Characterisation of anode plasma deposited IN718 TBC system after thermal cycle shocking test

2021 ◽  
pp. 1-9
Author(s):  
Priyanka Sharma ◽  
Vijay Kumar Dwivedi ◽  
Dipak Kumar
Keyword(s):  
Thermal Cycle ◽  
Anode Plasma

Correlation between dislocation, grain boundary and interface of duplex SS in stress corrosion cracking(SCC)

1990 ◽  
Vol 48 (4) ◽  
pp. 928-929
Author(s):  
Wang Zheng-fang ◽  
Z.F. Wang
Keyword(s):  
Stainless Steel ◽  
Thermal Cycle ◽  
Secondary Phase ◽  
Corrosion Cracking ◽  
Coarse Grained ◽  
Test Environment ◽  
Fine Grained ◽  
Evaluation Test ◽  
Welding Thermal Cycle ◽  
Micro Analysis

The main purpose of this study highlights on the evaluation of chloride SCC resistance of the material,duplex stainless steel,OOCr18Ni5Mo3Si2 (18-5Mo) and its welded coarse grained zone(CGZ).18-5Mo is a dual phases (A+F) stainless steel with yield strength:512N/mm2 .The proportion of secondary Phase(A phase) accounts for 30-35% of the total with fine grained and homogeneously distributed A and F phases(Fig.1).After being welded by a specific welding thermal cycle to the material,i.e. Tmax=1350°C and t8/5=20s,microstructure may change from fine grained morphology to coarse grained morphology and from homogeneously distributed of A phase to a concentration of A phase(Fig.2).Meanwhile,the proportion of A phase reduced from 35% to 5-10°o.For this reason it is known as welded coarse grained zone(CGZ).In association with difference of microstructure between base metal and welded CGZ,so chloride SCC resistance also differ from each other.Test procedures:Constant load tensile test(CLTT) were performed for recording Esce-t curve by which corrosion cracking growth can be described, tf,fractured time,can also be recorded by the test which is taken as a electrochemical behavior and mechanical property for SCC resistance evaluation. Test environment:143°C boiling 42%MgCl2 solution is used.Besides, micro analysis were conducted with light microscopy(LM),SEM,TEM,and Auger energy spectrum(AES) so as to reveal the correlation between the data generated by the CLTT results and micro analysis.

Counterfeit Parts Recognition and Detection for Failure Analysts

2010 ◽  
Author(s):  
Katherine V. Whittington
Keyword(s):  
Thermal Cycle ◽  
Visual Inspection ◽  
Acoustic Microscopy ◽  
Scanning Acoustic Microscopy ◽  
3D Measurement ◽  
X Ray ◽  
Wide Range ◽  
Electronic Parts ◽  
Testing Awareness

Abstract The electronics supply chain is being increasingly infiltrated by non-authentic, counterfeit electronic parts, whose use poses a great risk to the integrity and quality of critical hardware. There is a wide range of counterfeit parts such as leads and body molds. The failure analyst has many tools that can be used to investigate counterfeit parts. The key is to follow an investigative path that makes sense for each scenario. External visual inspection is called for whenever the source of supply is questionable. Other methods include use of solvents, 3D measurement, X-ray fluorescence, C-mode scanning acoustic microscopy, thermal cycle testing, burn-in technique, and electrical testing. Awareness, vigilance, and effective investigations are the best defense against the threat of counterfeit parts.

scholarly journals Study of the effect of inter-pass temperature on weld overlap start-stop defects and mitigation by application of laser defocusing

2021 ◽  
Vol 114 (1-2) ◽  
pp. 117-130
Author(s):  
Wai Jun Lai ◽  
Supriyo Ganguly ◽  
Wojciech Suder
Keyword(s):  
Thermal Cycle ◽  
Laser Initiation ◽  
Thick Section ◽  
Keyhole Welding ◽  
Run Off ◽  
And Control ◽  
Laser Keyhole Welding

