Stereo representation of atomic force micrographs: Optimizing the view

1995 ◽  
Vol 180 (2) ◽  
pp. 186-188 ◽  
Author(s):  
Z. SHAO ◽  
A. P. SOMLYO
Keyword(s):  
Atomic Force ◽  
Atomic Force Micrographs

Optical Properties of Sputtered Silver Granular Films

2005 ◽  
Vol 480-481 ◽  
pp. 287-292 ◽  
Author(s):  
S.E. Paje ◽  
F. Teran ◽  
J.M. Riveiro ◽  
J. Llopis ◽  
M.A. García ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Optical Properties ◽  
Optical Absorption ◽  
Surface Morphology ◽  
Silver Clusters ◽  
Plasmon Excitation ◽  
Granular Films ◽  
Silver Films ◽  
Atomic Force ◽  
Atomic Force Micrographs

In this research we study optical absorption and morphology of silver films prepared with a sputtering method. Silver granular films are obtained on a glass substrate for films with thickness smaller than about 60 Å. Superficial silver clusters of around 100 nm in diameter are clearly seen in the atomic force micrographs. The absorption of these samples are characterized by plasmon excitation in the 450-650 nm spectral range, which differs from the known excitation of silver nanoparticles fabricated by different techniques. The optical absorption of silver granular films depend on sputtering conditions like substrate temperature or deposition rate and correlates with the surface morphology.

Experimental Investigations on Magnetic Field Assisted Abrasive Micro Finishing of Austenitic Stainless Steel 304L

2012 ◽  
Vol 584 ◽  
pp. 192-196
Author(s):  
T.C. Kanish ◽  
P. Kuppan ◽  
S. Narayanan
Keyword(s):  
Magnetic Field ◽  
Surface Roughness ◽  
Stainless Steel ◽  
Experimental Investigations ◽  
Optimum Conditions ◽  
Taguchi Design Of Experiments ◽  
Atomic Force ◽  
Work Material ◽  
Abrasive Finishing ◽  
Atomic Force Micrographs

This paper presents the experimental investigations on magnetic field assisted abrasive finishing of SS304L flat work material. The experiments are designed using Taguchi design of experiments method. The results indicate that process parameters such as voltage and machining gap are significant on improvement of surface finish (∆Ra). The surface roughness value as low as 0.09 µm is achieved at optimum conditions. The surface topography of the work material is analyzed by means of the surface roughness profile, optical and atomic force micrographs.

Influence of oxidized starch on physicomechanical, thermal properties, and atomic force micrographs of cassava starch bioplastic film

2019 ◽  
Vol 135 ◽  
pp. 282-293 ◽  
Author(s):  
Olugbenga O. Oluwasina ◽  
Feranmi K. Olaleye ◽  
Sunday J. Olusegun ◽  
Olayinka O. Oluwasina ◽  
Nelcy D.S. Mohallem
Keyword(s):  
Thermal Properties ◽  
Cassava Starch ◽  
Oxidized Starch ◽  
Atomic Force ◽  
Bioplastic Film ◽  
Atomic Force Micrographs

Analyzing Atomic Force Micrographs Using Spectral Methods

1995 ◽  
Vol 386 ◽  
Author(s):  
Sameer D. Halepete ◽  
H. C. Lin ◽  
Simon J. Fang ◽  
C. R. Helms
Keyword(s):  
Silicon Surface ◽  
Critical Parameter ◽  
Spectral Information ◽  
Root Mean Square Roughness ◽  
Atomic Force ◽  
Frequency Components ◽  
Height Data ◽  
Insight Into ◽  
Atomic Force Micrographs ◽  
Analyze Data

ABSTRACTMicroroughness is a critical parameter in ULSI device interface reliability and has been shown to effect several critical MOS electrical properties. The atomic force microscope (AFM) has become the instrument of choice for silicon surface microroughness analysis. The parameters usually specified to characterize roughness are average and root mean square roughness. However, these parameters are spatial averages and can have the same value for two significantly different surfaces. Spectral analysis using the Fast Fourier Transform (FFT) has been applied as a powerful tool to analyze AFM data by looking at roughness as a function of spatial wavelength. The Fast Hartley Transform, being a real transform, is faster than the FFT and is better suited for this analysis. It has been used here to derive spectral information from the AFM height data. Before evaluating the transform, cancellation of any tilt or warp in the AFM data is done to remove frequency components which interfere with other spectral information. A PC-based computer program to determine the transform and its magnitude will be described. The application of this method to analyze data from Si and SiO2 surfaces as a function of pre-oxidation cleaning chemistry will be presented. Significantly better insight into the spatial distribution of roughness is obtained, when compared to previous implementations.

