scholarly journals Optimization of insoluble dietary fiber preparation technology from rosa roxburghii pomace by chemical method

2020 ◽  
Vol 145 ◽  
pp. 01027
Author(s):  
Zhou Xiao-li ◽  
Yang Yan-sheng ◽  
Yang Qiao-mei ◽  
Guan Qing-lin ◽  
Zhu Guang-xu

Rosa roxburghii residue as raw material, we studied the extraction process of dietary fiber from rosa roxburghii pomace by chemical method. The effects of temperature, time, pH, solid-liquid ratio on the IDF yield under the effect of alkali and acid were explored by single factor experiments and orthogonal experiment. The results showed that the optimal condition of extracting IDF was as follows: the 60 mesh rosa roxburghii pomace were 80 min in water bath at 60°C under the condition of the solid-liquid ratio 1:15 and the pH 12; and then rosa roxburghii pomace were 100 min in water bath at 50°C on the condition of the solid-liquid ratio 1:15, and pH 3.0 after rinsing, the average IDF yield which reached (86.3±1.0)%. This experiment provides experimental basis for the selection of dietary fiber raw materials, and also provides theoretical basis for increasing the added value of rosa roxburghii.

Foods ◽  
2021 ◽  
Vol 10 (3) ◽  
pp. 485
Author(s):  
Vera Schmid ◽  
Antje Trabert ◽  
Judith (Schäfer) Keller ◽  
Mirko Bunzel ◽  
Heike P. Karbstein ◽  
...  

Food by-products can be used as natural and sustainable food ingredients. However, a modification is needed to improve the technofunctional properties according to the specific needs of designated applications. A lab-scale twin-screw extruder was used to process enzymatically treated apple pomace from commercial fruit juice production. To vary the range of the thermomechanical treatment, various screw speeds (200, 600, 1000 min−1), and screw configurations were applied to the raw material. Detailed chemical and functional analyses were performed to develop a comprehensive understanding of the impact of the extrusion processing on apple pomace composition and technofunctional properties as well as structures of individual polymers. Extrusion at moderate thermomechanical conditions increased the water absorption, swelling, and viscosity of the material. An increase in thermomechanical stress resulted in a higher water solubility index, but negatively affected the water absorption index, viscosity, and swelling. Scanning electron microscopy showed an extrusion-processing-related disruption of the cell wall. Dietary fiber analysis revealed an increase of soluble dietary fiber from 12.6 to 17.2 g/100 g dry matter at maximum thermo-mechanical treatment. Dietary fiber polysaccharide analysis demonstrated compositional changes, mainly in the insoluble dietary fiber fraction. In short, pectin polysaccharides seem to be susceptible to thermo-mechanical stress, especially arabinans as neutral side chains of rhamnogalacturonan I.


2014 ◽  
Vol 1082 ◽  
pp. 106-111
Author(s):  
Yu Hong Yang ◽  
Zong Li Kang ◽  
Rui Xin Guo ◽  
Hong Ling Wang ◽  
Zhuo Wang ◽  
...  

We had studied using single factor and orthogonal experimental design method for extracted from actinidia arguta of wild fructification polyphenols conditions optimization, as actinidia arguta of wild raw material. The results showed that: extracted from actinidia arguta of wild fructification polyphenols optimization the best conditions is acetone solution of 30 percent, according to the solid-liquid ratio of 1:9, at 35°C, the extraction 30 min best, the amount of polyphenols extracted 763.8 mg / L.


2019 ◽  
Vol 11 (11) ◽  
pp. 1607-1611
Author(s):  
Lifeng Cheng ◽  
Shengwen Duan ◽  
Xiangyuan Feng ◽  
Ke Zheng ◽  
Qi Yang ◽  
...  

Pectin was extracted from Ramie [Boehmeria nivea (L.) Gaud] through ammonium oxalate extraction method. The influences of single factors (ammonium oxalate concentration, extraction time, solid–liquid ratio, and reaction temperature) on the yield of ramie pectin were studied. Orthogonal experiment was then performed to optimize the combination of the given conditions using pectin yield as the measuring indicator. Finally, the partial physicochemical properties of ramie pectin extracted in the optimal conditions were analyzed. Results showed that the optimal conditions for single-element experiment were 3.5 h (extraction time), 1:25 (solid–liquid ratio), 0.85% (concentration of ammonium oxalate) and 95 °C (extraction temperature), and that the optimal combination conditions for orthogonal experiment was 4 h, 1:30, 0.95% and 90 °C. The ramie pectin yield extracted in optimal conditions reached 15.81%, and its protein content, galacturonic acid content, and esterification degree were 0.659 mg/g, 49.92%, and 53.11%, respectively. Therefore, the proposed method was successfully applied to obtain ramie pectin and may provide scientific basis for improving the multi-utilization value of ramie.


