Recent IAEA reference materials and intercomparison exercises for radionuclides in the marine environment

Author(s):  
M.K. Pham ◽  
J. Gastaud ◽  
J. La Rosa ◽  
S.-H. Lee ◽  
I. Levy-Palomo ◽  
...  
1983 ◽  
Vol 40 (S2) ◽  
pp. s100-s110 ◽  
Author(s):  
V. Holden ◽  
G. Topping ◽  
J. F. Uthe

The results of several intercomparison exercises for heavy metals and organochlorine residues in marine samples are reviewed. We conclude that, with few exceptions, the levels of agreement between the participating analysts are not good enough to allow them all to take part in multilaboratory monitoring programs, particularly with respect to monitoring residues in fish to determine whether they comply with standards set for human consumption or for comparing levels of contamination in different areas. Reproducibility of analysis is generally better at the higher concentrations and may be sufficient to measure a decrease in contamination following the removal of a highly polluting discharge. However, at the lower concentrations existing in cleaner environments many techniques that analysts currently use may be unable to achieve a degree of precision (or accuracy) sufficient to measure long-term trends in contamination. Analyses carried out by individual laboratories for the purpose of measuring trends in contamination levels must include regular intralaboratory checks to ensure a constant level of performance throughout the period of study.


Author(s):  
G. Remond ◽  
R.H. Packwood ◽  
C. Gilles ◽  
S. Chryssoulis

Merits and limitations of layered and ion implanted specimens as possible reference materials to calibrate spatially resolved analytical techniques are discussed and illustrated for the case of gold analysis in minerals by means of x-ray spectrometry with the EPMA. To overcome the random heterogeneities of minerals, thin film deposition and ion implantation may offer an original approach to the manufacture of controlled concentration/ distribution reference materials for quantification of trace elements with the same matrix as the unknown.In order to evaluate the accuracy of data obtained by EPMA we have compared measured and calculated x-ray intensities for homogeneous and heterogeneous specimens. Au Lα and Au Mα x-ray intensities were recorded at various electron beam energies, and hence at various sampling depths, for gold coated and gold implanted specimens. X-ray intensity calculations are based on the use of analytical expressions for both the depth ionization Φ (ρz) and the depth concentration C (ρz) distributions respectively.


2020 ◽  
pp. 66-72
Author(s):  
Irina A. Piterskikh ◽  
Svetlana V. Vikhrova ◽  
Nina G. Kovaleva ◽  
Tatyana O. Barynskaya

Certified reference materials (CRM) composed of propyl (11383-2019) and isopropyl (11384-2019) alcohols solutions were created for validation of measurement procedures and control of measurement errors of measurement results of mass concentrations of toxic substances (alcohol) in biological objects (urine, blood) and water. Two ways of establishing the value of the certified characteristic – mass consentration of propanol-1 or propanol-2 have been studied. The results obtained by the preparation procedure and comparison with the standard are the same within the margin of error.


2020 ◽  
pp. 64-70
Author(s):  
Mariya Y. Medvedevskikh ◽  
Anna S. Sergeeva

The article raises the problem of ensuring metrological traceability of the measurement results of indicators of quality and nutritional value for food products and food raw materials: water (moisture), nitrogen (protein, crude protein), fat, ash and carbohydrates. The problem under consideration can be solved by applying reference materials of food composition, traceable to state primary measurement standards GET 173-2017 and GET 176-2019 and primary reference measurement procedures (PRMP), for attestation of measurement procedures and accuracy checking of measurement results. The article discusses the results of the PRMP development of mass fraction of fat, ash and carbohydrates in food products and food raw materials, as well as mass fraction of crude fat (oil content) in oil crops seeds and products based on them. The paper also presents metrological characteristics of reference materials of composition of dry dairy products, grain-milk dry porridges for nutrition of babies, grain dry porridges for nutrition of babies, egg powder, freeze-dried meat products, animal feed. The results of the work allow for building a chain of metrological traceability from GET 173-2017, GET 176-2019 and PRMP to routine measurement procedures, thereby ensuring the uniformity of measurements of nutritional value of food products.


