A New Hot Stage for the Philips EM 200 and Its Calibration
A hot stage for use in metallurgical investigations with the electron microscope should have several, if not all, of the following characteristics.The specimen temperature should be measurable with accuracy over the full range of operation of the stage.The stage should allow a large tilt angle for diffraction and contrast work.The stage should not restrict expansion of the sample during temperature cycling thus avoiding alteration to the sample's defect structure from the presence of thermal stress.The heater and sample should approach equilibrium rapidly after any change in temperature, with a minimum of drift during the change, and a high degree of stability at temperature.The stage should permit study of as much of the thinned specimen area as is possible compatible with adequate thermal coupling to the furnace.