scholarly journals Precise SEM Cross Section Polishing via Argon Beam Milling

2006 ◽  
Vol 14 (3) ◽  
pp. 22-25 ◽  
Author(s):  
N. Erdman ◽  
R. Campbell ◽  
S. Asahina

SEM observation of a specimen cross section can provide important information for research and development as well as failure analysis. In most cases, surface observation alone cannot provide information concerning the cross sectional structure of granular materials, layered materials, fibrous materials, and powders. Preparing highly-polished cross sections of these materials is both a science and an art.Typically, a cross section is prepared using mechanical means like conventional mechanical polishing methods or a microtome. The sample is first embedded in a holder or device, and then polished to achieve a flat cross section. In some cases, a staining procedure is used to highlight a specific component of the sample. Such methods can be lengthy procedures that require a great deal of skill, and can introduce artifacts into soft materials, deform the material around voids, or compress layers of soft and hard materials in composite samples. Mechanical polishing can miss fine details such as the presence of hairline cracks, and present a challenge to water-soluble phases.

2012 ◽  
Vol 27 (2) ◽  
pp. 264-269 ◽  
Author(s):  
Christian Lorbach ◽  
Ulrich Hirn ◽  
Johannes Kritzinger ◽  
Wolfgang Bauer

Abstract We present a method for 3D measurement of fiber cross sectional morphology from handsheets. An automated procedure is used to acquire 3D datasets of fiber cross sectional images using an automated microtome and light microscopy. The fiber cross section geometry is extracted using digital image analysis. Simple sample preparation and highly automated image acquisition and image analysis are providing an efficient tool to analyze large samples. It is demonstrated that if fibers are tilted towards the image plane the images of fiber cross sections are always larger than the true fiber cross section geometry. In our analysis the tilting angles of the fibers to the image plane are measured. The resulting fiber cross sectional images are distorted to compensate the error due to fiber tilt, restoring the true fiber cross sectional shape. We use an approximated correction, the paper provides error estimates of the approximation. Measurement results for fiber wall thickness, fiber coarseness and fiber collapse are presented for one hardwood and one softwood pulp.


2020 ◽  
Author(s):  
J. Lee ◽  
et al.

<div>Figure 6. Interpretative cross sections illustrating the cross-sectional geometry of several paleovalleys. See Figure 3 for location of all cross sections and Figure 8 for location of cross section CCʹ. Cross sections AAʹ and BBʹ are plotted at the same scale, and cross section CCʹ is plotted at a smaller scale. Figure 6 is intended to be viewed at a width of 45.1 cm.</div>


2021 ◽  
Vol 15 (58) ◽  
pp. 77-85
Author(s):  
Amor Bouaricha ◽  
Naoual Handel ◽  
Aziza Boutouta ◽  
Sarah Djouimaa

In this experimental work, strength results obtained on short columns subjected to concentric loads are presented. The specimens used in the tests have made of cold-rolled, thin-walled steel. Twenty short columns of the same cross-section area and wall thickness have been tested as follows: 8 empty and 12 filled with ordinary concrete. In the aim to determine the column section geometry with the highest resistance, three different types of cross-sections have been compared: rectangular, I-shaped unreinforced and, reinforced with 100 mm spaced transversal links. The parameters studied are the specimen height and the cross-sectional steel geometry. The registered experimental results have been compared to the ultimate loads intended by Eurocode 3 for empty columns and by Eurocode 4 for compound columns. These results showed that a concrete-filled composite column had improved strength compared to the empty case. Among the three cross-section types, it has been found that I-section reinforced is the most resistant than the other two sections. Moreover, the load capacity and mode of failure have been influenced by the height of the column. Also, it had noted that the experimental strengths of the tested columns don’t agree well with the EC3 and EC4 results.


Author(s):  
Lawrence N Virgin

Locating the shear, or flexural, center of non-symmetric cross-sectional beams is a key element in the teaching of structural mechanics. That is, establishing the point on the plane of the cross-section where an applied load, generating a bending moment about a principal axis, results in uni-directional deflection, and no twisting. For example, in aerospace structures it is particularly important to assess the propensity of an airfoil section profile to resist bending and torsion under the action of aerodynamic forces. Cross-sections made of thin-walls, whether of open or closed form are of special practical importance and form the basis of the material in this paper. The advent of 3D-printing allows the development of tactile demonstration models based on non-trivial geometry and direct observation.


