Macroprobe Mode for the Study of Segregation in Steels

1990 ◽  
Vol 48 (2) ◽  
pp. 260-261
Author(s):  
Auclair Gilles ◽  
Benoit Danièle
Keyword(s):  
Mechanical Properties ◽  
Spatial Distribution ◽  
High Performance ◽  
Volume Fraction ◽  
Sheet Steel ◽  
Acquisition Time ◽  
Chemical Information ◽  
X Ray ◽  
Accurate Quantitative Analysis ◽  
Optical Micrographs

During these last 10 years, high performance correction procedures have been developed for classical EPMA, and it is nowadays possible to obtain accurate quantitative analysis even for soft X-ray radiations. It is also possible to perform EPMA by adapting this accurate quantitative procedures to unusual applications such as the measurement of the segregation on wide areas in as-cast and sheet steel products.The main objection for analysis of segregation in steel by means of a line-scan mode is that it requires a very heavy sampling plan to make sure that the most significant points are analyzed. Moreover only local chemical information is obtained whereas mechanical properties are also dependant on the volume fraction and the spatial distribution of highly segregated zones. For these reasons we have chosen to systematically acquire X-ray calibrated mappings which give pictures similar to optical micrographs. Although mapping requires lengthy acquisition time there is a corresponding increase in the information given by image anlysis.

scholarly journals Enhancement of Chloroprene/Natural/Butadiene Rubber Nanocomposite Properties Using Organoclays and Their Combination with Carbon Black as Fillers

Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1085
Author(s):  
Patricia Castaño-Rivera ◽  
Isabel Calle-Holguín ◽  
Johanna Castaño ◽  
Gustavo Cabrera-Barjas ◽  
Karen Galvez-Garrido ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Carbon Black ◽  
High Performance ◽  
Rubber Matrix ◽  
Butadiene Rubber ◽  
X Ray Diffraction ◽  
X Ray ◽  
Rubber Blends ◽  
Ft Ir ◽  
Chloroprene Rubber

Organoclay nanoparticles (Cloisite® C10A, Cloisite® C15) and their combination with carbon black (N330) were studied as fillers in chloroprene/natural/butadiene rubber blends to prepare nanocomposites. The effect of filler type and load on the physical mechanical properties of nanocomposites was determined and correlated with its structure, compatibility and cure properties using Fourier Transformed Infrared (FT-IR), X-ray Diffraction (XRD), Thermogravimetric Analysis (TGA) and rheometric analysis. Physical mechanical properties were improved by organoclays at 5–7 phr. Nanocomposites with organoclays exhibited a remarkable increase up to 46% in abrasion resistance. The improvement in properties was attributed to good organoclay dispersion in the rubber matrix and to the compatibility between them and the chloroprene rubber. Carbon black at a 40 phr load was not the optimal concentration to interact with organoclays. The present study confirmed that organoclays can be a reinforcing filler for high performance applications in rubber nanocomposites.

Effect of Si Content on Microstructure and Properties of 60Si2CrVA Spring Steel

2014 ◽  
Vol 968 ◽  
pp. 63-66 ◽  
Author(s):  
Fei Zhao ◽  
Zhan Ling Zhang ◽  
Jun Shuai Li ◽  
Cui Ye ◽  
Ni Li
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Testing Machine ◽  
Spring Steel ◽  
Impact Testing ◽  
X Ray ◽  
Comprehensive Properties ◽  
Spring Steels ◽  
Si Content

The microstructure and mechanical properties of the four spring steels with different Si content treated by Q-I-Q-T process were studied by metallographic microscope, MTS, impact testing machine and X-ray stress analyzer. The results show that the tensile strength and yield strength is first increased and then decreased with the increase of Si content, the volume fraction of retained austenite and elongation are fist decreased and then increased when the Si content is less than 2.1%, and the microstructure become finer and homogeneous. When Si content reaches 2.1%, the comprehensive properties of 60Si2CrVA spring steel is the best.

