Nonimaging characterization of imperfect single crystals by means of a three‐crystal diffractometer for high energy synchrotron radiation

1993 ◽  
Vol 73 (8) ◽  
pp. 3680-3684 ◽  
Author(s):  
R. Bouchard ◽  
S. Kouptsidis ◽  
H. B. Neumann ◽  
T. Schmidt ◽  
J. R. Schneider
2007 ◽  
Vol 539-543 ◽  
pp. 2353-2358 ◽  
Author(s):  
Ulrich Lienert ◽  
Jonathan Almer ◽  
Bo Jakobsen ◽  
Wolfgang Pantleon ◽  
Henning Friis Poulsen ◽  
...  

The implementation of 3-Dimensional X-Ray Diffraction (3DXRD) Microscopy at the Advanced Photon Source is described. The technique enables the non-destructive structural characterization of polycrystalline bulk materials and is therefore suitable for in situ studies during thermo-mechanical processing. High energy synchrotron radiation and area detectors are employed. First, a forward modeling approach for the reconstruction of grain boundaries from high resolution diffraction images is described. Second, a high resolution reciprocal space mapping technique of individual grains is presented.


2007 ◽  
pp. 2353-2358
Author(s):  
Ulrich Lienert ◽  
Jon Almer ◽  
Bo Jakobsen ◽  
Wolfgang Pantleon ◽  
Henning Friis Poulsen ◽  
...  

2017 ◽  
Vol 373 ◽  
pp. 193-196
Author(s):  
Oksana Melikhova ◽  
Jakub Čížek ◽  
Ivan Procházka ◽  
Petr Hruška ◽  
Wolfgang Anwand ◽  
...  

Positron annihilation spectroscopy (PAS) was employed for characterization of defects in the hydrothermally (HT) grown zinc oxide single crystals irradiated by high energy ions. Defects created in ZnO crystals by 2.5 MeV protons, 7.5 MeV N3+ and 167 MeV Xe26+ ions were compared. The virgin ZnO crystals contain Zn-vacancies associated with hydrogen. Ion implantation introduced additional defects, namely Zn+O di-vacancies in crystals irradiated by protons and small vacancy clusters in samples implanted by N and Xe ions.


1999 ◽  
Vol 38 (S1) ◽  
pp. 616
Author(s):  
Yoshiyuki Tsusaka ◽  
Shingo Takeda ◽  
Kengo Takai ◽  
Kazushi Yokoyama ◽  
Yasushi Kagoshima ◽  
...  

2010 ◽  
Vol 652 ◽  
pp. 185-190
Author(s):  
Abdelilah Benmarouane ◽  
Helene Citterio-Bigot ◽  
Pierre Millet ◽  
Thomas Buslaps ◽  
Alain Lodini

Technology developments of implant composition and manufacture have been used in the medical field. Several different implants have been developed with varying degrees of commercial success. As a long-term establishment is a measure of the therapeutic success, it is necessary to use biocompatible implants in order to have good mechanical and fracture resistance of new bone reconstructed at the interface with the implant. Titanium (Ti-Al-4V) implants coated with hydroxyapatite (HAp), Ca10 (PO4)6 (OH)2 are widely used in orthopedic applications in order to obtain a stable and functional direct connection between the bone and the implant. At the implant-bone interface the new bone reconstituted after implantation must have the same orientation as the natural bone in order to accept the implant. Therefore we studied the texture and the crystallinity of the new bone crystals reconstituted at the interface applying by high-energy synchrotron radiation on beamline ID15 at ESRF in Grenoble, France.


2009 ◽  
Vol 635 ◽  
pp. 195-199 ◽  
Author(s):  
Robert Chulist ◽  
Andrea Böhm ◽  
Thomas Lippmann ◽  
Werner Skrotzki ◽  
Welf Guntram Drossel ◽  
...  

Up to now most of the research on Ni-Mn-Ga alloys was concentrated on single crystals. However, there is a great interest in polycrystals for technical applications. Recently, polycrystalline Ni50Mn29Ga21 rods of 25 mm diameter and 400 mm length were prepared by hot extrusion. The <100> <110> double fibre texture of the extruded rods was measured with high-energy synchrotron radiation. The microstructure after hot extrusion was analyzed with electron backscatter diffraction. Within the recrystallized grains all three martensitic variants have developed during cooling. Variants with twin boundaries preferentially aligned along the extrusion direction predominate.


2015 ◽  
Vol 30 (8) ◽  
pp. 887 ◽  
Author(s):  
HUANG Chang-Bao ◽  
NI You-Bao ◽  
WU Hai-Xin ◽  
WANG Zhen-You ◽  
XIAO Rui-Chun ◽  
...  
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