High-performance monochromator of parallel x-rays on the basis of Kumakhov polycapillary optics

2005 ◽  
Author(s):  
E. V. Likhoushina ◽  
M. A. Kumakhov ◽  
N. S. Ibraimov ◽  
S. V. Nikitina ◽  
A. A. Bolotokov ◽  
...  
Author(s):  
Marc H. Peeters ◽  
Max T. Otten

Over the past decades, the combination of energy-dispersive analysis of X-rays and scanning electron microscopy has proved to be a powerful tool for fast and reliable elemental characterization of a large variety of specimens. The technique has evolved rapidly from a purely qualitative characterization method to a reliable quantitative way of analysis. In the last 5 years, an increasing need for automation is observed, whereby energy-dispersive analysers control the beam and stage movement of the scanning electron microscope in order to collect digital X-ray images and perform unattended point analysis over multiple locations.The Philips High-speed Analysis of X-rays system (PHAX-Scan) makes use of the high performance dual-processor structure of the EDAX PV9900 analyser and the databus structure of the Philips series 500 scanning electron microscope to provide a highly automated, user-friendly and extremely fast microanalysis system. The software that runs on the hardware described above was specifically designed to provide the ultimate attainable speed on the system.


2014 ◽  
Vol 606 ◽  
pp. 265-268 ◽  
Author(s):  
Martin Bednarik ◽  
David Manas ◽  
Miroslav Manas ◽  
Martin Ovsik ◽  
Jan Navratil ◽  
...  

Radiation cross-linking gives inexpensive commodity plastics and technical plastics the mechanical, thermal, and chemical properties of high-performance plastic. This upgrading of the plastics enables them to be used in conditions which they would not be able to with stand otherwise. The irradiation cross-linking of thermoplastic materials via electron beam or cobalt 60 (gammy rays) is performed separately, after processing. Generally, ionizing radiation includes accelerated electrons, gamma rays and X-rays. Radiation processing with an electron beam offers several distinct advantages when compared with other radiation sources, particularly γ-rays and x-rays. The process is very fast, clean and can be controlled with much precision. There is no permanent radioactivity since the machine can be switched off. In contrast to γ-rays and x-rays, the electron beam can steered relatively easily, thus allowing irradiation of a variety of physical shapes. The energy-rich beta rays trigger chemical reactions in the plastics which results in networking of molecules (comparable to the vulcanization of rubbers which has been in industrial use for so long). The energy from the rays is absorbed by the material and cleavage of chemical bonds takes place. This releases free radicals which in next phase from desired molecular bonds. This article describes the effect of radiation cross-linking on the surface and adhesive properties of low-density polyethylene.


2020 ◽  
Author(s):  
Tuan Pham

Chest X-rays have been found to be very promising for assessing COVID-19 patients, especially for resolving emergency-department and urgent-care-center overcapacity. Deep-learning (DL) methods in artificial intelligence (AI) play a dominant role as high-performance classifiers in the detection of the disease using chest X-rays. While many new DL models have been being developed for this purpose, this study aimed to investigate the fine tuning of pretrained convolutional neural networks (CNNs) for the classification of COVID-19 using chest X-rays. Three pretrained CNNs, which are AlexNet, GoogleNet, and SqueezeNet, were selected and fine-tuned without data augmentation to carry out 2-class and 3-class classification tasks using 3 public chest X-ray databases. In comparison with other recently developed DL models, the 3 pretrained CNNs achieved very high classification results in terms of accuracy, sensitivity, specificity, precision, F1 score, and area under the receiver-operating-characteristic curve. AlexNet, GoogleNet, and SqueezeNet require the least training time among pretrained DL models, but with suitable selection of training parameters, excellent classification results can be achieved without data augmentation by these networks. The findings contribute to the urgent need for harnessing the pandemic by facilitating the deployment of AI tools that are fully automated and readily available in the public domain for rapid implementation.


2019 ◽  
Vol 12 (3) ◽  
pp. 3847-3853
Author(s):  
Hsiao-Chi Lu ◽  
Jen-Iu Lo ◽  
Yu-Chain Peng ◽  
Sheng-Lung Chou ◽  
Bing-Ming Cheng ◽  
...  

2005 ◽  
Vol 498-499 ◽  
pp. 506-511 ◽  
Author(s):  
Maria do Carmo de Andrade Nono

CeO2- ZrO2 ceramics are considered a candidate material for applications as structural high performance ceramics. In this work are presented and discussed the tetragonal-to-monoclinic stress-induced transformation influence on the mechanical properties in these ceramics. Sintered ceramics were fabricated from powders mixtures containing ZrO2 and 8 to 14 CeO2 % mol. SEM observations were used to study de ceramic microstructures and X-rays diffraction to identification and determination of tetragonal and monoclinic phases. It was adopted the 4-point bending tests, Vickers surface hardness and fracture toughness technique to the determination of the mechanical parameters. The results showed that the mechanical properties were strongly dependent of the CeO2 content, the microstructure and the fraction of tetragonal-to-monoclinic stress-induced transformation.