Cryogenic atomic force microscopy

1991 ◽  
Vol 49 ◽  
pp. 54-55
Author(s):  
K. A. Fisher ◽  
M. G. L. Gustafsson ◽  
M. B. Shattuck ◽  
J. Clarke
Keyword(s):  
Room Temperature ◽  
Rapid Freezing ◽  
Cryogenic Temperatures ◽  
Soft Or ◽  
Electrically Conductive ◽  
Force Microscopy ◽  
Flexible Molecules ◽  
Advantages And Disadvantages ◽  
Atomic Force ◽  
Chemical Perturbation

The atomic force microscope (AFM) is capable of imaging electrically conductive and non-conductive surfaces at atomic resolution. When used to image biological samples, however, lateral resolution is often limited to nanometer levels, due primarily to AFM tip/sample interactions. Several approaches to immobilize and stabilize soft or flexible molecules for AFM have been examined, notably, tethering coating, and freezing. Although each approach has its advantages and disadvantages, rapid freezing techniques have the special advantage of avoiding chemical perturbation, and minimizing physical disruption of the sample. Scanning with an AFM at cryogenic temperatures has the potential to image frozen biomolecules at high resolution. We have constructed a force microscope capable of operating immersed in liquid n-pentane and have tested its performance at room temperature with carbon and metal-coated samples, and at 143° K with uncoated ferritin and purple membrane (PM).

AFM study of the dynamics of α-alumina surface faceting during high-temperature processing

1995 ◽  
Vol 53 ◽  
pp. 334-335 ◽  
Author(s):  
Michael W. Bench ◽  
Jason R. Heffelfinger ◽  
C. Barry Carter
Keyword(s):  
High Temperature ◽  
Thin Foil ◽  
Sem Analysis ◽  
Conductive Coatings ◽  
Force Microscopy ◽  
Minimal Sample ◽  
Atomic Force ◽  
Formation And Evolution ◽  
High Temperature Processing ◽  
Nominal Surface

To gain a better understanding of the surface faceting that occurs in α-alumina during high temperature processing, atomic force microscopy (AFM) studies have been performed to follow the formation and evolution of the facets. AFM was chosen because it allows for analysis of topographical details down to the atomic level with minimal sample preparation. This is in contrast to SEM analysis, which typically requires the application of conductive coatings that can alter the surface between subsequent heat treatments. Similar experiments have been performed in the TEM; however, due to thin foil and hole edge effects the results may not be representative of the behavior of bulk surfaces.The AFM studies were performed on a Digital Instruments Nanoscope III using microfabricated Si3N4 cantilevers. All images were recorded in air with a nominal applied force of 10-15 nN. The alumina samples were prepared from pre-polished single crystals with (0001), , and nominal surface orientations.

Characterization of photosystem II with the atomic-force microscope

1992 ◽  
Vol 50 (2) ◽  
pp. 1146-1147
Author(s):  
Kathleen M. Marr ◽  
Mary K. Lyon
Keyword(s):  
Photosystem Ii ◽  
Atomic Force Microscope ◽  
Three Dimensional ◽  
Biologically Active ◽  
Atomic Force ◽  
Freeze Etching ◽  
Image Averaging ◽  
Oxygen Evolving ◽  
Averaging Techniques

Photosystem II (PSII) is different from all other reaction centers in that it splits water to evolve oxygen and hydrogen ions. This unique ability to evolve oxygen is partly due to three oxygen evolving polypeptides (OEPs) associated with the PSII complex. Freeze etching on grana derived insideout membranes revealed that the OEPs contribute to the observed tetrameric nature of the PSIl particle; when the OEPs are removed, a distinct dimer emerges. Thus, the surface of the PSII complex changes dramatically upon removal of these polypeptides. The atomic force microscope (AFM) is ideal for examining surface topography. The instrument provides a topographical view of individual PSII complexes, giving relatively high resolution three-dimensional information without image averaging techniques. In addition, the use of a fluid cell allows a biologically active sample to be maintained under fully hydrated and physiologically buffered conditions. The OEPs associated with PSII may be sequentially removed, thereby changing the surface of the complex by one polypeptide at a time.

X-ray Gabor holography

1995 ◽  
Vol 53 ◽  
pp. 612-613
Author(s):  
Steve Lindaas ◽  
Chris Jacobsen ◽  
Alex Kalinovsky ◽  
Malcolm Howells
Keyword(s):  
Surface Relief ◽  
Biological Imaging ◽  
Specimen Preparation ◽  
X Rays ◽  
X Ray ◽  
Water Window ◽  
Biological Objects ◽  
Transmission Imaging ◽  
Atomic Force ◽  
Electron Microscopes

Soft x-ray microscopy offers an approach to transmission imaging of wet, micron-thick biological objects at a resolution superior to that of optical microscopes and with less specimen preparation/manipulation than electron microscopes. Gabor holography has unique characteristics which make it particularly well suited for certain investigations: it requires no prefocussing, it is compatible with flash x-ray sources, and it is able to use the whole footprint of multimode sources. Our method serves to refine this technique in anticipation of the development of suitable flash sources (such as x-ray lasers) and to develop cryo capabilities with which to reduce specimen damage. Our primary emphasis has been on biological imaging so we use x-rays in the water window (between the Oxygen-K and Carbon-K absorption edges) with which we record holograms in vacuum or in air.The hologram is recorded on a high resolution recording medium; our work employs the photoresist poly(methylmethacrylate) (PMMA). Following resist “development” (solvent etching), a surface relief pattern is produced which an atomic force microscope is aptly suited to image.

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