A new low temperature diffusion bonding technology between large-area, high-power devices and internal Mo electrodes using Au-Al films

Author(s):  
J. Onuki ◽  
M. Satou ◽  
S. Murakami ◽  
T. Morita ◽  
T. Yatsuo
Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1223
Author(s):  
Guoqian Mu ◽  
Wenqing Qu ◽  
Haiyun Zhu ◽  
Hongshou Zhuang ◽  
Yanhua Zhang

Interfacial heat transfer is essential for the development of high-power devices with high heat flux. The metallurgical bonding of Cu substrates is successfully realized by using a self-made interlayer at 10 °C, without any flux, by Cu/Ga solid-liquid inter-diffusion bonding (SLID), which can be used for the joining of heat sinks and power devices. The microstructure and properties of the joints were investigated, and the mechanism of Cu/Ga SLID bonding was discussed. The results show that the average shear strength of the joints is 7.9 MPa, the heat-resistant temperature is 200 °C, and the thermal contact conductance is 83,541 W/(m2·K) with a holding time of 30 h at the bonding temperature of 100 °C. The fracture occurs on one side of the copper wire mesh which is caused by the residual gallium. The microstructure is mainly composed of uniform θ-CuGa2 phase, in addition to a small amount of residual copper, residual gallium and γ3-Cu9Ga4 phase. The interaction product of Cu and Ga is mainly θ-CuGa2 phase, with only a small amount of γ3-Cu9Ga4 phase occurring at the temperature of 100 °C for 20 h. The process of Cu/Ga SLID bonding can be divided into three stages as follows: the pressurization stage, the reaction diffusion stage and the isothermal solidification stage. This technology can meet our requirements of low temperature bonding, high reliability service and interfacial heat transfer enhancement.


Membranes ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 338
Author(s):  
Duck-Kyu Oh ◽  
Kwan-Young Lee ◽  
Jong-Soo Park

This study investigates a compact palladium membrane module (CPMM) for hydrogen purification, assembled by diffusion bonding at a low-temperature (450 °C). This CPMM resulted in hydrogen (H2) flux of 18.3 mL cm−2 min−1 with H2/N2 selectivity of over 1100. The H2 purification test using a 60% H2/40% CO2 mixed gas confirmed that the CPMM can separate H2 with a concentration of more than 99%, with a pressure difference of 5 bar. Moreover, the volume of the diffusion bonded membrane module is decreased by 81.4% than the flame-type membrane module pre-studied in our laboratory.


Author(s):  
Kenneth K. Chu ◽  
Pane C. Chao ◽  
Jose A. Diaz ◽  
Thomas Yurovchak ◽  
Carlton T. Creamer ◽  
...  

Coatings ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 401 ◽  
Author(s):  
Cherng-Yuh Su ◽  
Jia-Liang Huang ◽  
Po-Chun Chen ◽  
Hsin-Jung Yu ◽  
Dai-Liang Ma ◽  
...  

Ceramic-to-metal heterojunctions have been established to improve high-temperature stability for applications in aerospace and harsh environments. In this work, we employed low-temperature diffusion bonding to realize an alumina/Cu heterogeneous joint. Using a thin layer of lanthanum-doped titanium (La-doped Ti) to metallize the alumina surface, we achieved the bonding at a temperature range of 250–350 °C. We produced a uniform, thermally stable, and high-strength alumina/Cu joint after a hot-press process in vacuum. Signals from X-ray diffraction (XRD) suggested the successful diffusion of Ti and La into the alumina substrate, as Ti can easily substitute Al in alumina, and La has a better oxygen affinity than that of Al. The transmission electron microscopy and XRD results also showed the existence of CuxTiyO phases without CuxTiy or LaOx. In addition, the bonding strength of alumina/copper hot-pressed at 250, 300, and 350 °C were 7.5, 9.8 and 15.0 MPa, respectively. The process developed in this study successfully lowered the bonding temperature for the alumina/copper joint.


2000 ◽  
Vol 28 (2) ◽  
pp. 88 ◽  
Author(s):  
DR Petersen ◽  
RE Link ◽  
Y Greenberg ◽  
D Itzhak ◽  
G Kohn

2010 ◽  
Vol 63 (6) ◽  
pp. 853-857 ◽  
Author(s):  
P. S. Gawde ◽  
R. Kishore ◽  
A. L. Pappachan ◽  
G. B. Kale ◽  
G. K. Dey

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