scholarly journals Pore Structure and Connectivity of Mixed Siliciclastic-Carbonate Tight Reservoirs in the Palaeogene from Qaidam Basin, NW China

Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-20
Author(s):  
Xin Wang ◽  
Jianhui Zeng ◽  
Kunyu Wu ◽  
Xiangcheng Gao ◽  
Yibo Qiu ◽  
...  
Keyword(s):  
Spatial Distribution ◽  
Pore Structure ◽  
Carbonate Rocks ◽  
Qaidam Basin ◽  
Spontaneous Imbibition ◽  
Throat Radius ◽  
Number Range ◽  
X Ray ◽  
Tight Reservoirs ◽  
Intercrystalline Pores

The pore structure and connectivity in petroleum reservoirs are controlled in part by their petrological properties. Mixed siliciclastic-carbonate rocks have complex compositions and heterogeneous spatial distributions of the various minerals. As a result, the study of the pore structure and connectivity of mixed siliciclastic-carbonate tight reservoirs has been limited. In this study, methods such as thin section microscopy, X-ray diffraction, X-ray computed tomography, low pressure N2 adsorption, and spontaneous imbibition were adopted to comprehensively analyze the petrological properties, pore structure, and connectivity of the mixed siliciclastic-carbonate tight reservoirs in the upper member of the Xiaganchaigou Formation in the Yingxi Area, Qaidam Basin. The results showed that micrometer-sized pores in mixed siliciclastic-carbonate tight reservoirs are mainly dissolution pores, and that the spatial distribution of the pores is highly heterogeneous. The average pore radius range, average throat radius range, and average coordination number range of micronmeter-sized pores are 2.09~3.42 μm, 1.32~2.19 μm, and 0.48~1.49, respectively. Restricted by the concentrated distribution of local anhydrite, the connectivity of micronmeter-sized pores develops well only in the anhydrite, showing negligible contribution to the overall reservoir connectivity. In contrast, nanometer-sized pores in the mixed siliciclastic-carbonate tight reservoirs are mainly intercrystalline pores in dolomite. The range of nanometer-sized pores diameters is mainly distributed in 1.73-31.47 nm. The pores have a smooth surface, simple structure, and relatively homogeneous spatial distribution. The dissolution of dolomite intercrystalline pores by acidic fluids increases the connectivity of the nanometer-sized pores. This paper presents genetic models for microscopic pore structures and connectivity of mixed siliciclastic-carbonate rocks, making possible the evaluation on the quality of the mixed siliciclastic-carbonate tight reservoirs.

scholarly journals Pore throat characteristics of tight reservoirs by a combined mercury method: A case study of the member 2 of Xujiahe Formation in Yingshan gasfield, North Sichuan Basin

2021 ◽  
Vol 13 (1) ◽  
pp. 1174-1186
Author(s):  
Youzhi Wang ◽  
Cui Mao ◽  
Qiang Li ◽  
Wei Jin ◽  
Simiao Zhu ◽  
...  
Keyword(s):  
Pore Structure ◽  
Distribution Range ◽  
Contribution Rate ◽  
Pore Throat ◽  
Tight Sandstone ◽  
Throat Radius ◽  
Xujiahe Formation ◽  
Mercury Injection ◽  
Tight Reservoirs ◽  
Sandstone Reservoirs

Abstract The complex pore throat characteristics are significant factors that control the properties of tight sandstone reservoirs. Due to the strong heterogeneity of the pore structure in tight reservoirs, it is difficult to characterize the pore structure by single methods. To determine the pore throat, core, casting thin sections, micrographs from scanning electron microscopy, rate-controlled mercury injection, and high-pressure mercury injection were performed in member 2 of Xujiahe Formation of Yingshan gasfield, Sichuan, China. The pore throat characteristics were quantitatively characterized, and the distribution of pore throat at different scales and its controlling effect on reservoir physical properties were discussed. The results show that there are mainly residual intergranular pores, intergranular dissolved pores, ingranular dissolved pores, intergranular pores, and micro-fractures in the second member of the Xujiahe Formation tight sandstone reservoir. The distribution range of pore throat is 0.018–10 μm, and the radius of pore throat is less than 1 μm. The ranges of pore radius were between 100 and 200 μm, the peak value ranges from 160 to 180 μm, and the pore throat radius ranges from 0.1 to 0.6 μm. With the increase of permeability, the distribution range of throat radius becomes wider, and the single peak throat radius becomes larger, showing the characteristic of right skew. The large throat of the sandy conglomerate reservoir has an obvious control effect on permeability, but little influence on porosity. The contribution rate of nano-sized pore throat to permeability is small, ranging from 3.29 to 34.67%. The contribution rate of porosity was 48.86–94.28%. Therefore, pore throat characteristics are used to select high-quality reservoirs, which can guide oil and gas exploration and development of tight sandstone reservoirs.

