Material ratio curve as information on the state of surface topography—A review

2020 ◽  
Vol 65 ◽  
pp. 240-258 ◽  
Author(s):  
Pawel Pawlus ◽  
Rafal Reizer ◽  
Michal Wieczorowski ◽  
Grzegorz Krolczyk
Author(s):  
S. Anand Kumar ◽  
Anigani Sudarshan Reddy ◽  
Snehith Mathias ◽  
Abhishek Shrivastava ◽  
Prasad Raghupatruni

Currently, the surface integrity-related issues of additively manufactured parts are limiting the potential high-end applications. The present work investigates the effectiveness of the pulsed-electropolishing technique to improve the surface integrity of aluminium alloys fabricated using the selective laser melting (SLM) technique. Due to its low density, high corrosion resistance, the aluminium alloys considerably enhance the performance of lightweight critical parts for different industrial applications. In this study, selective laser melted AlSi10Mg samples were subjected to microstructural examinations using optical microscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction technique. The microhardness and tensile properties were determined using a microhardness tester and a universal testing machine, respectively. The pulsed-electropolishing process was employed for the surface finishing of the SLM-processed AlSi10Mg samples. The effect of current density on the electropolishing of selective laser melted AlSi10Mg alloy were also investigated. The microstructures of printed samples revealed a density of greater than 99.9% and weld beads along the build direction (longitudinal) and laser scan paths perpendicular to the build direction (transverse). The microhardness, yield and tensile strength properties were similar in both as-printed conditions. The pulsed electropolishing results showed a beneficial effect of higher current density values, resulting in decreased surface roughness of the SLM-processed AlSi10Mg samples. Compared to as-printed conditions, a significant decrease in surface roughness of about ∼73.35% under optimized electropolishing conditions was noted. The material ratio curve shows that the surface topography becomes more uniform with increased current density and has lesser surface undulations for as-printed samples. The 2D line profilogram and 3D surface topography of electropolished SLM-processed samples reveal the surface finish quality characteristics. The material ratio curve aids as an effective method to assess and qualify the surface topography of electropolished samples.


Author(s):  
C. T. Nightingale ◽  
S. E. Summers ◽  
T. P. Turnbull

The ease of operation of the scanning electron microscope has insured its wide application in medicine and industry. The micrographs are pictorial representations of surface topography obtained directly from the specimen. The need to replicate is eliminated. The great depth of field and the high resolving power provide far more information than light microscopy.


Author(s):  
P.G. Pawar ◽  
P. Duhamel ◽  
G.W. Monk

A beam of ions of mass greater than a few atomic mass units and with sufficient energy can remove atoms from the surface of a solid material at a useful rate. A system used to achieve this purpose under controlled atmospheres is called an ion miliing machine. An ion milling apparatus presently available as IMMI-III with a IMMIAC was used in this investigation. Unless otherwise stated, all the micro milling operations were done with Ar+ at 6kv using a beam current of 100 μA for each of the two guns, with a specimen tilt of 15° from the horizontal plane.It is fairly well established that ion bombardment of the surface of homogeneous materials can produce surface topography which resembles geological erosional features.


Author(s):  
T. A. Welton

Various authors have emphasized the spatial information resident in an electron micrograph taken with adequately coherent radiation. In view of the completion of at least one such instrument, this opportunity is taken to summarize the state of the art of processing such micrographs. We use the usual symbols for the aberration coefficients, and supplement these with £ and 6 for the transverse coherence length and the fractional energy spread respectively. He also assume a weak, biologically interesting sample, with principal interest lying in the molecular skeleton remaining after obvious hydrogen loss and other radiation damage has occurred.


Author(s):  
David C. Joy ◽  
Dennis M. Maher

High-resolution images of the surface topography of solid specimens can be obtained using the low-loss technique of Wells. If the specimen is placed inside a lens of the condenser/objective type, then it has been shown that the lens itself can be used to collect and filter the low-loss electrons. Since the probeforming lenses in TEM instruments fitted with scanning attachments are of this type, low-loss imaging should be possible.High-resolution, low-loss images have been obtained in a JEOL JEM 100B fitted with a scanning attachment and a thermal, fieldemission gun. No modifications were made to the instrument, but a wedge-shaped, specimen holder was made to fit the side-entry, goniometer stage. Thus the specimen is oriented initially at a glancing angle of about 30° to the beam direction. The instrument is set up in the conventional manner for STEM operation with all the lenses, including the projector, excited.


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