scholarly journals Osteogenic capacity of mixed-acid and heat-treated titanium mesh prepared by a selective laser melting technique

RSC Advances ◽  
2018 ◽  
Vol 8 (46) ◽  
pp. 26069-26077
Author(s):  
Kayoko Yamamoto ◽  
Seiji Yamaguchi ◽  
Tomiharu Matsushita ◽  
Shigeo Mori ◽  
Azumi Hirata ◽  
...  

The practical use of additive manufacturing to create artificial bone as a material for repairing complex bone defects is currently attracting attention.

Materials ◽  
2021 ◽  
Vol 14 (18) ◽  
pp. 5360
Author(s):  
Naoko Imagawa ◽  
Kazuya Inoue ◽  
Keisuke Matsumoto ◽  
Michi Omori ◽  
Kayoko Yamamoto ◽  
...  

Jaw reconstruction using an additive-manufacturing titanium artificial bone (AMTAB) has recently attracted considerable attention. The synthesis of a titanium artificial bone is based on three-dimensional computed tomography images acquired before surgery. A histological evaluation of porous AMTAB (pAMTAB) embedded in rat calvarial bone defects was conducted. This study examined three groups: rats implanted with mixed-acid and heat-treated pAMTAB, rats implanted with untreated pAMTAB, and rats with no implant. In both pAMTAB groups, bone defects were created in rat calvarial bones using a 5-mm trephine bar, followed by pAMTAB implantation. The pAMTAB was fixed to the defect using the fitting force of the surrounding bones. The rats were sacrificed at 4, 8, and 16 weeks after implantation, and the skull was dissected. Undecalcified ground slides were prepared and stained with Villanueva Goldner. Compared with the no implant control group, both pAMTAB groups exhibited new bone formation inside the defect, with greater bone formation in the mixed-acid and heat-treated pAMTAB group than in the untreated pAMTAB group, but the difference was not significant. These data suggest that pAMTAB induces bone formation after implantation in bone defects. Bone formation appears to be enhanced by prior mixed-acid and heat-treated pAMTAB.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3668
Author(s):  
Tian Xia ◽  
Rui Wang ◽  
Zhongnan Bi ◽  
Guoliang Zhu ◽  
Qingbiao Tan ◽  
...  

Additive manufacturing (AM) of nickel-based superalloys is of high interest for application in complex hot end parts. However, it has been widely suggested that the microstructure-properties of the additive manufacturing processed superalloys are not yet fully clear. In this study, the GTD222, an important superalloy for high-temperature hot-end part, were prepared using selective laser melting and then subjected to heat treatment. The microstructure evolution of the GTD222 was investigated and the mechanical properties of heat treated GTD222 were tested. The results have shown that the grain size of the heat treated GTD222 was close to its as-built counterparts. Meanwhile, a large amount of γ’ and nano-scaled carbides were precipitated in the heat treated GTD222. The microstructure characteristics implied that the higher strength of the heat treated GTD222 can be attributed to the γ’ and nano-scaled carbides. This study provides essential microstructure and mechanical properties information for optimizing the heat treatment process of the AM processed GTD222.


2017 ◽  
Vol 26 (3) ◽  
pp. 257-260 ◽  
Author(s):  
Kayoko Yamamoto ◽  
Seiji Yamaguchi ◽  
Tomiharu Matsushita ◽  
Shigeo Mori ◽  
Hisashi Kitagaki ◽  
...  

Author(s):  
D. Ahmadkhaniha ◽  
H. Möller ◽  
C. Zanella

AbstractSelective laser melting is one of the additive manufacturing technologies that have been known for building various and complicated shapes. Despite numerous advantages of additive manufacturing technologies, they strongly influence the microstructure and typically show a relatively high surface roughness. In this study, maraging steel was produced by selective laser melting (SLM), and its microstructure, hardness and corrosion behavior before and after heat treatment were studied and compared to traditionally manufactured ones (wrought, forged samples). In addition, the effect of electropolishing on the surface roughness was evaluated. The microstructural study was carried out by scanning electron microscopy equipped with electron backscattered diffraction in three different sections: parallel to the top surface (xy), transverse cross section (xz) and longitudinal cross section (yz). The same characterization was applied to heat-treated samples, austenitized and quenched as well as the aged ones. The results showed that selective laser melting produced a fine grain martensitic structure (in the as-printed condition) with a surface roughness (Ra) of about 10 µm. There was no sign of preferred texture or anisotropy in the microstructure of as-print SLM materials. The SLM microstructure was similar in all 3 sections (xy, xz and yz). Despite finer microstructure, nano-hardness and corrosion behavior of SLM and conventional wrought maraging steel in heat-treated conditions were similar. Aging resulted in the maximum nano-hardness and the minimum corrosion potential values. Precipitation has the main role in both hardness and corrosion behavior. Electropolishing was optimized and reduced the surface roughness (Ra) by 65%.


