatan % reduksi masing-masing sebesar 12,4%; 8,2%; lalu meningkat menjadi 11,2%. Hal tersebut disebabkan karena adanya fenomena rekristalisasi parsial yang dibuktikan dengan kehadiran butir kecil berukuran mikron. Keywords:Cu-Zn 70/30 alloy, warm rolling, anneal, % reduction, mechanical properties 


Author(s):  
S. Fujishiro

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.


Author(s):  
L.J. Chen ◽  
H.C. Cheng ◽  
J.R. Gong ◽  
J.G. Yang

For fuel savings as well as energy and resource requirement, high strength low alloy steels (HSLA) are of particular interest to automobile industry because of the potential weight reduction which can be achieved by using thinner section of these steels to carry the same load and thus to improve the fuel mileage. Dual phase treatment has been utilized to obtain superior strength and ductility combinations compared to the HSLA of identical composition. Recently, cooling rate following heat treatment was found to be important to the tensile properties of the dual phase steels. In this paper, we report the results of the investigation of cooling rate on the microstructures and mechanical properties of several vanadium HSLA steels.The steels with composition (in weight percent) listed below were supplied by China Steel Corporation: 1. low V steel (0.11C, 0.65Si, 1.63Mn, 0.015P, 0.008S, 0.084Aℓ, 0.004V), 2. 0.059V steel (0.13C, 0.62S1, 1.59Mn, 0.012P, 0.008S, 0.065Aℓ, 0.059V), 3. 0.10V steel (0.11C, 0.58Si, 1.58Mn, 0.017P, 0.008S, 0.068Aℓ, 0.10V).


Author(s):  
D. R. Clarke ◽  
G. Thomas

Grain boundaries have long held a special significance to ceramicists. In part, this has been because it has been impossible until now to actually observe the boundaries themselves. Just as important, however, is the fact that the grain boundaries and their environs have a determing influence on both the mechanisms by which powder compaction occurs during fabrication, and on the overall mechanical properties of the material. One area where the grain boundary plays a particularly important role is in the high temperature strength of hot-pressed ceramics. This is a subject of current interest as extensive efforts are being made to develop ceramics, such as silicon nitride alloys, for high temperature structural applications. In this presentation we describe how the techniques of lattice fringe imaging have made it possible to study the grain boundaries in a number of refractory ceramics, and illustrate some of the findings.


Author(s):  
Li Li-Sheng ◽  
L.F. Allard ◽  
W.C. Bigelow

The aromatic polyamides form a class of fibers having mechanical properties which are much better than those of aliphatic polyamides. Currently, the accepted morphology of these fibers as proposed by M.G. Dobb, et al. is a radial arrangement of pleated sheets, with the plane of the pleats parallel to the axis of the fiber. We have recently obtained evidence which supports a different morphology of this type of fiber, using ultramicrotomy and ion-thinning techniques to prepare specimens for transmission and scanning electron microscopy.


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