Representation of information in SEM by equal signal lines

1978 ◽  
Vol 36 (1) ◽  
pp. 144-145
Author(s):  
E. Rau ◽  
N. Karelin ◽  
V. Dukov ◽  
M. Kolomeytsev ◽  
S. Gavrikov ◽  
...  
Keyword(s):  
Electronic System ◽  
Space Distribution ◽  
Specimen Surface ◽  
Universal Method ◽  
Base Level ◽  
Signal Value ◽  
Information Signal ◽  
Fixed Base ◽  
Scanning Line ◽  
Amplitude Analyzer

There are different methods and devices for the increase of the videosignal information in SEM. For example, with the help of special pure electronic [1] and opto-electronic [2] systems equipotential areas on the specimen surface in SEM were obtained. This report generalizes quantitative universal method for space distribution representation of research specimen parameter by contour equal signal lines. The method is based on principle of comparison of information signal value with the fixed levels.Transformation image system for obtaining equal signal lines maps was developed in two versions:1)In pure electronic system [3] it is necessary to compare signal U (see Fig.1-a), which gives potential distribution on specimen surface along each scanning line with fixed base level signals εifor obtaining quantitative equipotential information on solid state surface. The amplitude analyzer-comparator gives flare sport videopulses at any fixed coordinate and any instant time when initial signal U is equal to one of the base level signals ε.

scholarly journals The effect of thermal agitation on atomic arrangement in alloys

1934 ◽  
Vol 145 (855) ◽  
pp. 699-730 ◽  
Keyword(s):  
Single Phase ◽  
Chemical Compounds ◽  
Alloy System ◽  
Electronic System ◽  
Atomic Ratio ◽  
The Other ◽  
Space Distribution ◽  
Binding Forces ◽  
Binary Alloy System ◽  
The One

When two metals are allowed together in various proportions, a series of solid phases is formed. A characteristic phase diagram of a binary alloy system has regions of single phase, throughout which the alloy is homogeneous, alternating with regions in which two neighbouring phases coexist. The composition of a single phase can be varied continuously over a certain range. This feature of an alloy is in contrast to tire constant atomic ratio of a chemical compound, and is explained by the nature of the binding forces in an alloy which are predominantly those between the metal atoms of both kinds on the one hand and the common electronic system on the other hand, as opposed to the binding forces between atom and atom which predominate in other chemical compounds. Not only may the atomic ratio in a given phase be varied, but also an orderly space distribution of one kind of atom relative to the other, as found in topical chemical compounds, does not necessarily exist in an alloy. Although each phase is distinguished by possessing a characteristic crystalline structure which differs from that of other phases in the same alloy system, yet this structure may be merely an orderly arrangement of sites occupied by atoms. The manner in which the atoms are distributed amongst the sites of a given phase is often variable, and is, for instance, affected by the thermal treatment which the alloy has undergone.

scholarly journals Potential Design of Seismic Vulnerable Buildings Incorporating Lead Rubber Bearing

Buildings ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 37 ◽  
Author(s):  
Walid Al-Kutti ◽  
A. Islam
Keyword(s):  
Structural Damage ◽  
New Technologies ◽  
Structural Parameters ◽  
Response Spectrum ◽  
Base Shear ◽  
Characteristic Strength ◽  
Base Level ◽  
Rubber Bearing ◽  
Lead Rubber Bearing ◽  
Fixed Base

The seismic hazard of vulnerable regions warrants the investigation of new technologies, such as base level isolation by lead rubber bearing (LRB) devices, that can help to mitigate structural damage on seismic prone buildings. The behavior adopting such technologies can be dynamically observed in simulated environments and thus serves as a valuable metric for their feasibility. LRB base isolators were incorporated into the design of 16 model buildings to better understand how they affected a building’s seismic response while also providing information on the structural parameters. A total of 12 different types of bearing systems were tested in base isolated (BI) buildings against conventional fixed-base (FB) isolated buildings. The system of each model high-rise building was represented by the finite element package. Static as well as dynamic analysis were conducted using response spectrum analysis (RSA) based on the seismic excitation to determine the influence of the model type in the aseismic design and the alteration in superstructure behavior. The study reveals that the LRB isolators can potentially diminish respective story accelerations, story inertia, and base shear. Use of LRB isolators in BI buildings resulted in a 10–20% reduction in base shear compared to FB buildings. A notable lateral shift of superstructure is offered by LRB-induced flexibility. The reduction of story acceleration for response spectrum varies 30% on lower stories up to 70% on upper stories. The LRB systems with higher characteristic strength and relatively less isolation periods shows better productivity to minimize displacements in the bearing face for dropping structural shift. However, the LRB with comparatively lower characteristic strength and high isolation periods shows the most efficiency in controlling base shear, offering least story accelerations and consenting lower story inertia forces.

