Numerical Studies on Channel Formation and Growth During Solidification: Effect of Process Parameters

2006 ◽  
Vol 129 (4) ◽  
pp. 548-558 ◽  
Author(s):  
Jayesh Jain ◽  
Arvind Kumar ◽  
Pradip Dutta

In the present work, solidification of a hyper-eutectic ammonium chloride solution in a bottom-cooled cavity (i.e. with stable thermal gradient) is numerically studied. A Rayleigh number based criterion is developed, which determines the conditions favorable for freckles formation. This criterion, when expressed in terms of physical properties and process parameters, yields the condition for plume formation as a function of concentration, liquid fraction, permeability, growth rate of a mushy layer, and thermophysical properties. Subsequently, numerical simulations are performed for cases with initial and boundary conditions favoring freckle formation. The effects of parameters, such as cooling rate and initial concentration, on the formation and growth of freckles are investigated. It was found that a high cooling rate produced larger and more defined channels which are retained for a longer durations. Similarly, a lower initial concentration of solute resulted in fewer but more pronounced channels. The number and size of channels are also found to be related to the mushy zone thickness. The trends predicted with regard to the variation of number of channels with time under different process conditions are in accordance with the experimental observations reported in the literature.

2019 ◽  
Vol 3 (2) ◽  
pp. 1
Author(s):  
Susila Candra ◽  
Witantyo Witantyo ◽  
Aldo Rendra Djoenaedy

Heating temperature (Quenching temperature), holding time and cooling rate (cooling rate) is an important process parameter in the hardening processes, to obtain maximum hardness number of materials. To determine the optimum parameters influenced by the type of material, process conditions and quenching media. Different process conditions, then the process parameters should also be defined with different process parameters. Thus experiments on the process of hardening steel materials Mod SK3 is done to get the setting parameters of the optimum quenching temperature and holding time. Optimization of process parameters using Response Surface methode. The experimental results: if the cooling media (cooling fluid) used  "engine oil ", the optimal parameter is "quencing temperature" = 828.9 oC, holding time = 40.12198 minutes (40 minutes 8 seconds). If the cooling media used Issodur 220, the optimal process parameters are "quencing temperature" = 832.88 oC, holding time = 39 818 minutes (39 minutes 50 seconds). Kekersaan maximum material that can be achieved is 59.7 HRC (quenching media: "engine oil") and 62.2 HRC (quenching media: "Ussodur 220").


Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 796
Author(s):  
Aya Takase ◽  
Takuya Ishimoto ◽  
Naotaka Morita ◽  
Naoko Ikeo ◽  
Takayoshi Nakano

Ti-6Al-4V alloy fabricated by laser powder bed fusion (L-PBF) and electron beam powder bed fusion (EB-PBF) techniques have been studied for applications ranging from medicine to aviation. The fabrication technique is often selected based on the part size and fabrication speed, while less attention is paid to the differences in the physicochemical properties. Especially, the relationship between the evolution of α, α’, and β phases in as-grown parts and the fabrication techniques is unclear. This work systematically and quantitatively investigates how L-PBF and EB-PBF and their process parameters affect the phase evolution of Ti-6Al-4V and residual stresses in the final parts. This is the first report demonstrating the correlations among measured parameters, indicating the lattice strain reduces, and c/a increases, shifting from an α’ to α+β or α structure as the crystallite size of the α or α’ phase increases. The experimental results combined with heat-transfer simulation indicate the cooling rate near the β transus temperature dictates the resulting phase characteristics, whereas the residual stress depends on the cooling rate immediately below the solidification temperature. This study provides new insights into the previously unknown differences in the α, α’, and β phase evolution between L-PBF and EB-PBF and their process parameters.


BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 4947-4962
Author(s):  
Jin Yan ◽  
Jianan Liu ◽  
Liqiang Zhang ◽  
Zhili Tan ◽  
Haoran Zhang ◽  
...  

The influence of the process parameters on the mechanical properties of compact wood powder generated via hot-pressing was analyzed through a single-factor experiment. The mechanical properties exhibited a nonlinear trend relative to the process conditions of hot-pressed compact wood powder. The relationship models between the process parameters and the mechanical properties for the compact wood powder were established by applying a multiple regression analysis and neural network methods combined with data from an orthogonal array design. A comparison between experimental and predicted results was made to investigate the accuracy of the established models by applying several data groups among the single-factor experiments. The results showed that the accuracy of the neural network model in terms of predicting the mechanical properties was greater compared with the multiple regression model. This demonstrates that the established neural network model had a better prediction performance, and it can accurately map the relationship between the process conditions and the mechanical properties of the compact wood powder.