Author(s):  
Xiaokang Xin ◽  
Fengpeng Bai ◽  
Kefeng Li

A numerical model based on the Saint-Venant equations (one-dimensional shallow water equations) is proposed to simulate shallow flows in an open channel with regular and irregular cross-section shapes. The Saint-Venant equations are solved by the finite-volume method based on Godunov-type framework with a modified Harten, Lax, and van Leer (HLL) approximate Riemann solver. Cross-sectional area is replaced by water surface level as one of primitive variables. Two numerical integral algorithms, compound trapezoidal and Gauss–Legendre integrations, are used to compute the hydrostatic pressure thrust term for natural streams with arbitrary and irregular cross-sections. The Monotonic Upstream-Centered Scheme for Conservation Laws (MUSCL) and second-order Runge–Kutta methods is adopted to achieve second-order accuracy in space and time, respectively. The performance of the resulting scheme is evaluated by application in rectangular channels, trapezoidal channels, and a natural mountain river. The results are compared with analytical solutions and experimental or measured data. It is demonstrated that the numerical scheme can simulate shallow flows with arbitrary cross-section shapes in practical conditions.


Author(s):  
Ehsan Sadeghi ◽  
Majid Bahrami ◽  
Ned Djilali

In many practical instances such as basic design, parametric study, and optimization analysis of thermal systems, it is often very convenient to have closed form relations to obtain the trends and a reasonable estimate of the Nusselt number. However, finding exact solutions for many practical singly-connected cross-sections, such as trapezoidal microchannels, is complex. In the present study, the square root of cross-sectional area is proposed as the characteristic length scale for Nusselt number. Using analytical solutions of rectangular, elliptical, and triangular ducts, a compact model for estimation of Nusselt number of fully-developed, laminar flow in microchannels of arbitrary cross-sections with “H1” boundary condition (constant axial wall heat flux with constant peripheral wall temperature) is developed. The proposed model is only a function of geometrical parameters of the cross-section, i.e., area, perimeter, and polar moment of inertia. The present model is verified against analytical and numerical solutions for a wide variety of cross-sections with a maximum difference on the order of 9%.


2005 ◽  
Vol 871 ◽  
Author(s):  
Han Young Woo ◽  
Dmitry Korystov ◽  
Alexander Mikhailovsky ◽  
Guillermo C. Bazan

AbstractA series of tetradonor substituted [2.2]paracyclophane-based two-photon absorption (TPA) fluorophores were designed, synthesized and characterized. Different substituents were chosen to modulate the conjugation and the donor strength and to allow the molecules to be neutral (N series, organic-soluble) or charged (C series, water-soluble). The overall set of compounds series allows us to examine the correlation among the solvent polarity, donor ability of the substituents, and TPA action cross section (ηδd, where δ is the TPA cross section and η is the quantum yield). In water, a significant drop of both δ and η is observed, approximately one-third relative to those in toluene. Weaker donors and/or weaker acceptors with enhanced conjugation are a better choice due to a minimized quenching related to strong charge transfer (CT) upon excitation. One thus needs to fine-tune the magnitude of CT and find an optimal balance among CT,δ and η.


2011 ◽  
Vol 18 (4) ◽  
pp. 555-562 ◽  
Author(s):  
Bulent Yardimoglu ◽  
Levent Aydin

Longitudinal natural vibration frequencies of rods (or bars) with variable cross-sections are obtained from the exact solutions of differential equation of motion based on transformation method. For the rods having cross-section variations as power of the sinusoidal functions ofax+b, the differential equation is reduced to associated Legendre equation by using the appropriate transformations. Frequency equations of rods with certain cross-section area variations are found from the general solution of this equation for different boundary conditions. The present solutions are benchmarked by the solutions available in the literature for the special case of present cross-sectional variations. Moreover, the effects of cross-sectional area variations of rods on natural characteristics are studied with numerical examples.


2010 ◽  
Vol 638-642 ◽  
pp. 1579-1584 ◽  
Author(s):  
A.V. Nagasekhar ◽  
Carlos H. Cáceres ◽  
Mark Easton

Specimens of rectangular and circular cross section of a Mg-9Al binary alloy have been tensile tested and the cross section of undeformed specimens examined using scanning electron microscopy. The rectangular cross sections showed three scales in the cellular intermetallics network: coarse at the core, fine at the surface and very fine at the corners, whereas the circular ones showed only two, coarse at the core and fine at the surface. The specimens of rectangular cross section exhibited higher yield strength in comparison to the circular ones. Possible reasons for the observed increased strength of the rectangular sections are discussed.


2014 ◽  
Vol 679 ◽  
pp. 1-5 ◽  
Author(s):  
Sumayah Abdulsalam Mustafa ◽  
Mohd Zulham Affandi bin Mohd Zahid ◽  
Md.Hadli bin Abu Hassan

Cross sectional areas optimization is to be implemented to study the influence of the cross section shape on the optimum truss weight. By the aid of analysis and design engines with advanced finite element analysis that is the steel design software STAAD. Four rolled steel sections (angle, tube, channel, and pipe) which are used in industrial roof trusses are applied for comparison. Many previous studies, use the areas of cross sections as design variables without highlight to the shape of cross section at the start of the process, consequently the result area will be adequate if the designer choose the effective shape than others. Results of this research show that the chosen cross section shape has a significant impact on the optimum truss weight for same geometry of truss type under the same circumstances of loading and supports.


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