A Laboratory Plant for Gas Liquefaction

2015 ◽  
Vol 23 (02) ◽  
pp. 1550010 ◽  
Author(s):  
M. De Salve ◽  
D. Milani ◽  
B. Panella ◽  
G. Roveta

A prototype gas liquefaction plant has been designed and manufactured for Politecnico di Torino cryogenic laboratory and has been used for cryogenic applications like superconducting cables and low temperature refrigeration devices. The plant is able to liquefy nitrogen and, by means of little changes, hydrogen and other cryogenic fluids too. The thermal energy is removed by four high speed (up to 360 000 revolutions per minute) helium turbines that are connected in series. The gas liquefaction is carried out by the cooling condensation process of the gas flow that feeds a 0.15 m3 super insulated tank that is cooled inside. The cryogenic system is based on the Claude and Collins cycles, fed with helium that provides the cold sink. The paper shows the characteristics of the plant main components, and the time history of the measured temperatures, pressures, and flow rates during the plant start-up, as well as the steady state liquefied gas production rate. From the energetic point of view, the plant performance is acceptable for a research laboratory and the plant efficiency is not far from that of commercial larger size plants.

Energies ◽  
2020 ◽  
Vol 13 (6) ◽  
pp. 1522
Author(s):  
Zhongyi Xu ◽  
Shaohua Gu ◽  
Daqian Zeng ◽  
Bing Sun ◽  
Liang Xue

Sulfur deposition commonly occurs during the development of a high-sulfur gas reservoirs. Due to the high gas flow velocity near the wellbore, some of the deposited sulfur particles re-enter the pores and continue to migrate driven by the high-speed gas flow. The current mathematical model for sulfur deposition ignores the viscosity between particles, rising flow caused by turbulence, and the corresponding research on the release ratio of particles. In order to solve the above problems, firstly, the viscous force and rising force caused by turbulence disturbance are introduced, and the critical release velocity of sulfur particles is derived. Then, a release model of sulfur particles that consider the critical release velocity and release ratio is proposed by combining the probability theory with the hydrodynamics theory. Notably, based on the experimental data, the deposition ratio of sulfur particles and the damage coefficient in the sulfur damage model are determined. Finally, a comprehensive particle migration model considering the deposition and release of sulfur particles is established. The model is then applied to the actual gas wells with visible sulfur deposition that target the Da-wan gas reservoir, and the results show that the model correctly reflects flow transport during the process of sulfur deposition in porous media. In addition, through the numerical simulation experiments, it was found that considering the release of sulfur particles reduces the saturation of sulfur particles within a specific range around the well and improve the reservoir permeability in this range. From the perspective of gas production rate, the release of sulfur particles has a limited effect on the gas production rate, which is mainly due to the sulfur particle release being limited, having only a 5 m range near the wellbore area, and thus the amount of gas flow from the unaffected area is basically unchanged.


2018 ◽  
Vol 15 (1) ◽  
pp. 21-33
Author(s):  
Ying Wei ◽  
Yongqiao Liu ◽  
Yifan Hele ◽  
Weiwei Sun ◽  
Yang Wang ◽  
...  

Background: Gentianella acuta (Michx.) Hulten is an important type of medicinal plant found in several Chinese provinces. It has been widely used in folk medicine to treat various illnesses. However, there is not enough detailed information about the chemical constituents of this plant or methods for their content determination. Objective: The focus of this work is the isolation and characterization of the major chemical constituents of Gentianella acuta, and developing an analytical method for their determination. Methods: The components of Gentianella acuta were isolated using (1) ethanol extraction and adsorption on macroporous resin. (2) and ethyl acetate extraction and high speed countercurrent chromatography. A HPLC-DAD method was developed using a C18 column and water-acetonitrile as the mobile phase. Based on compound polarities, both isocratic and gradient elution methods were developed. Results: A total of 29 compounds were isolated from this plant, of which 17 compounds were isolated from this genus for the first time. The main components in this plant were found to be xanthones. The HPLC-DAD method was developed and validated for their determination, and found to show good sensitivity and reliability. Conclusion: The results of this work add to the limited body of work available on this important medicinal plant. The findings will be useful for further investigation and development of Gentianella acuta for its valuable medicinal properties.


2010 ◽  
Vol 5 (2) ◽  
pp. 1934578X1000500 ◽  
Author(s):  
Maria Graça Miguel ◽  
Cláudia Cruz ◽  
Leonor Faleiro ◽  
Mariana T. F. Simões ◽  
Ana Cristina Figueiredo ◽  
...  

The essential oils from Foeniculum vulgare commercial aerial parts and fruits were isolated by hydrodistillation, with different distillation times (30 min, 1 h, 2 h and 3 h), and analyzed by GC and GC-MS. The antioxidant ability was estimated using four distinct methods. Antibacterial activity was determined by the agar diffusion method. Remarkable differences, and worrying from the quality and safety point of view, were detected in the essential oils. trans-Anethole (31-36%), α-pinene (14-20%) and limonene (11-13%) were the main components of the essentials oil isolated from F. vulgare dried aerial parts, whereas methyl chavicol (= estragole) (79-88%) was dominant in the fruit oils. With the DPPH method the plant oils showed better antioxidant activity than the fruits oils. With the TBARS method and at higher concentrations, fennel essential oils showed a pro-oxidant activity. None of the oils showed a hydroxyl radical scavenging capacity >50%, but they showed an ability to inhibit 5-lipoxygenase. The essential oils showed a very low antimicrobial activity. In general, the essential oils isolated during 2 h were as effective, from the biological activity point of view, as those isolated during 3 h.


