Nanoindentation Testing of SAC305 Solder Joints Subjected to Thermal Cycling Loading

Author(s):  
Abdullah Fahim ◽  
S. M. Kamrul Hasan ◽  
Jeffrey C. Suhling ◽  
Pradeep Lall

Abstract Solder joints in electronic packages are frequently exposed to thermal cycling environment. Such exposures can occur in real life application as well as in accelerated thermal cycling tests used for the fatigue behavior characterization. Because of temperature variations and CTE mismatches of the assembly materials, cyclic temperature leads to damage accumulation and material property evolution in the solder joints. This eventually results in crack initiation, and subsequent crack growth and failure. In this study, the nanoindentation technique was used to understand the evolution of mechanical properties (modulus, hardness and creep behavior) of SAC305 BGA solder joints and Cu pad subjected to thermal cycling loading for various durations. In addition, microstructural changes in those joints that occur during thermal cycling were observed using both SEM and optical microscopy. BGA solder joint strip specimens were first prepared by cross sectioning BGA assemblies followed by surface polishing to facilitate SEM imaging and nanoindentation testing. The strip specimens were chosen to contain several single grain solder joints. This enabled large regions of solder material with equivalent mechanical behavior, which could then be indented several times after various durations of cycling. After preparation, the solder joint strip samples were thermally cycled from T = −40 to 125 °C in an environmental chamber. At various points in the cycling (e.g. after 0, 50, 100, and 250 cycles), the package was taken out from the chamber, and nanoindentation was performed on each single grain joint and joint Cu pads to obtain the modulus, hardness, and creep behavior at 25 °C. This allowed the evolution of the mechanical properties with the duration of thermal cycling to be determined. Moreover, microstructural changes were also observed after various durations of cycling using optical microscopy. From the nanoindentation test results, it was found that the modulus and hardness of the SAC305 solder joints dropped significantly with thermal cycling. However, the Cu pad did not show any change in the mechanical behavior during cycling. Moreover, the nanoindentation creep test results showed significant increases in the creep deformation for solder joints whereas Cu pad did now show any significant changes in creep behavior when both of them were subjected to thermal cycling up to 250 cycles.


Author(s):  
Abdullah Fahim ◽  
Kamrul Hasan ◽  
Jeffrey C. Suhling ◽  
Pradeep Lall

Abstract Electronic packages are frequently exposed to a thermal cycling environment in real life applications. Particularly, the plastic ball grid array (PBGA) is one of the most widely used electronic package, and consists of various component materials, e.g. solder joint, silicon die, die attachment adhesive, mold compound, solder mask, etc. All of these materials play a significant role on the reliability of the overall package. Failure under creep deformation is one of the significant failure mode for electronic packages. Hence, it is important to study their creep behavior and evolution under the thermal cycling environment. These changes must be evaluated in order to understand and predict their failure behavior due to creep damage in operation. In our previous study, evolution of mechanical properties of SAC305 solder joints in a PBGA package up to 250 thermal cycles was evaluated using the nanoindentation technique. In this work, nanoindentation technique was utilized to understand the evolution of creep behavior of the SAC305 solder joint, die attachment adhesive, silicon die, and solder mask material for various durations of thermal cycling. Test specimens were first prepared by cross sectioning a PBGA package to reveal the different materials, followed by surface polishing to facilitate SEM imaging and nanoindentation testing. After preparation, the package samples were thermally cycled from T = −40 to 125 °C in an environmental chamber. At various points in the cycling (e.g. after 0, 50, 100, 250 and 500 cycles), the package was taken out from the chamber, and nanoindentation was performed on above mentioned materials to obtain creep behavior at room temperature (25 °C). From the nanoindentation test data, it was found that creep deformation of SAC305 increased upto 500 cycles. Die attachment and solder mask materials showed initial decrease in creep deformation up to 250 cycles and then increased value at 500 cycles. As expected, the silicon die material does not show any significant change in creep deformation behavior upto 500 cycles.



Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 733
Author(s):  
Lu Liu ◽  
Songbai Xue ◽  
Ruiyang Ni ◽  
Peng Zhang ◽  
Jie Wu

In this study, a Sn–Bi composite solder paste with thermosetting epoxy (TSEP Sn–Bi) was prepared by mixing Sn–Bi solder powder, flux, and epoxy system. The melting characteristics of the Sn–Bi solder alloy and the curing reaction of the epoxy system were measured by differential scanning calorimeter (DSC). A reflow profile was optimized based on the Sn–Bi reflow profile, and the Organic Solderability Preservative (OSP) Cu pad mounted 0603 chip resistor was chosen to reflow soldering and to prepare samples of the corresponding joint. The high temperature and humidity reliability of the solder joints at 85 °C/85% RH (Relative Humidity) for 1000 h and the thermal cycle reliability of the solder joints from −40 °C to 125 °C for 1000 cycles were investigated. Compared to the Sn–Bi solder joint, the TSEP Sn–Bi solder joints had increased reliability. The microstructure observation shows that the epoxy resin curing process did not affect the transformation of the microstructure. The shear force of the TSEP Sn–Bi solder joints after 1000 cycles of thermal cycling test was 1.23–1.35 times higher than the Sn–Bi solder joint and after 1000 h of temperature and humidity tests was 1.14–1.27 times higher than the Sn–Bi solder joint. The fracture analysis indicated that the cured cover layer could still have a mechanical reinforcement to the TSEP Sn–Bi solder joints after these reliability tests.



2020 ◽  
Author(s):  
Hui YANG ◽  
Jihui Wu

Abstract The simulation of nano-silver solder joints in flip-chips is performed by the finite element software ANSYS, and the stress-strain distribution results of the solder joints are displayed. In this simulation, the solder joints use Anand viscoplastic constitutive model, which can reasonably simulate the stress and strain of solder joints under thermal cycling load. At the same time this model has been embedded in ANSYS software, so it is more convenient to use. The final simulation results show that the areas where the maximum stresses and strains occur at the solder joints are mostly distributed in the contact areas between the solder joints and the copper pillars and at the solder joints. During the entire thermal cycling load process, the area where the maximum change in stress and strain occurs is always at the solder joint, and when the temperature changes, the temperature at the solder joint changes significantly. Based on comprehensive analysis, the relevant empirical correction calculation equation is used to calculate and predict the thermal fatigue life of nano-silver solder joints. The analysis results provide a reference for the application of nano-silver solder in the electronic packaging industry.



2021 ◽  
Vol 18 (3) ◽  
pp. 137-144
Author(s):  
Dania Bani Hani ◽  
Raed Al Athamneh ◽  
Mohammed Aljarrah ◽  
Sa’d Hamasha

Abstract SAC-based alloys are one of the most common solder materials that are utilized to provide mechanical support and electrical connection between electronic components and the printed circuit board. Enhancing the mechanical properties of solder joints can improve the life of the components. One of the mechanical properties that define the solder joint structure integrity is the shear strength. The main objective of this study is to assess the shear strength behavior of SAC305 solder joints under different aging conditions. Instron 5948 Micromechanical Tester with a customized fixture is used to perform accelerated shear tests on individual solder joints. The shear strength of SAC305 solder joints with organic solderability preservative (OSP) surface finish is investigated at constant strain rate under different aging times (2, 10, 100, and 1,000 h) and different aging temperatures (50, 100, and 150°C). The nonaged solder joints are examined as well for comparison purposes. Analysis of variance (ANOVA) is accomplished to identify the contribution of each parameter on the shear strength. A general empirical model is developed to estimate the shear strength as a function of aging conditions using the Arrhenius term. Microstructure analysis is performed at different aging conditions using scanning electron microscope (SEM). The results revealed a significant reduction in the shear strength when the aging level is increased. An increase in the precipitates coarsening and intermetallic compound (IMC) layer thickness are observed with increased aging time and temperature.