Macroprobe Mode for the Study of Segregation in Steels

1990 ◽  
Vol 48 (2) ◽  
pp. 260-261
Author(s):  
Auclair Gilles ◽  
Benoit Danièle
Keyword(s):  
Mechanical Properties ◽  
Spatial Distribution ◽  
High Performance ◽  
Volume Fraction ◽  
Sheet Steel ◽  
Acquisition Time ◽  
Chemical Information ◽  
X Ray ◽  
Accurate Quantitative Analysis ◽  
Optical Micrographs

During these last 10 years, high performance correction procedures have been developed for classical EPMA, and it is nowadays possible to obtain accurate quantitative analysis even for soft X-ray radiations. It is also possible to perform EPMA by adapting this accurate quantitative procedures to unusual applications such as the measurement of the segregation on wide areas in as-cast and sheet steel products.The main objection for analysis of segregation in steel by means of a line-scan mode is that it requires a very heavy sampling plan to make sure that the most significant points are analyzed. Moreover only local chemical information is obtained whereas mechanical properties are also dependant on the volume fraction and the spatial distribution of highly segregated zones. For these reasons we have chosen to systematically acquire X-ray calibrated mappings which give pictures similar to optical micrographs. Although mapping requires lengthy acquisition time there is a corresponding increase in the information given by image anlysis.

scholarly journals Freeze–Thaw Resistance and Air-Void Analysis of Concrete with Recycled Glass–Pozzolan Using X-ray Micro-Tomography

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 154
Author(s):  
Marija Krstic ◽  
Julio F. Davalos ◽  
Emanuele Rossi ◽  
Stefan C. Figueiredo ◽  
Oguzhan Copuroglu
Keyword(s):  
Fly Ash ◽  
Pore Structure ◽  
The United States ◽  
Adsorption Method ◽  
X Ray ◽  
Freeze Thaw ◽  
Void System ◽  
Spatial Parameters ◽  
Micro Tomography ◽  
Air Void

Recent studies have shown promising potential for using Glass Pozzolan (GP) as an alternative supplementary cementitious material (SCM) due to the scarcity of fly ash and slag in the United States. However, comprehensive studies on the freeze–thaw (FT) resistance and air void system of mixtures containing GP are lacking. Therefore, this study aimed to evaluate GP’s effect on FT resistance and characterize mixtures with different GP contents, both macro- and microscopically. In this study, six concrete mixes were considered: Three mixes with 20%, 30% and 40% GP as cement replacements and two other comparable mixes with 30% fly ash and 40% slag, as well as a mix with 100% Ordinary Portland cement (OPC) as a reference. Concrete samples were prepared, cured and tested according to the ASTM standards for accelerated FT resistance for 1000 cycles and corresponding dynamic modulus of elasticity (Ed). All the samples showed minimal deterioration and scaling and high F/T resistance with a durability factor of over 90%. The relationships among FT resistance parameters, air-pressured method measurements of fresh concretes and air void analysis parameters of hardened concretes were examined in this study. X-ray micro-tomography (micro-CT scan) was used to evaluate micro-cracks development after 1000 freeze–thaw cycles and to determine spatial parameters of air voids in the concretes. Pore structure properties obtained from mercury intrusion porosimetry (MIP) and N2 adsorption method showed refined pore structure for higher cement replacement with GP, indicating more gel formation (C-S-H) which was verified by thermogravimetric analysis (TGA).

Comparative Studies of Ultra Low-κ Porous Silica Films with 2-D Hexagonal and Disordered Pore Structures

2004 ◽  
Vol 812 ◽  
Author(s):  
Nobutoshi Fujii ◽  
Kazuhiro Yamada ◽  
Yoshiaki Oku ◽  
Nobuhiro Hata ◽  
Yutaka Seino ◽  
...  
Keyword(s):  
Pore Structure ◽  
Nonionic Surfactants ◽  
Porous Silica ◽  
Silica Film ◽  
X Ray Diffraction ◽  
Silica Films ◽  
X Ray ◽  
X Ray Scattering ◽  
Porous Silica Film ◽  
Diffraction Peaks

AbstractPeriodic 2-dimensional (2-D) hexagonal and the disordered pore structure silica films have been developed using nonionic surfactants as the templates. The pore structure was controlled by the static electrical interaction between the micelle of the surfactant and the silica oligomer. No X-ray diffraction peaks were observed for the disordered mesoporous silica films, while the pore diameters of 2.0-4.0 nm could be measured by small angle X-ray scattering spectroscopy. By comparing the properties of the 2-D hexagonal and the disordered porous silica films which have the same porosity, it is found that the disordered porous silica film has advantages in terms of the dielectric constant and Young's modulus as well as the hardness. The disordered porous silica film is more suitable for the interlayer dielectrics for ULSI.

Element-specific structural analysis of Si/B4C using resonant X-ray reflectivity

2015 ◽  
Vol 48 (3) ◽  
pp. 786-796 ◽  
Author(s):  
Maheswar Nayak ◽  
P. C. Pradhan ◽  
G. S. Lodha
Keyword(s):  
Thin Film ◽  
Spatial Distribution ◽  
Structural Analysis ◽  
Chemical Changes ◽  
X Ray ◽  
Buried Interfaces ◽  
Smooth Interface ◽  
Specific Composition ◽  
Applied Fields ◽  
Spatial Modulations

Element-specific structural analysis at the buried interface of a low electron density contrast system is important in many applied fields. The analysis of nanoscaled Si/B4C buried interfaces is demonstrated using resonant X-ray reflectivity. This technique combines information about spatial modulations of charges provided by scattering, which is further enhanced near the resonance, with the sensitivity to electronic structure provided by spectroscopy. Si/B4C thin-film structures are studied by varying the position of B4C in Si layers. Measured values of near-edge optical properties are correlated with the resonant reflectivity profile to quantify the element-specific composition. It is observed that, although Si/B4C forms a smooth interface, there are chemical changes in the sputtered B4C layer. Nondestructive quantification of the chemical changes and the spatial distribution of the constituents is reported.

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