1998 ◽  
Vol 524 ◽  
Author(s):  
S. Tamura ◽  
K. Ohtani ◽  
M. Yasumoto ◽  
K. Murali ◽  
N. Kamuo ◽  
...  

ABSTRACTA hard X-ray microbeam with submicrometer spot size from synchrotron radiation (SR) sources is expected to add a new dimension to various X-ray analysis methods. A Fresnel zone plate (FZP) is one of the promising focusing elements for X-rays. In order to develop high performance multilayer FZP for use in the hard X-ray region, Cu/Al concentric multilayers were fabricated by use of a DC sputtering deposition process. Lower Ar gas pressure or higher rotating speed of a wire substrate has been effective in forming smoother multilayer interfaces. From a focusing test of the Cu/Al FZP (100-zones) by the SR (λ= 0.154nm), microbeams of 1.5 μm φ and 0.8 μm φ have been achieved for the first- and third-order focal beams, respectively.


2002 ◽  
Vol 17 (2) ◽  
pp. 70-80 ◽  
Author(s):  
Paul J. Schields ◽  
David M. Gibson ◽  
Walter M. Gibson ◽  
Ning Gao ◽  
Huapeng Huang ◽  
...  

Polycapillary optics are utilized in a wide variety of applications and are integral components in many state of the art instruments. Polycapillary optics operate by collecting X-rays and efficiently propagating them by total external reflection to form focused and parallel beams. We discuss the general parameters for designing these optics and provide specific examples on balancing the interrelations of beam flux, source size, focal spot-size, and beam divergence. The development of compact X-ray sources with characteristics tailored to match the requirements of polycapillary optics allows substantial reduction in size, weight, and power of complete X-ray systems. These compact systems have enabled the development of portable, remote, and in-line sensors for applications in industry, science and medicine. We present examples of the utility and potential of these optics for enhancing a wide variety of X-ray analyses.


2010 ◽  
Vol 638-642 ◽  
pp. 967-972
Author(s):  
Bernd R. Müller ◽  
Axel Lange ◽  
M. Harwardt ◽  
M.P. Hentschel

X-ray computed tomography is an important tool for evaluating the three dimensional microstructure of modern materials non-destructively. To resolve material structures in the micrometre range and below high brilliance synchrotron radiation has to be taken. But materials of low absorption or mixed phases show a weak absorption contrast at there interfaces. A Contrast enhancement can be achieved by exploiting the refraction of X-rays at interfaces. This technique was developed and applied at the NDT department of the Federal Institute for Materials Research and Testing (BAM) during the last decade. It meets the actual demand for improved non-destructive characterisation of high performance composites, ceramics and other low density materials and components. The technique is based on Ultra Small Angle Scattering (USAXS) by micro structural elements causing phase related effects like refraction and total reflection at a few minutes of arc as the refractive index of X-rays is nearly unity. The extraordinary refraction contrast of inner surfaces is far beyond absorption effects and hence especially useful for materials of low absorption or mixed phases, showing similar X-ray absorption properties. Crack orientation and fibre-matrix debonding in plastics, polymers, ceramics and metal-matrix-composites after cyclic loading and hydro thermal aging can be visualized. By combining the refraction technique with the computed tomography technique the three dimensional imaging of the micro structure of the materials is obtained. In most cases the investigated inner surface and interface structures correlate to mechanical properties. Recent results with a sub-micrometer resolution will be presented.


2021 ◽  
Vol 28 (2) ◽  
pp. 439-447
Author(s):  
Yasukazu Nakaye ◽  
Takuto Sakumura ◽  
Yasutaka Sakuma ◽  
Satoshi Mikusu ◽  
Arkadiusz Dawiec ◽  
...  

Hybrid photon counting (HPC) detectors are widely used at both synchrotron facilities and in-house laboratories. The features of HPC detectors, such as no readout noise, high dynamic range, high frame rate, excellent point spread function, no blurring etc. along with fast data acquisition, provide a high-performance detector with a low detection limit and high sensitivity. Several HPC detector systems have been developed around the world. A number of them are commercially available and used in academia and industry. One of the important features of an HPC detector is a fast readout speed. Most HPC detectors can easily achieve over 1000 frames s−1, one or two orders of magnitude faster than conventional CCD detectors. Nevertheless, advanced scientific challenges require ever faster detectors in order to study dynamical phenomena in matter. The XSPA-500k detector can achieve 56 kframes s−1 continuously, without dead-time between frames. Using `burst mode', a special mode of the UFXC32k ASIC, the frame rate reaches 1 000 000 frames s−1. XSPA-500k was fully evaluated at the Metrology beamline at Synchrotron SOLEIL (France) and its readout speed was confirmed by tracking the synchrotron bunch time structure. The uniformity of response, modulation transfer function, linearity, energy resolution and other performance metrics were also verified either with fluorescence X-rays illuminating the full area of the detector or with the direct beam.


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