2021 ◽  
Vol 11 (9) ◽  
pp. 4045
Author(s):  
Amilcar Duque-Prata ◽  
Carlos Serpa ◽  
Pedro J. S. B. Caridade

The photodegradation mechanism of 1-phenyl-4-allyl-tetrazol-5-one has been studied using (time-dependent) density functional theory with the M06-HF, B3LYP, and PBE0 functionals and the VDZ basis set. All calculations have been carried out using the polarizable continuum model to simulate the solvent effects of methanol. The reaction pathway evolution on the triplet state has been characterised to validate a previously postulated experimental-based mechanism. The transition states and minimums have been initially located by local scanning in partial constrained optimisation, followed by a fully relaxed search procedure. The UV spectra has shown to be better described with PBE0 functional when compared with the experimental results, having the M06-HF a shift of 40 nm. From the energetic point of view, the postulated mechanism has been validated in this work showing a concerted photoextrusion of the N2 molecule. The intramolecular proton transfer occurs at a later stage of the mechanism after cyclization of the allyl group on a triplet biradical intermediate. The photoproduct observed experimentally, a pyrimidinone, has been characterised. The infrared spectroscopic reaction profile has also been proposed.


2021 ◽  
Vol 21 (4) ◽  
Author(s):  
Hytham Elwardany ◽  
Robert Jankowski ◽  
Ayman Seleemah

AbstractSeismic-induced pounding between adjacent buildings may have serious consequences, ranging from minor damage up to total collapse. Therefore, researchers try to mitigate the pounding problem using different methods, such as coupling the adjacent buildings with stiff beams, connecting them using viscoelastic links, and installing damping devices in each building individually. In the current paper, the effect of using linear and nonlinear fluid viscous dampers to mitigate the mutual pounding between a series of structures is investigated. Nonlinear finite-element analysis of a series of adjacent steel buildings equipped with damping devices was conducted. Contact surfaces with both contactor and target were used to model the mutual pounding. The results indicate that the use of linear or nonlinear dampers leads to the significant reduction in the response of adjacent buildings in series. Moreover, the substantial improvement of the performance of buildings has been observed for almost all stories. From the design point of view, it is concluded that dampers implemented in adjacent buildings should be designed to resist maximum force of 6.20 or 1.90 times the design independent force in the case of using linear or nonlinear fluid viscous dampers, respectively. Also, designers should pay attention to the design of the structural elements surrounding dampers, because considerable forces due to pounding may occur in the dampers at the maximum displaced position of the structure.


1952 ◽  
Vol 18 (67) ◽  
pp. 31-35
Author(s):  
Kensuke KAWASHIMO ◽  
Shigebumi AOKI

2018 ◽  
Vol 192 ◽  
pp. 02028
Author(s):  
Hassan Zulkifli Abu ◽  
Ibrahim Aniza ◽  
Mohamad Nor Norazman

Small-scale blast tests were carried out to observe and measure the influence of sandy soil towards explosive blast intensity. The tests were to simulate blast impact imparted by anti-vehicular landmine to a lightweight armoured vehicle (LAV). Time of occurrence of the three phases of detonation phase in soil with respect to upward translation time of the test apparatus were recorded using high-speed video camera. At the same time the target plate acceleration was measured using shock accelerometer. It was observed that target plate deformation took place at early stage of the detonation phase before the apparatus moved vertically upwards. Previous data of acceleration-time history and velocity-time history from air blast detonation were compared. It was observed that effects of soil funnelling on blast wave together with the impact from soil ejecta may have contributed to higher blast intensity that characterized detonation in soil, where detonation in soil demonstrated higher plate velocity compared to what occurred in air blast detonation.


Author(s):  
Marcin Lefik ◽  
Krzysztof Komeza ◽  
Ewa Napieralska-Juszczak ◽  
Daniel Roger ◽  
Piotr Andrzej Napieralski

Purpose The purpose of this paper is to present a comparison between reluctance synchronous machine-enabling work at high internal temperature (HT° machine) with laminated and solid rotor. Design/methodology/approach To obtain heat sources for the thermal model, calculations of the electromagnetic field were made using the Opera 3D program including effect of rotation and the resulting eddy current losses. To analyse the thermal phenomenon, the 3D coupled thermal-fluid (CFD) model is used. Findings The presented results show clearly that laminated construction is much better from a point of view of efficiency and temperature. However, solid construction can be interesting for high speed machines due to their mechanical robustness. Research limitations/implications The main problem, despite the use of parallel calculations, is the long calculation time. Practical implications The obtained simulation and experimental results show the possibility of building a machine operating at a much higher ambient temperature than it was previously produced for example in the vicinity of the aircraft turbines. Originality/value The paper presents the application of fully three-dimensional coupled electromagnetic and thermal analysis of new machine constructions designed for elevated temperature.


2005 ◽  
Author(s):  
Balaji Gopalan ◽  
Edwin Malkiel ◽  
Jian Sheng ◽  
Joseph Katz

High-speed in-line digital holographic cinematography was used to investigate the diffusion of droplets in locally isotropic turbulence. Droplets of diesel fuel (0.3–0.9mm diameter, specific gravity of 0.85) were injected into a 37×37×37mm3 sample volume located in the center of a 160-liter tank. The turbulence was generated by 4 spinning grids, located symmetrically in the corners of the tank, and was characterized prior to the experiments. The sample volume was back illuminated with two perpendicular collimated beams of coherent laser light and time series of in-line holograms were recorded with two high-speed digital cameras at 500 frames/sec. Numerical reconstruction generated a time series of high-resolution images of the droplets throughout the sample volume. We developed an algorithm for automatically detecting the droplet trajectories from each view, for matching the two views to obtain the three-dimensional tracks, and for calculating the time history of velocity. We also measured the mean fluid motion using 2-D PIV. The data enabled us to calculate the Lagrangian velocity autocorrelation function.


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