2021 ◽  
Author(s):  
Youshan Sun ◽  
Xuyang Zhang ◽  
Fei Wang ◽  
Meiyan Wang

Abstract Calcium peroxide (CaO2) pretreatment was employed to remove lignin and subsequently facilitate enzymatic digestibility of wheat straw. An optimal condition was obtained at 130°C for 10 min with 0.35 g CaO2/g dried material of wheat straw and a 1:8 solid-liquid ratio. Under this condition, 57.8% of initial lignin, 7.2% of initial glucan, and 30.6% of initial xylan were removed from CaO2 pretreatment, respectively, meanwhile, a glucose recovery of 90.6 % and a xylose recovery of 65.9 % were obtained from the subsequent enzymatic hydrolysis of treated wheat straw, respectively. CaO2 pretreatment was proved to be a very effective method in delignification and improving enzymatic digestibility. Compared to raw material, the complex structure of lignocellulose was drastically disrupted with a wide emergence of scaly bulges and fully exposed microfibers, which still retained in the solid.


2021 ◽  
Vol 292 ◽  
pp. 03079
Author(s):  
Hui-hui Li ◽  
Rong Huang ◽  
Ming-chen Li

Cordyceps flower is a new resource as a food and drug, which has a broad market prospect. The paper using Cordyceps flower sporocarp as raw material and adopting sensory results as evaluation criteria, through single factor and orthogonal experiments optimize cordyceps flower beverage formula. The results show that Cordyceps powder should be first leached in a water bath at 80℃ for 15 min at a feed-liquid ratio of 1:30. After centrifugation and filtration, cordyceps flower liquid was obtained. Then the liquid should be reconstitute into 30% diluent. Third, adding 0.04% aspartame, 0.06% citric acid and 0.1% sodium carboxyl methyl cellulose (CMC), a tasty and nutritious cordyceps flower beverage was developed ultimately.


2013 ◽  
Vol 2013 ◽  
pp. 1-3 ◽  
Author(s):  
Chen Leishan ◽  
Wang Cunjing ◽  
Miao Yu ◽  
Chen Gairong

The reactions were performed to synthesize carbon materials using wheat straw powder as raw material. The wheat straw powder was first hydrolyzed at the absence of a catalyst at 190°C for 1 h, then the hydrolyzate solution was used as carbon source to prepare carbon materials via hydrothermal carbonization at 180°C in the absence of a catalyst for 8 h. The influence of solid-liquid-ratio of wheat straw to water on the morphology of the product was investigated. The samples were examined by a scanning electron microscope and Fourier transform infrared spectroscopy. The results show that the product was carbon microspheres with a large number of O–H, CHO, and other functional groups, and the diameters of carbon microspheres noticeably depended on the solid-liquid ratio. When the solid-liquid ratio was 1 : 60, the diameters of carbon microspheres were in the range of 100 to 300 nm when the solid-liquid ratio was 1 : 40, carbon microspheres with larger and more uniform diameters mostly about 250 nm were obtained, and when the solid-liquid-ratio was 1 : 20, there were more larger carbon microspheres with diameters about 800 nm in the product and the surface of these carbon microspheres is smoother, whereas; the uniformity of the product deteriorates.


2011 ◽  
Vol 236-238 ◽  
pp. 2499-2504 ◽  
Author(s):  
Chu Shu Zhang ◽  
Qing Li Yang ◽  
Ke Jia ◽  
Zhi Qiang Liu ◽  
Li Na Yu ◽  
...  

The cell wall of peanut skin was destroyed by cellulase enzymolysis from peanut skin fermentation, which was beneficial to extract proanthocyanidin. The extraction conditions of proanthocyanidin from fermented peanut skin were studied according to orthogonal experiment based on single factor experiments. And the optimum conditions were obtained as follows: extraction time 40min, extraction temperature 55°C, Concentrations of ethanol 45%, solid-liquid ratio 1:15. The extraction rate was 16.17 %.


2011 ◽  
Vol 295-297 ◽  
pp. 2088-2091
Author(s):  
Wei Kong ◽  
Yong Ling Yu ◽  
Li Hua Lv

Process of the separation of waste polyester-cotton fiber with dilute hydrochloric acid was studied. Acid mass fraction, reaction time, reaction temperature and solid-liquid ratio were studied on the effect of separation with the method of Orthogonal experiment. The results showed that the priority order of the factors was reaction time > acid mass fraction > reaction temperature > solid-liquid ratio. The optimal conditions through serious research on such factors were: acid mass fraction 10%, solid-liquid ratio 4g/100ml, reaction temperature 95°Cand reaction time 90 minutes. Through the microscope, polyester and cotton fibers were separated completely in which polyester into fibrous and cotton fibers were hydrolyzed into tiny powder.


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