A universal method for the calibration of swing-scanning line structured light measurement system

Optik ◽  
2021 ◽  
pp. 166930
Author(s):  
Yuehua Li ◽  
Bochong Zhao ◽  
Jingbo Zhou ◽  
Youzhi Ren
Keyword(s):  
Measurement System ◽  
Structured Light ◽  
Universal Method ◽  
Light Measurement ◽  
Scanning Line

A one-dimensional self-gravitating stellar gas

1966 ◽  
Vol 25 ◽  
pp. 46-48 ◽  
Author(s):  
M. Lecar
Keyword(s):  
Gravitational Field ◽  
Phase Space ◽  
Motion Picture ◽  
Space Distribution ◽  
Two Dimensional ◽  
One Dimensional ◽  
Phase Space Distribution ◽  
Dimensional Phase Space ◽  
The Mean

“Dynamical mixing”, i.e. relaxation of a stellar phase space distribution through interaction with the mean gravitational field, is numerically investigated for a one-dimensional self-gravitating stellar gas. Qualitative results are presented in the form of a motion picture of the flow of phase points (representing homogeneous slabs of stars) in two-dimensional phase space.

An Attack on the Contamination Problem in the Electron Microscope

1967 ◽  
Vol 25 ◽  
pp. 368-368
Author(s):  
J. J. Kelsch ◽  
A. Holtz
Keyword(s):  
Electron Microscope ◽  
Pressure Gradient ◽  
Ionization Potential ◽  
Simple Solution ◽  
Specimen Surface ◽  
Contamination Rate ◽  
Local Pressure ◽  
High Ionization ◽  
Hydrocarbon Molecules ◽  
Contamination Problem

A simple solution to the serious problem of specimen contamination in the electron microscope is presented. This is accomplished by the introduction of clean helium into the vacuum exactly at the specimen position. The local pressure gradient thus established inhibits the migration of hydrocarbon molecules to the specimen surface. The high ionization potential of He permits the use of relatively large volumes of the gas, without interfering with gun stability. The contamination rate is reduced on metal samples by a factor of 10.

Experiments in Bright-Field Imaging with Hollow-Cone Illumination

1981 ◽  
Vol 39 ◽  
pp. 226-227
Author(s):  
W. Kunath ◽  
K. Weiss ◽  
E. Zeitler
Keyword(s):  
Signal To Noise Ratio ◽  
Carbon Support ◽  
Electronic System ◽  
Optic Axis ◽  
Hollow Cone ◽  
Signal To Noise ◽  
Bright Field ◽  
Noise Ratio ◽  
Single Field ◽  
Field Imaging

Bright-field images taken with axial illumination show spurious high contrast patterns which obscure details smaller than 15 ° Hollow-cone illumination (HCI), however, reduces this disturbing granulation by statistical superposition and thus improves the signal-to-noise ratio. In this presentation we report on experiments aimed at selecting the proper amount of tilt and defocus for improvement of the signal-to-noise ratio by means of direct observation of the electron images on a TV monitor.Hollow-cone illumination is implemented in our microscope (single field condenser objective, Cs = .5 mm) by an electronic system which rotates the tilted beam about the optic axis. At low rates of revolution (one turn per second or so) a circular motion of the usual granulation in the image of a carbon support film can be observed on the TV monitor. The size of the granular structures and the radius of their orbits depend on both the conical tilt and defocus.

