scholarly journals Structure, electronic properties, morphology evolution, and photocatalytic activity in PbMoO4 and Pb1−2xCaxSrxMoO4 (x = 0.1, 0.2, 0.3, 0.4 and 0.5) solid solutions

2020 ◽  
Vol 22 (44) ◽  
pp. 25876-25891
Author(s):  
E. O. Gomes ◽  
L. Gracia ◽  
A. A. G. Santiago ◽  
R. L. Tranquilin ◽  
F. V. Motta ◽  
...  
Keyword(s):  
Photocatalytic Activity ◽  
Electronic Properties ◽  
Solid Solutions ◽  
Precipitation Method ◽  
Morphology Evolution ◽  
Water Based ◽  
Co Precipitation ◽  
First Time

In this work PbMoO4 and Pb1−2xCaxSrxMoO4 (x = 0.1, 0.2, 0.3, 0.4 and 0.5) solid solutions have been successfully prepared, for the first time, by a simple co-precipitation method and the as-synthesized samples were subjected to a water-based reflux treatment.

Photocatalytic Activity of Fe-Doped ZnO/Montmorillonite Nanocomposite for Degradation of Malachite Green

2015 ◽  
Vol 827 ◽  
pp. 19-24 ◽  
Author(s):  
Nur Afifah ◽  
Nadia Febiana Djaja ◽  
Rosari Saleh
Keyword(s):  
Photocatalytic Activity ◽  
Malachite Green ◽  
Organic Dyes ◽  
Uv Light ◽  
Precipitation Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Spin Resonance ◽  
Doped Zno ◽  
Co Precipitation

In this study, the photocatalytic activity of pure Fe- doped ZnO and Fe- doped ZnO/Montmorillonite nanocomposite has been investigated for the degradation of malachite green under UV light irradiation. Both photocatalysts were synthesized using co-precipitation method and characterized by X-ray diffraction, energy dispersive X-ray spectroscopy, Fourier-transform infrared absorption, and electron spin resonance. The results showed that the photocatalytic efficiency is better in the presence of montmorillonite compared to pure Fe- doped ZnO. To detect the possible reactive species involved in degradation of organic dyes control experiments with introducing scavengers into the solution of organic dyes were carried out. It is found that electron plays an important role in the degradation of malachite green.

Improved photocatalytic activity for degradation of textile dyeing waste water and thiazine dyes using PbWO4 nanoparticles synthesized by co-precipitation method

2021 ◽  
pp. 111721
Author(s):  
K. Asha ◽  
C. Hentry ◽  
M.R. Bindhu ◽  
Amal M. Al-Mohaimeed ◽  
Mohamed Ragab AbdelGawwad ◽  
...  
Keyword(s):  
Waste Water ◽  
Photocatalytic Activity ◽  
Precipitation Method ◽  
Textile Dyeing ◽  
Thiazine Dyes ◽  
Co Precipitation

scholarly journals Nitrogen and Bromide Co-Doped Hydroxyapatite Thin Films with Antimicrobial Properties

Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1505
Author(s):  
Simona Liliana Iconaru ◽  
Carmen Steluta Ciobanu ◽  
Daniela Predoi ◽  
Mikael Motelica-Heino ◽  
Constantin Cătălin Negrilă ◽  
...  
Keyword(s):  
Thin Films ◽  
Antimicrobial Activity ◽  
Spin Coating ◽  
Thin Layers ◽  
Precipitation Method ◽  
X Ray ◽  
Co Precipitation ◽  
First Time ◽  
Co Doped