2021 ◽  
Author(s):  
Anand Mohan ◽  
Dariusz Ceglarek ◽  
Michael Auinger

Abstract This research aims at understanding the impact of welding process parameters and beam oscillation on the weld thermal cycle during laser welding. A three-dimensional heat transfer model is developed to simulate the welding process, based on the finite element (FE) method. The calculated thermal cycle and weld morphology are in good agreement with experimental results from literature. By utilizing the developed heat transfer model, the effect of welding process parameters such as heat source power, welding speed, radius of oscillation, and frequency of oscillation on the intermediate performance indicators (IPIs) such as peak temperature, heat-affected zone volume (HAZ), and cooling rate is quantified. Parametric contour maps for peak temperature, HAZ volume, and cooling rate are developed for the estimation of the process capability space. An integrated approach for rapid process assessment, process capability space refinement, based on IPIs is proposed. The process capability space will guide the identification of the initial welding process parameters window and help in reducing the number of experiments required by refining the feasible region of process parameters based on the interactions with the IPIs. Here, the peak temperature indicates the mode of welding performed while the HAZ volume and cooling rate are weld quality indicators. The regression relationship between the welding process parameters and the IPIs is established for quick estimation of IPIs to replace time-consuming numerical simulations. The proposed approach provides a unique ability to simulate the laser welding process and provides a robust range of process parameters.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Rafael Kakitani ◽  
Cassio Augusto Pinto da Silva ◽  
Bismarck Silva ◽  
Amauri Garcia ◽  
Noé Cheung ◽  
...  

Purpose Overall, selection maps about the extent of the eutectic growth projects the solidification velocities leading to given microstructures. This is because of limitations of most of the set of results when obtained for single thermal gradients within the experimental spectrum. In these cases, associations only with the solidification velocity could give the false impression that reaching a given velocity would be enough to reproduce a result. However, that velocity must necessarily be accompanied by a specific thermal gradient during transient solidification. Therefore, the purpose of this paper is to not only project velocity but also include the gradients acting for each velocity. Design/methodology/approach Compilation of solidification velocity, v, thermal gradient, G, and cooling rate, Ṫ, data for Sn-Cu and Sn-Bi solder alloys of interest is presented. These data are placed in the form of coupled growth zones according to the correlated microstructures in the literature. In addition, results generated in this work for Sn-(0.5, 0.7, 2.0, 2.8)% Cu and Sn-(34, 52, 58)% Bi alloys solidified under non-stationary conditions are added. Findings When analyzing the cooling rate (Ṫ = G.v) and velocity separately, in or around the eutectic composition, a consensus cannot be reached on the resulting microstructure. The (v vs. G) + cooling rate diagrams allow comprehensive analyzes of the combined v and G effects on the subsequent microstructure of the Sn-Cu and Sn-Bi alloys. Originality/value The present paper is devoted to the establishment of (v vs. G) + cooling rate diagrams. These plots may allow comprehensive analyses of the combined v and G effects on the subsequent microstructure of the Sn-Cu and Sn-Bi alloys. This microstructure-processing mapping approach is promising to predict phase competition and resulting microstructures in soldering of Sn-Cu and Sn-Bi alloys. These two classes of alloys are of interest to the soldering industry, whereas manipulation of their microstructures is considered of utmost importance for the metallurgical quality of the product.


2021 ◽  
Vol 36 (4) ◽  
pp. 423-434
Author(s):  
F. Schulte-Hubbert ◽  
D. Drummer ◽  
L. Hoffmann

Abstract The underlying process for the production of textile reinforced thermoplastics is the impregnation of dry textile reinforcements with a thermoplastic matrix. The process parameters such as temperature, time and pressure of the impregnation are mainly determined by the permeability of the reinforcement. This results from a complex interaction of hydrodynamic compaction and relaxation behavior caused by textile and process parameters. The foundation for the description and optimization of impregnation progresses is therefore the determination of the pressure-dependent permeability of fibre textiles. Previous experimental investigations have shown that the dynamic compaction behavior during the impregnation of fibre reinforcements with thermoplastics or thermosets can be successfully characterized. However, for most cases, an analytical representation has not been possible due to the complexity of the process. Although it may be possible to reproduce this behavior by numerical calculations, the results need to be confirmed by experiments. This paper lays the analytical foundation for building a scaled model system, based on the theory of similarity, to observe, measure, and evaluate the dynamic compaction behavior of textile reinforcements under controlled process conditions.