Stress in Hydrogenated Microcrystalline Silicon Thin Films

1999 ◽  
Vol 557 ◽  
Author(s):  
D. Peiró ◽  
C. Voz ◽  
J. Bertomeu ◽  
J. Andreu ◽  
E. Martínez ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Vapor Deposition ◽  
Volume Fraction ◽  
Chemical Vapor ◽  
Hot Wire ◽  
X Ray Diffraction ◽  
Microcrystalline Silicon ◽  
X Ray ◽  
Silicon Thin Films ◽  
Abrupt Changes

AbstractHydrogenated microcrystalline silicon films have been obtained by hot-wire chemical vapor deposition (HWCVD) in a silane and hydrogen mixture at low pressure (<5 × 10-2 mbar). The structure of the samples and the residual stress were characterised by X- ray diffraction (XRD). Raman spectroscopy was used to estimate the volume fraction of the crystalline phase, which is in the range of 86 % to 98%. The stress values range between 150 and -140 MPa. The mechanical properties were studied by nanoindentation. Unlike monocrystalline wafers, there is no evidence of abrupt changes in the force-penetration plot, which have been attributed to a pressure-induced phase transition. The hardness was 12.5 GPa for the best samples, which is close to that obtained for silicon wafers.

scholarly journals Characterisation of a High-Performance Al–Zn–Mg–Cu Alloy Designed for Wire Arc Additive Manufacturing

Materials ◽  
2020 ◽  
Vol 13 (7) ◽  
pp. 1610 ◽  
Author(s):  
Paulo J. Morais ◽  
Bianca Gomes ◽  
Pedro Santos ◽  
Manuel Gomes ◽  
Rudolf Gradinger ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
High Performance ◽  
Mechanical Performance ◽  
Fluorescence Analysis ◽  
Cold Metal Transfer ◽  
Direction Parallel ◽  
X Ray ◽  
Wire Arc Additive Manufacturing

Ever-increasing demands of industrial manufacturing regarding mechanical properties require the development of novel alloys designed towards the respective manufacturing process. Here, we consider wire arc additive manufacturing. To this end, Al alloys with additions of Zn, Mg and Cu have been designed considering the requirements of good mechanical properties and limited hot cracking susceptibility. The samples were produced using the cold metal transfer pulse advanced (CMT-PADV) technique, known for its ability to produce lower porosity parts with smaller grain size. After material simulations to determine the optimal heat treatment, the samples were solution heat treated, quenched and aged to enhance their mechanical performance. Chemical analysis, mechanical properties and microstructure evolution were evaluated using optical light microscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray fluorescence analysis and X-ray radiography, as well as tensile, fatigue and hardness tests. The objective of this research was to evaluate in detail the mechanical properties and microstructure of the newly designed high-performance Al–Zn-based alloy before and after ageing heat treatment. The only defects found in the parts built under optimised conditions were small dispersed porosities, without any visible cracks or lack of fusion. Furthermore, the mechanical properties are superior to those of commercial 7xxx alloys and remarkably independent of the testing direction (parallel or perpendicular to the deposit beads). The presented analyses are very promising regarding additive manufacturing of high-strength aluminium alloys.

Impact of Steel Fibers on Workability and Properties of UHPC

2016 ◽  
Vol 249 ◽  
pp. 57-61 ◽  
Author(s):  
Milan Rydval ◽  
Tomáš Bittner ◽  
Jiří Kolísko ◽  
Šárka Nenadálová
Keyword(s):  
Mechanical Properties ◽  
High Performance ◽  
High Performance Concrete ◽  
Volume Fraction ◽  
Fresh Concrete ◽  
Mixture Design ◽  
Steel Fibers ◽  
Hardened Concrete ◽  
Hardened Cement ◽  
The Impact

This paper is focused on properties of fresh and hardened cement-based composite Ultra-High Performance Concrete with regard to different volume fraction of short brass coated steel fibers BASF MASTERFIBER® 482. Workability of fresh concrete and basic mechanical properties (tensile strength in bending, compressive strength) of hardened UHPC were found out. The workability of fresh concrete was measured by small mortar Haegermann cone. Percentage differences at cost were obtained at hardened concrete, too. The aim of the first experimental part of the research was the impact of volume fraction of steel fibers according to workability of fresh concrete and also according to mechanical properties of hardened UHPC with the same volume fraction of each component of the mixture, only the volume fraction of the steel fibers was different at each mixture. The mixture design of UHPC was changed to maintaining the workability of fresh concrete at the second part of the research. The workability at mixture with dosage of steel fibers of 300 kg/m3 measured by Haegermann cone was around 300 mm. In the framework of grant project GAČR 15-05791S the basic mechanical properties of hardened fine-grained cementitious composite material UHPC at small beams size of 160/40/40 mm and beams size 300/70/70 mm were determined. The aim of the research project was not only the determination of basic mechanical properties for each mixture design but also workability assessment and costs linked with higher amount of the volume fracture of steel fibers.