AbstractLaser keyhole initiation and termination-related defects, such as cracking and keyhole cavities due to keyhole collapse, are a well-known issue in laser keyhole welding of thick section steels. In longitudinal welding, run-on and run-off plates are used to avoid this problem. However, such an approach is not applicable in circumferential welding where start/stop defects remain within the workpiece. These issues can hinder industry from applying laser keyhole welding for circumferential welding applications. In this paper, the effect of inter-pass temperature on laser keyhole initiation and termination at the weld overlap start-stop region was investigated. This study has identified that defects occurring within this region were due to laser termination rather than laser initiation because of keyhole instabilities regardless of the thermal cycle. The laser termination defects were mitigated by applying a laser defocusing termination regime to reduce the keyhole depth gradually and control the closure of the keyhole.

scholarly journals Effect of Intermetallic Compound Bridging on the Cracking Resistance of Sn2.3Ag Microbumps with Different UBM Structures under Thermal Cycling

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1065
Author(s):  
Chun-Chieh Mo ◽  
Dinh-Phuc Tran ◽  
Jing-Ye Juang ◽  
Chih Chen
Keyword(s):  
Electron Microscope ◽  
Intermetallic Compound ◽  
Thermal Cycling ◽  
Thermal Cycle ◽  
Crack Formation ◽  
Thermal Cycling Test ◽  
Under Bump Metallization ◽  
Reflow Time ◽  
Cracking Resistance ◽  
Scanning Electron

In this study, the effect of intermetallic compound (IMC) bridging on the cracking resistance of microbumps with two different under bump metallization (UBM) systems, Cu/solder/Cu and Cu/solder/Ni, under a thermal cycling test (TCT) is investigated. The height of the Sn2.3Ag solders was ~10 µm, which resembles that of the most commonly used microbumps. We adjusted the reflow time to control the IMC bridging level. The samples with different bridging levels were tested under a TCT (−55–125 °C). After 1000 and 2000 TCT cycles (30 min/cycle), the samples were then polished and characterized using a scanning electron microscope (SEM). Before IMC bridging, various cracks in both systems were observed at the IMC/solder interfaces after the 1000-cycle tests. The cracks propagated as cyclic shapes from the sides to the center and became more severe as the thermal cycle was increased. With IMC bridging, we could not observe any further failure in all the samples even when the thermal cycle was up to 2000. We discovered that IMC bridging effectively suppressed crack formation in microbumps under TCTs.

scholarly journals Development of laser welding of high strength aluminium alloy 2024-T4 with controlled thermal cycle

2020 ◽  
Vol 326 ◽  
pp. 08005
Author(s):  
Mete Demirorer ◽  
Wojciech Suder ◽  
Supriyo Ganguly ◽  
Simon Hogg ◽  
Hassam Naeem
Keyword(s):  
Laser Beam ◽  
Laser Welding ◽  
Heat Input ◽  
Thermal Cycle ◽  
Laser Beam Welding ◽  
Base Material ◽  
High Strength ◽  
Cooling Rates ◽  
Aa 2024 ◽  
Welding Processes

An innovative process design, to avoid thermal degradation during autogenous fusion welding of high strength AA 2024-T4 alloy, based on laser beam welding, is being developed. A series of instrumented laser welds in 2 mm thick AA 2024-T4 alloys were made with different processing conditions resulting in different thermal profiles and cooling rates. The welds were examined under SEM, TEM and LOM, and subjected to micro-hardness examination. This allowed us to understand the influence of cooling rate, peak temperature, and thermal cycle on the growth of precipitates, and related degradation in the weld and heat affected area, evident as softening. Although laser beam welding allows significant reduction of heat input, and higher cooling rates, as compared to other high heat input welding processes, this was found insufficient to completely supress coarsening of precipitate in HAZ. To understand the required range of thermal cycles, additional dilatometry tests were carried out using the same base material to understand the time-temperature relationship of precipitate formation. The results were used to design a novel laser welding process with enhanced cooling, such as with copper backing bar and cryogenic cooling.

scholarly journals Simulation of the Evolutions in Real Microstructure of Material under Thermal Cycle with High Thermal Gradients