Hydroxyapatite (Ca10(PO4)6(OH)2, HAp), due to its high biocompatibility, is widely used as biomaterial. Doping with various ions of hydroxyapatite is performed to acquire properties as close as possible to the biological apatite present in bones and teeth. In this research the results of a study performed on thin films of hydroxyapatite co-doped with nitrogen and bromine (NBrHAp) are presented for the first time. The NBrHAp suspension was obtained by performing the adapted co-precipitation method using cetyltrimethylammonium bromide (CTAB). The thin layers of NBrHAp were obtained by spin-coating. The stability of the NBrHAp suspension was examined by ultrasound measurements. The thin layers obtained by the spin-coating method were examined by scanning electron microscopy (SEM), optical microscopy (OM), and metallographic microscopy (MM). The presence of nitrogen and bromine were highlighted by energy-dispersive X-ray spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS) studies. Fourier transform infrared spectroscopy (FTIR) was used to highlight the chemical status of nitrogen and bromine. In addition, the powder obtained from the NBrHAp suspension was analyzed by XRD. Moreover, the in vitro antimicrobial activity of the NBrHAp suspensions and coatings was investigated using the reference microbial strains Staphylococcus aureus ATCC 25923, Escherichia coli ATCC 25922, and Candida albicans ATCC 10231. The results highlighted the successful obtainment of N and Br co-doped hydroxyapatite suspension for the first time by an adapted co-precipitation method. The obtained suspension was used to produce pure NBrHAp composite thin films with superior morphological properties. The NBrHAp suspensions and coatings exhibited in vitro antimicrobial activity against bacterial and fungal strains and revealed their good antimicrobial activity.

One-step co-precipitation method to construct black phosphorus nanosheets/ZnO nanohybrid for enhanced visible light photocatalytic activity

2019 ◽  
Vol 497 ◽  
pp. 143682 ◽  
Author(s):  
Shutao Li ◽  
Pengfei Wang ◽  
Rendong Wang ◽  
Yifan Liu ◽  
Ruisen Jing ◽  
...  
Keyword(s):  
Photocatalytic Activity ◽  
Visible Light ◽  
Black Phosphorus ◽  
Precipitation Method ◽  
Visible Light Photocatalytic Activity ◽  
One Step ◽  
Co Precipitation ◽  
Visible Light Photocatalytic

Synthesis of tin oxide activated by DAN grafting and Mo nanoparticle insertion for optoelectronic properties improvement

RSC Advances ◽  
2016 ◽  
Vol 6 (98) ◽  
pp. 95405-95416 ◽  
Author(s):  
N. Bouazizi ◽  
R. Bargougui ◽  
A. Benghnia ◽  
J. Vieillard ◽  
S. Ammar ◽  
...  
Keyword(s):  
Tin Oxide ◽  
Optoelectronic Properties ◽  
Precipitation Method ◽  
New Material ◽  
Co Precipitation ◽  
First Time

Tin oxide (SnO2) was synthesized via a co-precipitation method and activated by 1,5 diaminonaphthalene (DAN) grafting and molybdenum nanoparticle (Mo-NPs) incorporation for the first time as a new material.

Preparation of highly luminescent BaSO4 protected CdTe quantum dots as conversion materials for excellent color-rendering white LEDs

2015 ◽  
Vol 3 (12) ◽  
pp. 2831-2836 ◽  
Author(s):  
Yajing Chang ◽  
Xudong Yao ◽  
Zhongping Zhang ◽  
Danlu Jiang ◽  
Yalan Yu ◽  
...  
Keyword(s):  
Quantum Dots ◽  
Cdte Quantum Dots ◽  
Precipitation Method ◽  
White Leds ◽  
Conversion Materials ◽  
Co Precipitation ◽  
Color Rendering ◽  
First Time ◽  
Excellent Color ◽  
Inorganic Matrix

For the first time, colloidal CdTe quantum dots are incorporated into an inorganic matrix, BaSO4, through a co-precipitation method.

Facile preparation of mesoporous Cu–Sn solid solutions as active catalysts for CO oxidation

RSC Advances ◽  
2015 ◽  
Vol 5 (33) ◽  
pp. 25755-25764 ◽  
Author(s):  
Yarong Li ◽  
Honggen Peng ◽  
Xianglan Xu ◽  
Yue Peng ◽  
Xiang Wang
Keyword(s):  
Solid Solution ◽  
Co Oxidation ◽  
Water Vapour ◽  
Solid Solutions ◽  
Precipitation Method ◽  
Oxidation Activity ◽  
Facile Preparation ◽  
Co Precipitation

A mesoporous Cu0.5Sn0.5Oy solid solution catalyst with Caramel-Treats-like morphology prepared easily by co-precipitation method exhibits remarkably improved CO oxidation activity and potent resistance to water vapour deactivation.