Three-Dimensional Characterization of the Microstructure of Bioglass/Polyethylene Composite by X-Ray Microtomography

2007 ◽  
Vol 330-332 ◽  
pp. 503-506
Author(s):  
Xiao Wei Fu ◽  
Jie Huang ◽  
E.S. Thian ◽  
Serena Best ◽  
William Bonfield
Keyword(s):  
Spatial Distribution ◽  
Volume Fraction ◽  
Three Dimensional ◽  
X Ray ◽  
Polyethylene Composite ◽  
Bioactive Properties ◽  
Recent Developments ◽  
3D Information

A Bioglass® reinforced polyethylene (Bioglass®/polyethylene) composite has been prepared, which combines the high bioactivity of Bioglass® and the toughness of polyethylene. The spatial distribution of Bioglass® particles within the composite is important for the performance of composites in-vivo. Recent developments in X-ray microtomography (XμT) have made it possible to visualize internal and microstructural details with different X-ray absorbencies, nondestructively, and to acquire 3D information at high spatial resolution. In this study, the volume fraction and 3D spatial distribution of Bioglass® particles has been acquired quantitatively by XμT. The information obtained provides a foundation for understanding the mechanical and bioactive properties of the Bioglass®/polyethylene composites.

Quantitative Evaluation of The Chemical Composition of γ-γ’Interfaces in Ni Superalloys

2001 ◽  
Vol 7 (S2) ◽  
pp. 264-265
Author(s):  
H. A. Calderon ◽  
M. Benyoucef ◽  
N. Clement
Keyword(s):  
Mechanical Properties ◽  
Spatial Distribution ◽  
Chemical Composition ◽  
Large Volume ◽  
Alloy Composition ◽  
Volume Fraction ◽  
Alloying Elements ◽  
Local Distribution ◽  
Strain Fields ◽  
Ni Alloys

The excellent mechanical properties of Ni based superalloys depend upon the presence of γ’ particles (LI2 structure). Their volume fraction, spatial distribution and size determine the mechanical strength of these alloys. Ni alloys for technological applications make use of large volume fractions of precipitates where processes of coarsening and coalescence take place during service leading in some cases to deterioration of properties. Addition of different alloying elements prevents accelerated coalescence by retarding diffusion and thus improving the mechanical properties of such alloys. Coalescence can also take place under the influence of an applied stress leading to the formation of rafts of the y' phase. For example the microstructure changes during creep deformation, depending on the alloy composition, with the corresponding formation of dislocation networks and rafts of different morphologies [1]. The γ-γ’ interfaces are also different depending on the alloy composition and most likely to the local distribution of alloying elements and their strain fields.

Stretching-Induced Orientation for Improving the Mechanical Properties of Electrospun Polyacrylonitrile Nanofiber Sheet

2008 ◽  
Vol 47-50 ◽  
pp. 1169-1172 ◽  
Author(s):  
Si Zhu Wu ◽  
Feng Zhang ◽  
Xiao Xiao Hou ◽  
Xiao Ping Yang
Keyword(s):  
Mechanical Properties ◽  
Carbon Nanofibers ◽  
Molecular Orientation ◽  
High Performance ◽  
Carbon Composites ◽  
X Ray Diffraction ◽  
Fiber Alignment ◽  
X Ray ◽  
N2 Atmosphere ◽  
Potential Precursor

Partially aligned and oriented polyacrylonitrile(PAN)-based nanofibers were electrospun from PAN and CNTs/PAN in the solution of dimethylformamide(DMF) to manufacture the carbon nanofibers. The as-spun nanofibers were hot-stretched in a temperature controlled oven to enhance its crystallinity and molecular orientation. Therefore it were stabilized at 250 ( under a stress, and carbonized at 1000 ( in N2 atmosphere by fixing the length of the stabilized nanofiber to convert them into carbon nanofibers. With the hot-stretched process and with the content of CNTs, the mechanical properties will be enhanced correspondingly. The crystallinity of the stretched fibers confirmed by X-ray diffraction has also increased. For PAN nanofibers, the improved fiber alignment and crystallinity resulted in the increased mechanical properties, such as the modulus and tensile strength of the nanofibers. It was concluded that the hot-stretched nanofiber and the CNTs/PAN nanofibers can be used as a potential precursor to produce high-performance carbon composites.