Procedia CIRP ◽  
2020 ◽  
Vol 95 ◽  
pp. 238-243
Author(s):  
T. Bergs ◽  
M. Mohammadnejad ◽  
R. Hess ◽  
L. Heidemanns ◽  
A. Klink
Keyword(s):  
Thermal Cycle ◽  
Thermal Gradients ◽  
Microstructure Of Material

scholarly journals Microstructure and Fracture Toughness of Fe–Nb Dissimilar Welded Joints

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 86
Author(s):  
Qiaoling Chu ◽  
Lin Zhang ◽  
Tuo Xia ◽  
Peng Cheng ◽  
Jianming Zheng ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Weld Metal ◽  
Thermal Cycle ◽  
Peak Load ◽  
Local Phase ◽  
Weld Formation ◽  
Lamellar Structures ◽  
Average Hardness ◽  
Radial Cracks

The relation between the microstructure and mechanical properties of the Fe–Nb dissimilar joint were investigated using nanoindentation. The weld metal consists mainly of Fe2Nb, α-Fe + Fe2Nb, Nb (s,s) and Fe7Nb6 phases. Radial cracks initiate from the corners of the impressions on the Fe2Nb phase (~20.5 GPa) when subjected to a peak load of 300 mN, whereas the fine lamellar structures (α-Fe + Fe2Nb) with an average hardness of 6.5 GPa are free from cracks. The calculated fracture toughness of the Fe2Nb intermetallics is 1.41 ± 0.53 MPam1/2. A simplified scenario of weld formation together with the thermal cycle is proposed to elaborate the way local phase determined the mechanical properties.

Microstructural evolution and mechanical integrity relationship of dissimilar metal welding between 2205 duplex stainless steel and composite bimetallic plates

2021 ◽  
pp. 095440622110036
Author(s):  
Changqing Ye ◽  
Weiguo Zhai ◽  
Guangyao Lu ◽  
Qingsong Liu ◽  
Liang Ni ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Weld Metal ◽  
Duplex Stainless Steel ◽  
Intergranular Corrosion ◽  
Thermal Cycle ◽  
Filler Metal ◽  
2205 Duplex Stainless Steel ◽  
Welding Thermal Cycle ◽  
Intergranular Corrosion Resistance

In this paper, shielded metal arc welding on the dissimilar joint between 2205 duplex stainless steel and composite bimetallic plates (304 L stainless steel/10CrNi3MoV steel) with a filler metal E2209 was performed. Furthermore, the microstructure, phase, mechanical properties and intergranular corrosion resistance of the joints were investigated and element distributions of the interfaces were characterized. The results show that austenite transformed to ferrite under the influence of welding thermal cycle, and then a large amount of ferrite appeared in heat affected zone (HAZ) of 2205 duplex stainless steel. Coarse bainite grains were formed in HAZ of the 10CrNi3MoV steel near the fusion line with high temperature welding thermal cycle. Fine granular bainite was also generated in HAZ of 10CrNi3MoV steel due to the relatively short exposure time to the active temperature of grain growth. Local peak temperature near the base 10CrNi3MoV steel was still high enough to recrystallize the 10CrNi3MoV steel to form partial-recrystallization HAZ due to phase change. The filler metal was compatible with the three kinds of base materials. The thickness of the elemental diffusion interfaces layers was about 100 µm. The maximum microhardness value was obtained in the HAZ of 2205 duplex stainless steel (287 ± 14 HV), and the minimum one appeared in HAZ of SS304L (213 ± 5 HV). The maximum tensile strength of the welded joint was about 670 ± 6 MPa, and the tensile specimens fractured in ductile at matrix of the composite bimetallic plates. The impact energy of the weld metal and HAZ of the 10CrNi3MoV steel tested at –20 °C were 274 ± 6 J and 308 ± 5 J, respectively. Moreover, the intergranular corrosion resistance of the weldment including 304 L stainless steel, weld metal, HAZs and 2205 duplex stainless steel was in good agreement with the functional design requirements of materials corrosion resistance.

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