Principles of Low-Vacuum SEM

1992 ◽  
Vol 50 (2) ◽  
pp. 1304-1305
Author(s):  
Klaus-Ruediger Peters
Keyword(s):  
New Technologies ◽  
High Vacuum ◽  
Optical Microscope ◽  
Specimen Surface ◽  
Electrical Field ◽  
Gaseous Environment ◽  
New Information ◽  
Gas Molecules ◽  
New Interactions ◽  
Gas Pressures

Only recently it became possible to expand scanning electron microscopy to low vacuum and atmospheric pressure through the introduction of several new technologies. In principle, only the specimen is provided with a controlled gaseous environment while the optical microscope column is kept at high vacuum. In the specimen chamber, the gas can generate new interactions with i) the probe electrons, ii) the specimen surface, and iii) the specimen-specific signal electrons. The results of these interactions yield new information about specimen surfaces not accessible to conventional high vacuum SEM. Several microscope types are available differing from each other by the maximum available gas pressure and the types of signals which can be used for investigation of specimen properties.Electrical non-conductors can be easily imaged despite charge accumulations at and beneath their surface. At high gas pressures between 10-2 and 2 torr, gas molecules are ionized in the electrical field between the specimen surface and the surrounding microscope parts through signal electrons and, to a certain extent, probe electrons. The gas provides a stable ion flux for a surface charge equalization if sufficient gas ions are provided.

Specimen Preparation of Near Surface Ion Irradiated Samples

1985 ◽  
Vol 43 ◽  
pp. 170-171
Author(s):  
K. F. Russell ◽  
L. L. Horton
Keyword(s):  
Radiation Damage ◽  
Heavy Ions ◽  
Target Material ◽  
Metal Alloys ◽  
Specimen Surface ◽  
Specimen Preparation ◽  
Particle Accelerators ◽  
Near Surface ◽  
Graaff Accelerator ◽  
Van De Graaff

Beams of heavy ions from particle accelerators are used to produce radiation damage in metal alloys. The damaged layer extends several microns below the surface of the specimen with the maximum damage and depth dependent upon the energy of the ions, type of ions, and target material. Using 4 MeV heavy ions from a Van de Graaff accelerator causes peak damage approximately 1 μm below the specimen surface. To study this area, it is necessary to remove a thickness of approximately 1 μm of damaged metal from the surface (referred to as “sectioning“) and to electropolish this region to electron transparency from the unirradiated surface (referred to as “backthinning“). We have developed electropolishing techniques to obtain electron transparent regions at any depth below the surface of a standard TEM disk. These techniques may be applied wherever TEM information is needed at a specific subsurface position.

Texture measurements in Al2O3 using BEKP

1994 ◽  
Vol 52 ◽  
pp. 608-609
Author(s):  
M. D. Vaudin ◽  
J. P. Cline
Keyword(s):  
Neutron Diffraction ◽  
Rapid Method ◽  
Crystallographic Orientation ◽  
Specimen Surface ◽  
X Ray Diffraction ◽  
Anisotropic Crystal ◽  
X Ray ◽  
Verification Method ◽  
Crystal Properties ◽  
Backscattered Electron

The study of preferred crystallographic orientation (texture) in ceramics is assuming greater importance as their anisotropic crystal properties are being used to advantage in an increasing number of applications. The quantification of texture by a reliable and rapid method is required. Analysis of backscattered electron Kikuchi patterns (BEKPs) can be used to provide the crystallographic orientation of as many grains as time and resources allow. The technique is relatively slow, particularly for noncubic materials, but the data are more accurate than any comparable technique when a sufficient number of grains are analyzed. Thus, BEKP is well-suited as a verification method for data obtained in faster ways, such as x-ray or neutron diffraction. We have compared texture data obtained using BEKP, x-ray diffraction and neutron diffraction. Alumina specimens displaying differing levels of axisymmetric (0001) texture normal to the specimen surface were investigated.BEKP patterns were obtained from about a hundred grains selected at random in each specimen.

The buckling of thin EM specimens

1990 ◽  
Vol 48 (4) ◽  
pp. 850-851
Author(s):  
A.R. Thölén
Keyword(s):  
Electron Microscope ◽  
Elastic Properties ◽  
Crystal Surface ◽  
Specimen Surface ◽  
Radius Of Curvature ◽  
Thin Foils ◽  
Thin Electron ◽  
Regular Patterns

Thin electron microscope specimens often contain irregular bend contours (Figs. 1-3). Very regular bend patterns have, however, been observed around holes in some ion-milled specimens. The purpose of this investigation is twofold. Firstly, to find the geometry of bent specimens and the elastic properties of extremely thin foils and secondly, to obtain more information about the background to the observed regular patterns.The specimen surface is described by z = f(x,y,p), where p is a parameter, eg. the radius of curvature of a sphere. The beam is entering along the z—direction, which coincides with the foil normal, FN, of the undisturbed crystal surface (z = 0). We have here used FN = [001]. Furthermore some low indexed reflections are chosen around the pole FN and in our fcc crystal the following g-vectors are selected:

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