Effect of calcination temperature on the photocatalytic activity of CaSb2O6 nanoparticles prepared by co-precipitation method

2014 ◽  
Vol 48 ◽  
pp. 29-32 ◽  
Author(s):  
Min Zhang ◽  
Liumin Chen ◽  
Shiyue Yao ◽  
Yumei Long ◽  
Weifeng Li ◽  
...  
Keyword(s):  
Photocatalytic Activity ◽  
Calcination Temperature ◽  
Precipitation Method ◽  
Co Precipitation

scholarly journals Study of co-precipitated nanomaterials magnetic MnxCo1-xFe2O4 (with x = 0.50 & 0.75) for Photocatalyst Application in MB degradation

2020 ◽  
Vol 4 (1) ◽  
pp. 36
Author(s):  
Wahid Sidik Sarifuddin ◽  
Utari Utari ◽  
Budi Purnama
Keyword(s):  
Magnetic Properties ◽  
Photocatalytic Activity ◽  
Crystallite Size ◽  
Life Time ◽  
Precipitation Method ◽  
Material Base ◽  
Lattice Constants ◽  
Ferrite Material ◽  
Ray Density ◽  
Co Precipitation

The crystalline structure and magnetic properties of Mn<sub>1-x</sub>Co<sub>x</sub>Fe<sub>2</sub>O<sub>4</sub> (x = 0 &amp; 0.25) was studied in this report. The ferrite materials were synthesized by the chemical co-precipitation method and calcinated at 1000<sup>o</sup>C for 5 hours. The obtained materials were characterized by FTIR, XRD and VSM, and for photocatalytic activity was measured by UV-Vis spectrometer. Vibration bands at tetrahedral and octahedral site were corresponded by <strong> </strong>= 581.56 cm<sup>-1</sup> and  = 465.83 cm<sup>-1</sup> and 474.51 cm<sup>-1</sup> . The obtained ferrite were confirmed by XRD as spinel structure and shown that the addition of number of Mn decreased crystallite size <em>(D)</em> and x-ray density (<em>ρ<sub>x</sub></em>), but lattice constants <em>(a)</em> increased. The crystallite size of samples with x = 0.50 was 34.85 nm, and x = 0.75 was 32.17 nm. The magnetic properties of nanoparticles shown that magnetization saturation <em>(</em><em>Ms)</em>from 42.05 emu/g to 54.16 emu/g increased with the addition of number of Mn. The coercive field (<em>H</em><sub>c</sub>)decreased from 408.27 Oe to 258.37 Oe. Photocatalytic activity was observed by UV-Vis spectrometer, where percentage of MB degradation <em>(E)</em> increase with the addition of number on Mn from 49.08% to 69.06%, either rate constant <em>(k<sub>app</sub>)</em> and half life time<em> (t<sub>1/2</sub>)</em>.  Furthermore, ferrite material base Mn-Co-ferrite has good characteristic to applied for photocatalyst.

scholarly journals Variation in the material properties by nickel substitution in copper tellurate

2020 ◽  
Author(s):  
Sudarshana Dhanarath Mardolkar ◽  
A. V. Salker
Keyword(s):  
Visible Region ◽  
Photoluminescence Property ◽  
Precipitation Method ◽  
Magnetic Studies ◽  
Dielectric Parameters ◽  
Chemical Route ◽  
Wide Range ◽  
Lower Temperature ◽  
Co Precipitation ◽  
First Time

Abstract A series of pristine and nickel doped copper tellurates possessing a wide range of applications are studied here. Use of a simple wet chemical route that is co-precipitation method has been employed for the first time, which involves the formation of desired compounds at a relatively lower temperature, thus modifying their properties. All the prepared compounds are characterized and investigated by XRD, TG – DTA, XPS, SEM, TEM to examine their phase purity, thermal stability, chemical state, and microstructural properties. The electrical resistivity studies showed an insulator - semiconductor transition behavior. Magnetic studies revealed the paramagnetic nature of the material. Antiferromagnetic to paramagnetic transition was observed at T N ~ 60 K in case of Cu 2.7 Ni 0.3 TeO 6 sample. Thermoelectric studies indicated a change in conduction mechanism with temperature. Dielectric properties with respect to frequency showed an increase in dielectric parameters with increasing dopant content. Photoluminescence property has been studied and found to show emission in the visible region.

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