Author(s):  
Filippo Simoni ◽  
Andrea Huxol ◽  
Franz-Josef Villmer

AbstractIn the last years, Additive Manufacturing, thanks to its capability of continuous improvements in performance and cost-efficiency, was able to partly replace and redefine well-established manufacturing processes. This research is based on the idea to achieve great cost and operational benefits especially in the field of tool making for injection molding by combining traditional and additive manufacturing in one process chain. Special attention is given to the surface quality in terms of surface roughness and its optimization directly in the Selective Laser Melting process. This article presents the possibility for a remelting process of the SLM parts as a way to optimize the surfaces of the produced parts. The influence of laser remelting on the surface roughness of the parts is analyzed while varying machine parameters like laser power and scan settings. Laser remelting with optimized parameter settings considerably improves the surface quality of SLM parts and is a great starting point for further post-processing techniques, which require a low initial value of surface roughness.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3603
Author(s):  
Tim Pasang ◽  
Benny Tavlovich ◽  
Omry Yannay ◽  
Ben Jakson ◽  
Mike Fry ◽  
...  

An investigation of mechanical properties of Ti6Al4V produced by additive manufacturing (AM) in the as-printed condition have been conducted and compared with wrought alloys. The AM samples were built by Selective Laser Melting (SLM) and Electron Beam Melting (EBM) in 0°, 45° and 90°—relative to horizontal direction. Similarly, the wrought samples were also cut and tested in the same directions relative to the plate rolling direction. The microstructures of the samples were significantly different on all samples. α′ martensite was observed on the SLM, acicular α on EBM and combination of both on the wrought alloy. EBM samples had higher surface roughness (Ra) compared with both SLM and wrought alloy. SLM samples were comparatively harder than wrought alloy and EBM. Tensile strength of the wrought alloy was higher in all directions except for 45°, where SLM samples showed higher strength than both EBM and wrought alloy on that direction. The ductility of the wrought alloy was consistently higher than both SLM and EBM indicated by clear necking feature on the wrought alloy samples. Dimples were observed on all fracture surfaces.


2019 ◽  
Vol 813 ◽  
pp. 171-177 ◽  
Author(s):  
Giacomo Maculotti ◽  
Gianfranco Genta ◽  
Massimo Lorusso ◽  
Maurizio Galetto

Selective Laser Melting (SLM) is one of the leader metal Additive Manufacturing (AM) processes thanks to its capability of coupling freeform design and environmental and economical sustainability to high mechanical properties. AlSi10Mg is a light weight Al-alloy with interesting processing properties and enhanced strength thanks to the presence of Mg, which, hence, finds application in several industrial fields. Furthermore, SLM allows overcoming those design constraints set by casting and melt spinning; however, SLM AlSi10Mg components require to be heat treated, both to strengthen the material and to engineer the microstructure. In this work, in order to assess the effectiveness of heat treatments on AlSi10Mg by SLM, an ad hoc analysis procedure based on statistical tools is applied in combination with indentation characterisation tests. In particular, to achieve full scale characterisation, traditional Brinell hardness and Instrumented Indentation Test (IIT) in macro and nano-range are considered. In particular, IIT is applied both at the lower end of macro range to provide consistency and statistically investigate relationship with Brinell scale and in the nano-range, enabling local, i.e. grain, and surface properties to be characterised.


Author(s):  
Weipeng Duan ◽  
Meiping Wu ◽  
Jitai Han

TC4, which is one of the most widely used titanium alloy, is frequently used in biomedical field due to its biocompatible. In this work, selective laser melting (SLM) was used to manufacture TC4 parts and the printed parts were heat-treated using laser rescanning technology. The experimental results showed that laser rescanning had a high impact on the quality of SLMed part, and a different performance on wear resistance can be found on the basis. It can be seen that the volume porosity of the sample was 7.6 ± 0.5% without using any further processing technology. The volume porosity of the sample processed using laser rescanning strategy was decreased and the square-framed rescanning strategy had a relative optimal volume porosity (1.5 ± 0.3%) in all these five samples. With the further decreasing of volume porosity, the wear resistance decreased at the same time. As its excellent bio-tribological properties, the square-framed rescanning may be a potential suitable strategy to forming TC4 which used in human body.


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