2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Dietmar Drummer ◽  
Steve Meister

In micro- and thin-wall injection moulding the process conditions affect the developed internal structures and thus the resulting part properties. This paper investigates exemplarily on polyamide 66 the interactions of different cooling conditions on the morphological and crystalline structures. The investigations reveal that a slow cooling rate of the melt results in a homogeneous morphology and a higher degree of crystallinity and also a favoured crystalline structure. Consequently, the dielectric behaviour and light transmitting part properties are affected.


Author(s):  
R Sarrafi ◽  
D Lin ◽  
R Kovacevic

Online observation is expected to provide a better understanding of the cathodic cleaning of oxides from the molten pool during variable-polarity gas tungsten arc welding (VP GTAW) of aluminium alloys. In this paper, a machine-vision system with appropriate illumination and filtering is used to monitor in real time the effect of different process parameters on the cleaning of oxides from the molten pool during VP GTAW of Al 6061. Based on the observations, the process conditions under which a clean molten pool can be achieved are determined. In addition, the control of the welding process to maintain the consistency of cathodic cleaning is discussed. The results showed that in order to have an oxide-free molten pool, the solid surface in front of the molten pool should be cleaned from oxides by the electric arc. The choice of process parameters to satisfy this condition has been discussed. It was found that the percentage of direct current electrode positive (DCEP) polarity in the cycle of current has the highest impact on the cathodic cleaning, with the arc current having less influence, and the welding speed showing the least effect. Furthermore, in order to keep the consistency of oxide cleaning, process parameters should be set or controlled to maintain the cleaned zone larger than the molten pool.


2021 ◽  
Vol 9 ◽  
Author(s):  
Malte Jörn Krafft ◽  
Jens Berger ◽  
Bodo Saake

The utilization of agricultural products and residues for the production of value-added and biobased products is a highly relevant topic in present research. Due to the natural recalcitrance of lignocellulosic biomass against enzymatic degradation, pretreatments are important requirement for further processes. For the raw material in this study, corn stover (CS) as highly available agricultural residue and maize silage (MS) as model substrate for an ensiled agricultural product were pretreated by steam refining. However, after processing a liquid fraction and fibers are present. Subsequent to steaming the fiber fraction is well characterized. Nonetheless, in depth characterizations of the filtrates are also important for their subsequent utilization. Decreasing molar masses from 7,900 g/mol to 1,100 g/mol for CS filtrates and 100.000–12.900 g/mol for MS filtrates were determined with increasing severity. Due to their proven inhibitory effect on microorganisms weak acids, furans and phenolic compounds within the liquid phased were analyzed. Especially formic acid increases with increasing severity from 0.27 to 1.20% based on raw material for CS and from 0.07 to 0.23% based on raw material for MS. Further GC/MS measurements indicate, that up to 8.25% (CS filtrate) and 5.23% (MS filtrates) of the total peak area is related to inhibitory phenols. Considering the data, detoxification strategies are of non-negligible importance for filtrates after steam refining and should be considered for further research and process or parameter optimizations. An alternative may be the application of milder process conditions in order to prevent the formation of inhibitory degradation products or the dilution of the gained filtrates.


2012 ◽  
Vol 134 (3) ◽  
Author(s):  
K. Suresh Kumar Reddy ◽  
Pravin Kannan ◽  
Ahmed Al Shoaibi ◽  
C. Srinivasakannan

The present work is an attempt to compile and analyze the most recent literature pertaining to thermal pyrolysis of plastic waste using fluidized bed reactors. The review is short owing to the small number of work reported in the open literature in particular to the fluidized beds. Although works on pyrolysis are reported in fixed beds, autoclaves, and fluidized beds, vast majority of them address to the utilization of fluidized bed due to their advantages and large scale adaptability. The pyrolysis temperature and the residence time are reported to have major influence on the product distribution, with the increase in pyrolysis temperature favoring gas production, with significant reduction in the wax and oil. The pyrolysis gas generally contains H2, CO, CO2, CH4, C2H4, C2H6 while liquid product comprises benzene, toluene, xylene, styrene, light oil, heavy oil, and gasoline with the variations depending on process conditions. The effects of other process parameters, namely fuel feed rate, fuel composition, and fluidizing medium have been reviewed and presented.


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