Solidification interface transformation and solute redistribution of FeCrAl stainless steel

2017 ◽  
Vol 114 (4) ◽  
pp. 409 ◽  
Author(s):  
Jianhua Liu ◽  
Xiaofeng Su ◽  
Hongbo Liu ◽  
Zhibiao Han ◽  
Yang He ◽  
...  
Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4240
Author(s):  
Gang Lu ◽  
Yisi Chen ◽  
Qingsong Yan ◽  
Pengpeng Huang ◽  
HongXing Zhan ◽  
...  

In this paper, in order to improve the performance of the ZL205A castings, continuous ultrasonic and pulsed ultrasonic treatments were applied to the melted alloy to study the effect of ultrasound propagation distance on microstructure and microhardness. The results indicated that ZL205A grains were significantly refined by ultrasonic vibration, but the refinement effect became weak gradually with the increase of sampling depth. The minimum grain sizes were 103.2 μm and 122.5 μm respectively in continuous and pulsed ultrasonic treatment. Grain boundary segregation also became more serious and coarser with the increase of vertical depth. In addition, microhardness and vertical depth are not positively correlated linearly. As the vertical depth increased, microhardness first decreased and then increased, the maximum hardnesses were 73.9 HV and 72.84 HV, respectively, in the two process modes. According to the experiment results and available studies, the mechanism of ultrasonic treatment maybe that: the cooling rate of solidification interface front increased by cavitation and streaming, thus changing the solute redistribution behavior of the ZL205A melt.


1994 ◽  
Vol 116 (3) ◽  
pp. 742-749 ◽  
Author(s):  
P. J. Prescott ◽  
F. P. Incropera ◽  
D. R. Gaskell

Experiments involving the solidification of a Pb-19 percent Sn alloy in an axisymmetric, annular mold of stainless steel are performed, and results are compared with numerical predictions. Agreement between measured and predicted cooling curves is reasonable, although undercooling and recalescence, which occur in the experiments, are not predicted by the model. Measured temperatures also indicate that dendrite fragments are transported throughout the mold cavity during early stages of solidification, and convection patterns similar to those predicted by numerical simulation can be inferred from the measurements. While there is general agreement between measured and predicted trends for macrosegregation, the numerical simulation, which assumes axial symmetry, cannot predict the inherently three-dimensional nature of solute redistribution. Conclusions drawn from temperature and composition measurements are supported by metallographic examinations of experimental ingot specimens.


1977 ◽  
Vol 63 (3) ◽  
pp. 441-449 ◽  
Author(s):  
Takateru UMEDA ◽  
Syunya MATSUYAMA ◽  
Hirokazu MURAYAMA ◽  
Masataka SUGIYAMA

Author(s):  
L.E. Murr ◽  
J.S. Dunning ◽  
S. Shankar

Aluminum additions to conventional 18Cr-8Ni austenitic stainless steel compositions impart excellent resistance to high sulfur environments. However, problems are typically encountered with aluminum additions above about 1% due to embrittlement caused by aluminum in solid solution and the precipitation of NiAl. Consequently, little use has been made of aluminum alloy additions to stainless steels for use in sulfur or H2S environments in the chemical industry, energy conversion or generation, and mineral processing, for example.A research program at the Albany Research Center has concentrated on the development of a wrought alloy composition with as low a chromium content as possible, with the idea of developing a low-chromium substitute for 310 stainless steel (25Cr-20Ni) which is often used in high-sulfur environments. On the basis of workability and microstructural studies involving optical metallography on 100g button ingots soaked at 700°C and air-cooled, a low-alloy composition Fe-12Cr-5Ni-4Al (in wt %) was selected for scale up and property evaluation.


Author(s):  
J. A. Korbonski ◽  
L. E. Murr

Comparison of recovery rates in materials deformed by a unidimensional and two dimensional strains at strain rates in excess of 104 sec.−1 was performed on AISI 304 Stainless Steel. A number of unidirectionally strained foil samples were deformed by shock waves at graduated pressure levels as described by Murr and Grace. The two dimensionally strained foil samples were obtained from radially expanded cylinders by a constant shock pressure pulse and graduated strain as described by Foitz, et al.


Author(s):  
R. Gonzalez ◽  
L. Bru

The analysis of stacking fault tetrahedra (SFT) in fatigued metals (1,2) is somewhat complicated, due partly to their relatively low density, but principally to the presence of a very high density of dislocations which hides them. In order to overcome this second difficulty, we have used in this work an austenitic stainless steel that deforms in a planar mode and, as expected, examination of the substructure revealed planar arrays of dislocation dipoles rather than the cellular structures which appear both in single and polycrystals of cyclically deformed copper and silver. This more uniform distribution of dislocations allows a better identification of the SFT.The samples were fatigue deformed at the constant total strain amplitude Δε = 0.025 for 5 cycles at three temperatures: 85, 293 and 773 K. One of the samples was tensile strained with a total deformation of 3.5%.


Author(s):  
Y. L. Chen ◽  
J. R. Bradley

Considerable effort has been directed toward an improved understanding of the production of the strong and stiff ∼ 1-20 μm diameter pyrolytic carbon fibers of the type reported by Koyama and, more recently, by Tibbetts. These macroscopic fibers are produced when pyrolytic carbon filaments (∼ 0.1 μm or less in diameter) are thickened by deposition of carbon during thermal decomposition of hydrocarbon gases. Each such precursor filament normally lengthens in association with an attached catalyst particle. The subject of filamentous carbon formation and much of the work on characterization of the catalyst particles have been reviewed thoroughly by Baker and Harris. However, identification of the catalyst particles remains a problem of continuing interest. The purpose of this work was to characterize the microstructure of the pyrolytic carbon filaments and the catalyst particles formed inside stainless steel and plain carbon steel tubes. For the present study, natural gas (∼; 97 % methane) was passed through type 304 stainless steel and SAE 1020 plain carbon steel tubes at 1240°K.


Author(s):  
M. R. Pinnel ◽  
A. Lawley

Numerous phenomenological descriptions of the mechanical behavior of composite materials have been developed. There is now an urgent need to study and interpret deformation behavior, load transfer, and strain distribution, in terms of micromechanisms at the atomic level. One approach is to characterize dislocation substructure resulting from specific test conditions by the various techniques of transmission electron microscopy. The present paper describes a technique for the preparation of electron transparent composites of aluminum-stainless steel, such that examination of the matrix-fiber (wire), or interfacial region is possible. Dislocation substructures are currently under examination following tensile, compressive, and creep loading. The technique complements and extends the one other study in this area by Hancock.The composite examined was hot-pressed (argon atmosphere) 99.99% aluminum reinforced with 15% volume fraction stainless steel wire (0.006″ dia.).Foils were prepared so that the stainless steel wires run longitudinally in the plane of the specimen i.e. the electron beam is perpendicular to the axes of the wires. The initial step involves cutting slices ∼0.040″ in thickness on a diamond slitting wheel.


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