2015 ◽  
Vol 2015 (1) ◽  
pp. 000644-000648
Author(s):  
Mary Liu ◽  
Wusheng Yin

Solder joint encapsulant adhesives have been successfully used to enhance the strength of solder joints and improve thermal cycling as well as drop performance in finished products. The use of solder joint encapsulant adhesives can eliminate the need for underfill materials and the underfill process altogether, thus simplifying rework, which results in a lower cost of ownership. Solder joint encapsulant adhesives include: low temperature and high temperature solder joint encapsulant adhesives, and their derivatives. Each solder joint encapsulant adhesive has: unfilled and filled solder joint encapsulant adhesives, and solder joint encapsulant paste. Each solder joint encapsulant product has been designed for different applications. In this paper, we are going to discuss the details and future of solder joint encapsulant adhesives.



1998 ◽  
Vol 120 (4) ◽  
pp. 322-327 ◽  
Author(s):  
H. Doi ◽  
K. Kawano ◽  
A. Yasukawa ◽  
T. Sato

The effect of a heat spreader on the life of the solder joints for underfill-encapsulated, flip-chip packages is investigated through stress analyses and thermal cycling tests. An underfill with suitable mechanical properties is found to be able to prolong the fatigue life of the solder joints even in a package with a heat spreader and an alumina substrate. The delamination of the underfill from the chip is revealed as another critical failure mode for which the shape of the underfill fillet has a large effect.



1992 ◽  
Vol 114 (4) ◽  
pp. 472-476 ◽  
Author(s):  
J. Sauber ◽  
J. Seyyedi

A power-law type creep equation has been added to finite element models to calculate solder joint response to time, temperature, and stress level. The ability of the models to predict solder joint behavior was verified by running a series of creep tests. The models were then solved to determine the solder joint creep strains which occur during thermal cycling. These creep strains were used to predict the degradation of pull strength resulting from thermal cycling. More than 8,600 solder joints were thermally cycled and then individually pull tested to verify the accuracy of the method.



Author(s):  
N. Islam ◽  
J. C. Suhling ◽  
P. Lall ◽  
T. Shete ◽  
H. S. Gale ◽  
...  

In this study, we have examined the thermal cycling reliability of several lead free chip resistor solder joint configurations. Five sizes of resistors (2512, 1206, 0805, 0603, 0402), 2 temperature ranges (−40 to 125°C and −40 to 150°C), and five different solder types have been examined. The solders include the normal SnAgCu alloy recommended by earlier studies (95.5Sn-3.8Ag-0.7Cu), and several variations that include small percentages of Bismuth and Indium to enhance fatigue resistance. Results have been compared to data for standard 63Sn-37Pb joints.



Author(s):  
Ouk Sub Lee ◽  
No Hoon Myoung ◽  
Dong Hyeok Kim

The use of Ball Grid Array (BGA) interconnects utilizing the BGA solder joint has grown rapidly because of its small volume and diversity of its application. Therefore, the continuous quantification and refinement of BGA solder joint in terms of its reliability are required. The creep and cyclically applied mechanical loads generally cause metal fatigue on the BGA solder joint which inevitably leads to an electrical discontinuity. In the field application, the BGA solder joints are known to experience mechanical loads during temperature changes caused by power up/down events as the result of the Coefficient of Thermal Expansion (CTE) mismatch between the substrate and the Si die. In this paper, extremely small resistance changes in the lead free joints corresponding to the through-cracks generated by the thermal fatigue were measured and the failure was defined in terms of anomalous changes in the joint resistance. Furthermore, the reliability of BGA solder joints under thermal cycling was evaluated by using a criterion that may define and distinguish a failure in the solder joint. Any changes in circuit resistance according to the accumulated damage induced by the thermal cycling in the joint were recorded and evaluated by the First Order Reliability Method (FORM) procedure in order to quantify the reliability of solder joint. The first order Taylor series expansion of the limit state function incorporating with thermal fatigue models is used in order to estimate the failure probability of solder joints under heated condition. Various thermal fatigue models are utilized in this study. Models based on various plastic-strain rates such as Coffin-Manson fatigue model, total strain fatigue model and Solomon fatigue model are utilized in this study. The effects of random variables such as the CTE, the pitch of solder joint, the diameter of solder joint, and the CTE difference solder joints on the failure probability of the solder joint are systematically investigated by using a failure probability model with the FORM.



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