Development of ZrO2/SiO2 bioinert ceramic coatings for biomedical application

2008 ◽  
Vol 1 (2) ◽  
pp. 165-171 ◽  
Author(s):  
M MORKS ◽  
A KOBAYASHI
2016 ◽  
Vol 840 ◽  
pp. 175-179 ◽  
Author(s):  
Te Chuan Lee ◽  
Mohd Hafifi Hafizat Mazlan ◽  
Mohamad Imran Abbas ◽  
Hasan Zuhudi Abdullah ◽  
Maizlinda Izwana Idris

Anodic oxidation is an electrochemical method to deposit ceramic coatings on the metals substrate to improve the bioactivity. This study aims to investigate the effect of bath temperature on the surface properties of anodised titanium. High-purity titanium foil was modified by anodising in mixture of β-glycerophosphate disodium salt pentahydrate (β-GP) and calcium acetate monohydrate (CA). The experiments were carried out at 350 V, 30 mA.cm-2 for 10 minutes at different bath temperature (4-100 °C). Field emission scanning electron microscopy (FESEM), glancing angle X-ray diffractometer (GAXRD) and goniometer were used to characterise the surface morphology, mineralogy and wettability of anodised titanium, respectively. The results showed that porosity and crystallinity of surface decreased as increasing of bath temperature. Interestedly, the α-tricalcium phosphate (α-TCP) was deposited on the samples which anodisation at higher bath temperature (≥ 60 °C) and resulted high hydrophilicity behaviour even the surface was found relatively smooth.


2015 ◽  
Vol 3 (3) ◽  
pp. 317-324 ◽  
Author(s):  
Karuppasamy Prem Ananth ◽  
Sudha Shanmugam ◽  
Sujin P. Jose ◽  
A. Joseph Nathanael ◽  
Tae Hwan Oh ◽  
...  

Author(s):  
K.R. Subramanian ◽  
A.H. King ◽  
H. Herman

Plasma spraying is a technique which is used to apply coatings to metallic substrates for a variety of purposes, including hardfacing, corrosion resistance and thermal barrier applications. Almost all of the applications of this somewhat esoteric fabrication technique involve materials in hostile environments and the integrity of the coatings is of paramount importance: the effects of process variables on such properties as adhesive strength, cohesive strength and hardness of the substrate/coating system, however, are poorly understood.Briefly, the plasma spraying process involves forming a hot plasma jet with a maximum flame temperature of approximately 20,000K and a gas velocity of about 40m/s. Into this jet the coating material is injected, in powder form, so it is heated and projected at the substrate surface. Relatively thick metallic or ceramic coatings may be speedily built up using this technique.


Author(s):  
Ozer Unal

Interest in ceramics as thermal barrier coatings for hot components of turbine engines has increased rapidly over the last decade. The primary reason for this is the significant reduction in heat load and increased chemical inertness against corrosive species with the ceramic coating materials. Among other candidates, partially-stabilized zirconia is the focus of attention mainly because ot its low thermal conductivity and high thermal expansion coefficient.The coatings were made by Garrett Turbine Engine Company. Ni-base super-alloy was used as the substrate and later a bond-coating with high Al activity was formed over it. The ceramic coatings, with a thickness of about 50 μm, were formed by EB-PVD in a high-vacuum chamber by heating the target material (ZrO2-20 w/0 Y2O3) above its evaporation temperaturef >3500 °C) with a high-energy beam and condensing the resulting vapor onto a rotating heated substrate. A heat treatment in an oxidizing environment was performed later on to form a protective oxide layer to improve the adhesion between the ceramic coating and substrate. Bulk samples were studied by utilizing a Scintag diffractometer and a JEOL JXA-840 SEM; examinations of cross-sectional thin-films of the interface region were performed in a Philips CM 30 TEM operating at 300 kV and for chemical analysis a KEVEX X-ray spectrometer (EDS) was used.


2000 ◽  
Vol 28 (3-4) ◽  
pp. 481-485 ◽  
Author(s):  
Alessandro Mantini ◽  
Corrado Di Natale ◽  
Antonella Macagnano ◽  
Roberto Paolesse ◽  
Alessandro Finazzi-Agro ◽  
...  

2020 ◽  
Vol 3 (3) ◽  
Author(s):  
Hemalatha D ◽  
Saraswath S

In material science, green method for synthesis of nanomaterials is feasible, cheaper and eco-friendly protocol. To accomplish this phenomenon, present study was aimed to synthesize Copper oxide nanoparticles using leaf extract of Aloevera with two different precursors CuCl2.2H2O (Cupric chloride) and CuSo4.5H2O (Cupric sulfate). The extraction of Aloevera is employed as reducing and stabilizing agent for this synthesis.Copper oxide Nanoparticles is effective use of biomedical application due to their antibacterial function. The synthesized Copper oxide nanoparticles were characterized by X-Ray Diffraction Spectroscopy (XRD), Energy Dispersive Spectroscopy (EDX), FourierTransform Infrared Spectroscopy (FT- IR) and Scanning Electron Microscope(SEM). XRD studies reveal the crystallographic nature of Copper oxide nanoparticles. Furthermore the Copper oxide nanoparticles have good Antibacterial activity against both gram negative (E.Coli, Klebsiella pneumonia) and gram positive (Bacillus cereus, Staphylococcus aureus)bacteria.


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