2020 ◽  
Vol 649 ◽  
pp. 125-140
Author(s):  
DS Goldsworthy ◽  
BJ Saunders ◽  
JRC Parker ◽  
ES Harvey

Bioregional categorisation of the Australian marine environment is essential to conserve and manage entire ecosystems, including the biota and associated habitats. It is important that these regions are optimally positioned to effectively plan for the protection of distinct assemblages. Recent climatic variation and changes to the marine environment in Southwest Australia (SWA) have resulted in shifts in species ranges and changes to the composition of marine assemblages. The goal of this study was to determine if the current bioregionalisation of SWA accurately represents the present distribution of shallow-water reef fishes across 2000 km of its subtropical and temperate coastline. Data was collected in 2015 using diver-operated underwater stereo-video surveys from 7 regions between Port Gregory (north of Geraldton) to the east of Esperance. This study indicated that (1) the shallow-water reef fish of SWA formed 4 distinct assemblages along the coast: one Midwestern, one Central and 2 Southern Assemblages; (2) differences between these fish assemblages were primarily driven by sea surface temperature, Ecklonia radiata cover, non-E. radiata (canopy) cover, understorey algae cover, reef type and reef height; and (3) each of the 4 assemblages were characterised by a high number of short-range Australian and Western Australian endemic species. The findings from this study suggest that 4, rather than the existing 3 bioregions would more effectively capture the shallow-water reef fish assemblage patterns, with boundaries having shifted southwards likely associated with ocean warming.


2019 ◽  
Vol 20 (1) ◽  
Author(s):  
Suganjar Suganjar ◽  
Renny Hermawati

<p><em>Safety management in the shipping industry is based on an international regulation. It is International Safety Management Code (ISM-Code) which is a translation of SOLAS ‘74 Chapter IX. It stated that t</em><em>he objectives of the Code are to ensure safety at sea, prevention of human injury or loss of life, and avoidance of damage to the environment, in particular, to the marine environment, and to property.it is also</em><em> requires commitment from top management to implementation on both company and on board. The implementation of the ISM-Code is expected to make the ship’s safety is more secure. The ISM-Code fulfillment refers to 16 elements, there are; General; Safety and Environmental Protection Policy; Company Responsibility and Authority; Designated Person(s); Master Responsibility and Authority; Resources and Personnel; Shipboard Operation; Emergency Preparedness; Report and Analysis of Non-conformities, Accidents and Hazardous Occurrences; Maintenance of the Ship and Equipment; Documentation; Company Verification, Review, and Evaluation;  Certification and Periodical Verification; Interim Certification; Verification; Forms of Certificate. The responsibility and authority of Designated Person Ashore / DPA in a shipping company is regulated in the ISM-Code. So, it is expected that DPA can carry out its role well, than can minimize the level of accidents in each vessels owned/operated by each shipping company.</em></p><p><em></em><strong><em>Keywords :</em></strong><em> ISM Code,</em><em> </em><em>Safety management, </em><em>Designated Person Ashore</em></p><p> </p><p> </p><p>Manajemen keselamatan di bidang pelayaran saat ini diimplementasikan dalam suatu peraturan internasional yaitu <em>International Safety Management Code</em> (<em>ISM-Code</em>) yang merupakan penjabaran dari <em>SOLAS 74 Chapter IX</em>-<em>Management for the safe operation of ships</em>. Tujuan dari <em>ISM-Code</em> <em>“The objectives of the Code are to ensure safety at sea, prevention of human injury or loss of life, and avoidance of damage to the environment, in particular, to the marine environment, and to property”</em> dan  <em>ISM-Code</em> menghendaki adanya komitmen dari manajemen tingkat puncak sampai pelaksanaan, baik di darat maupun di kapal.  Pemberlakuan <em>ISM-Code</em> tersebut diharapkan akan membuat keselamatan kapal menjadi lebih terjamin. Pemenuhan <em>ISM-Code</em> mengacu kepada 16 elemen yang terdiri dari ; umum; kebijakan keselamatan  dan perlindungan lingkungan; tanggung jawab dan wewenang perusahaan; petugas yang ditunjuk didarat; tanggung jawab dan wewenang nahkoda; sumber daya dan personil; pengopersian kapal; kesiapan menghadapi keadaan darurat; pelaporan dan analisis ketidaksesuaian, kecelakaan dan kejadian berbahaya; pemeliharaan kapal dan perlengkapan;  Dokumentasi; verifikasi, tinjauan ulang, dan evaluasi oleh perusahaan; sertifikasi dan verifikasi berkala; sertifikasi sementara; verifikasi; bentuk sertifikat. Tugas dan tanggungjawab <em>Designated Person Ashore/DPA </em>didalam suatu perusahaan pelayaran<em>, </em>telah diatur di dalam <em>ISM-Code.</em>  Sehingga diharapkan agar DPA dapat melaksanakan peranannya dengan baik, sehingga dapat menekan tingkat kecelakaan di setiap armada kapal yang dimiliki oleh setiap perusahaan pelayaran.</p><p class="Style1"><strong>Kata kunci</strong> : <em>ISM Code</em>, Manajemen keselamatan, <em>Designated Person Ashore</em></p>


2016 ◽  
Vol 1 (1) ◽  
Author(s):  
F. Sadatfaraji ◽  
A. Bashir Bhatti ◽  
F. Behzadi ◽  
M. Khani ◽  
M. Khani

Sign in / Sign up

Export Citation Format

Share Document