Fabrication and mechanical properties of Al/Al2O3 composite bodies by reactive infiltration of molten Al into SiO2 preform

2000 ◽  
Vol 15 (11) ◽  
pp. 2314-2321 ◽  
Author(s):  
Noboru Yoshikawa ◽  
Singo Funahashi ◽  
Shoji Taniguchi ◽  
Atsushi Kikuchi
Keyword(s):  
Mechanical Properties ◽  
Volume Fraction ◽  
Sintering Temperature ◽  
Pore Space ◽  
Pressure Infiltration ◽  
X Ray ◽  
Reactive Infiltration ◽  
Pore Size Distributions ◽  
Different Temperatures ◽  
Si Content

Al/Al2O3 composites were fabricated by a displacement reaction between SiO2 and molten Al. In this study, fabrication of Al/Al2O3 composites was attempted by means of reactive infiltration to provide variation of their mechanical properties. SiO2 preforms having various porosities and pore size distributions were prepared by sintering the powder at different temperatures between 1273 and 1723 K. Molten Al was infiltrated at 1373 K without application of pressure. Infiltration kinetics were studied and the microstructures of the composite bodies were observed by means of scanning electron microscopy (with energy dispersive x-ray microanalysis), wave dispersive x-ray microanalysis, and x-ray diffractions. The infiltrated specimens were mainly composed of Al and α–Al2O3 phases, and the Si content was less than 5 at.%. Volume fraction of Al phase in the composite bodies was not altered very much with the porosities of the SiO2 preforms because of the difficulty in filling out the entire pore space. Properties and microstructures of Al/Al2O3 composites, however, were dependent on the sintering temperature of the SiO2 preforms. In the case of low sintering temperature, a thick Al channel existed, which deformed upon compression. In the case of high sintering temperature, the microstructure became homogeneous and had thinner Al channels. The composite bodies became brittle. The deformation behavior was shown to be changed from ductile to brittle as an increase of the sintering temperature of the preforms.

Fast reconstruction tools for ptychography at Sirius, the fourth-generation Brazilian synchrotron

2020 ◽  
Vol 53 (6) ◽  
pp. 1550-1558
Author(s):  
Giovanni L. Baraldi ◽  
Carlos S. B. Dias ◽  
Francisco M. C. Silva ◽  
Hélio C. N. Tolentino ◽  
Eduardo X. Miqueles
Keyword(s):  
High Speed ◽  
High Performance ◽  
Phase Retrieval ◽  
Scattering Data ◽  
Fourth Generation ◽  
Acquisition Time ◽  
Optimization Strategy ◽  
X Ray ◽  
Mixed Precision ◽  
Synchrotron Light

Described here are image reconstruction optimizations for ptychographic coherent X-ray scattering data and X-ray fluorescence, which have been developed for the new fourth-generation synchrotron light source, Sirius, at the Brazilian Synchrotron Light Laboratory. The optimization strategy has been applied to the standard experimental strategy for ptychographic and fluorescence experiments on the Carnaúba beamline which involves the use of high-speed continuous scans (fly scans) for a fast acquisition time over large areas through the use of a newly proposed trajectory named the alternating linear trajectory. The scientific computing developments presented here target an efficient use of graphical processing units (GPUs) to the point where large fly-scan acquisitions can be processed in real time on a local high-performance computer. Some optimizations involving a custom fast Fourier transform implementation and use of mixed precision can be applied to other algorithms and phase-retrieval techniques, and therefore this work provides a general optimization scheme. Finally, the optimization strategy presented here has improved performance by a factor of ∼2.5 times faster when compared with non-optimized GPU implementations.

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