Effects of sintering temperature on interface microstructure and element diffusion of WC-Co-Ni-Fe / High-speed steel composites

2021 ◽  
pp. 131449
Author(s):  
Hongnan Li ◽  
Ling Yan ◽  
Hongmei Zhang ◽  
Fangfang Ai ◽  
Dadong Zhao ◽  
...  
2014 ◽  
Vol 788 ◽  
pp. 329-333
Author(s):  
Rui Zhou ◽  
Xiao Gang Diao ◽  
Jun Chen ◽  
Xiao Nan Du ◽  
Guo Ding Yuan ◽  
...  

Effects of sintering temperatures on the microstructure and mechanical performance of SPS M3:2 high speed steel prepared by spark plasma sintering was studied. High speed steel sintering curve of continuous heating from ambient temperature to 1200°C was estimated to analyze the sintering processes and sintering temperature range. The sintering temperature within this range was divided into groups to investigate hardness, relative density and microstructure of M3:2 high-speed steel. Strip and quadrate carbides were observed inside the equiaxed grains. SPS sintering temperature at 900°C can lead to nearly full densification with grain size smaller than 20μm. The hardness and bending strength are higher than that of the conventionally powder metallurgy fabricated ones sintered at 1270°C. However, fracture toughness of the high speed steel is lower than that of the conventional powder metallurgy steels. This can be attributed to the shape and distribution of M6C carbides which reduce the impact toughness of high speed steels.


2007 ◽  
Vol 23 ◽  
pp. 147-150 ◽  
Author(s):  
Manuela Covaciu ◽  
Traian Canta ◽  
Elena Gordo

The paper presents studies about reducing the sintering temperature of PM High-Speed Steel obtained by water atomization. The powder was characterized to proceed with compaction and sintering at different temperatures between 1140-1220°C in different atmospheres: nitrogen (N2), nitrogen-hydrogen-methane (N2/H2/CH4) and vacuum. It is described the experiment in able to increase hardness by a quenching and tempering heat treatment that was carried out on sintered samples at 1140°C in vacuum atmosphere at 1200°C in N2/H2/CH4.


2007 ◽  
Vol 539-543 ◽  
pp. 2749-2754 ◽  
Author(s):  
A. Kloc ◽  
Leszek Adam Dobrzański ◽  
G. Matula ◽  
José M. Torralba

Investigations carried out referred to obtaining material based on the high-speed steel and non-alloy steel. The conventional powder metallurgy method was used for manufacturing these materials, consisting in compacting the powder in the closed die and sintering it next, the isostatic pressing method, and the modern pressureless forming powder metallurgy. Forming methods were developed during the investigations for high-speed and non-alloy steel powders, making it possible to obtain materials with three layers in their structure. Investigations included determining the sintering conditions, and especially the temperature and treatment cycle, as well as examining the selected mechanical properties. It was found out, basing on the comparison of structures and properties of test pieces made with the pressureless forming method, as well as with the isostatic pressing and pressing in the closed die, with further sintering, that in structures of all examined test pieces in the sintered state fine carbides occurred distributed homogeneously in the high-speed steel layer. It was noticed, that increase of the sintering temperature, regardless of the manufacturing method, results in the uncontrolled growth and coagulation of the primary carbides and melting up to forming of eutectics in layers consisting of the high-speed steel. It was found out basing on the microhardness tests that hardness of test pieces both those pressureless formed, compacted in the closed die, and isostatically cold pressed and sintered grows along with the sintering temperature. It was also noted that the sintering temperature range is bigger in case of the pressureless formed materials.


Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1549
Author(s):  
Marcin Madej ◽  
Beata Leszczyńska-Madej ◽  
Dariusz Garbiec

Attempts were made to describe the effect of the sintering temperature and pure iron powder addition on the properties of high speed steel based materials produced by the spark plasma sintering technique. After sintering, their density, hardness, flexural strength, and tribological properties were determined. The sintered materials were also subjected to microstructural analysis in order to determine the phenomena occurring at the particle contact boundaries during sintering. Based on the analysis of the obtained results, it was found that the mechanical properties and microstructure were mainly influenced by the sintering temperature. Using the temperature of 1000 °C allowed materials with a density close to the theoretical density to be obtained, characterized by a high hardness of about 360 HB and a low wear rate of about 1E-07 g/s.


2012 ◽  
Vol 727-728 ◽  
pp. 90-95 ◽  
Author(s):  
Alexandre Wentzcovitch ◽  
Francisco Ambrozio Filho ◽  
Luís Carlos Elias da Silva ◽  
Maurício David Martins das Neves

The influence of adding 6 wt% (NbC) niobium carbide on the sintering temperature and microstructure of high speed steel - AISI M2(0.87% C, 5.00% Mo, 6.00% W, 4,00% Cr, 2.00% V and Fe bal.) powder was studied. The starting material was obtained by vacuum melting followed by atomization in water. The samples were axially cold compacted in a cylindrical matrix and then vacuum sintered at 1250 and 1350 °C. Dilatometry and differential scanning calorimetry measurements indicated an increase in sintering temperature with addition of niobium to the AISI M2steel. Optical and scanning electron microscope observations revealed a microstructure with uniformly distributed niobium carbides.


2006 ◽  
Vol 530-531 ◽  
pp. 358-363 ◽  
Author(s):  
Oscar O. Araujo Filho ◽  
Maurício David Martins das Neves ◽  
João Franklin Liberati ◽  
Luís Carlos Elias da Silva ◽  
Lucio Salgado ◽  
...  

Liquid phase sintering of high speed steels seems to be a cheaper processing route in the manufacturing of tool steels if compared to the well-known and expansive hot isostatic pressing high speed steels process. In a previous work a M3:2 high speed steel was vacuum sintered from irregular water atomized powders and had its sintering temperature determined. In this work the same powder was uniaxially cold compacted and vacuum sintered by adding some small quantity of graphite (0.3%C in weight) to prevent porosity and loss of carbon which result from the sintering cycle. The samples from all these experimental procedures were uniaxially cold compacted and vacuum sintered at five different temperatures and had its densities evaluated. The microstructure was evaluated using optical-electronic techniques in order to investigate the best range of sintering temperature. At least five parallel samples were tested to each condition of sintering.


2020 ◽  
Vol 38 (8A) ◽  
pp. 1226-1235
Author(s):  
Safa R. Fadhil ◽  
Shukry. H. Aghdeab

Electrical Discharge Machining (EDM) is extensively used to manufacture different conductive materials, including difficult to machine materials with intricate profiles. Powder Mixed Electro-Discharge Machining (PMEDM) is a modern innovation in promoting the capabilities of conventional EDM. In this process, suitable materials in fine powder form are mixed in the dielectric fluid. An equal percentage of graphite and silicon carbide powders have been mixed together with the transformer oil and used as the dielectric media in this work. The aim of this study is to investigate the effect of some process parameters such as peak current, pulse-on time, and powder concentration of machining High-speed steel (HSS)/(M2) on the material removal rate (MRR), tool wear rate (TWR) and the surface roughness (Ra). Experiments have been designed and analyzed using Response Surface Methodology (RSM) approach by adopting a face-centered central composite design (FCCD). It is found that added graphite-silicon carbide mixing powder to the dielectric fluid enhanced the MRR and Ra as well as reduced the TWR at various conditions. Maximum MRR was (0.492 g/min) obtained at a peak current of (24 A), pulse on (100 µs), and powder concentration (10 g/l), minimum TWR was (0.00126 g/min) at (10 A, 100 µs, and 10 g/l), and better Ra was (3.51 µm) at (10 A, 50 µs, and 10 g/l).


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