Utilizing Scanning Electron Microscopy Stereoscopy to Explain the Wear Behavior of Latch Needles

2009 ◽  
Vol 80 (1) ◽  
pp. 25-34
Author(s):  
Dilek Çukul ◽  
Cevza Candan ◽  
Servet Turan
2003 ◽  
Vol 767 ◽  
Author(s):  
A. K. Sikder ◽  
S. Thagella ◽  
P. B. Zantye ◽  
Ashok Kumar

AbstractLower mechanical strength, reduced cohesive strength and lack of compatibility with other interconnect materials, are the major challenges involved in chemical mechanical polishing (CMP) of Cu metallization with ultra low-k materials as interlayer dielectrics. In this study we have investigated the polishing behavior of patterned Cu samples with underneath different low-k materials using two different slurries and a wide range of machine parameters. CMP micro tribometer was used to polish the samples with different rotations of platen (50 to 250 RPM) and down forces (1-6 PSI). Friction co-efficient and wear behavior were also investigated at different conditions. Optical and scanning electron microscopy was used to investigate the polished surface. It was observed that the two different Cu slurries used for polishing have marked effects on the polishing of Cu-low-k stack with respect to wear and delamination.


2007 ◽  
Vol 546-549 ◽  
pp. 1699-1702
Author(s):  
Xi Ying Zhou ◽  
Liang He ◽  
Yan Hui Liu

Al-Cu-Fe quasicrystals powder was used to prepare the thin films on the surface of the A3 steel by the means of DMD-450 vacuum evaporation equipment. The thin films with different characterization were obtained through different parameters. The microstructures of the thin films were analyzed by Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD). Additionally, the nano-hardness and the modulus of the films are tested by MTS and Neophot micro-hardness meter. The results showed that the modulus of the films was about 160GPa. Nano hardness of the films was about 7.5 Gpa. The films consisted of CuAl2, AlCu3. The thickness and the micro-hardness of the films are improved. In same way, with the increase of the electric current, the thickness and the hardness of the films are also improved. Along with increase of the time and the electric current, the wear behavior of the films was improved. To some extent, the microstructure of films contained the quasicrystal phase of Al65Cu20Fe15.


Metals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 207
Author(s):  
Eleonora Santecchia ◽  
Marcello Cabibbo ◽  
Abdel Magid Salem Hamouda ◽  
Farayi Musharavati ◽  
Anton Popelka ◽  
...  

The applications of aluminum and its alloys are still limited by low hardness and low wear resistance properties. Surface modifications, such anodizing and plasma electrolytic oxidation, represent a feasible way to overcome these drawbacks. In this study, discs of AA6082 were subjected to the so-called G.H.A. hard anodizing process leading to an anodized layer having a honeycomb-like structure. Samples having alumina layer thicknesses of 10, 50 and 100 μm were subjected to unidirectional dry sliding wear tests, using bearing steel and silicon nitride as counterbody materials. Surface and structure characterization of the samples were performed before and after the tribological tests, using a wide range of techniques; atomic force microscopy and scanning electron microscopy techniques were used before the wear tests. The wear scars were characterized by scanning electron microscopy, energy dispersive spectroscopy and Fourier transform infrared spectroscopy techniques. Results show that the different thickness of the anodized layer does not affect the pores dimensions but has an influence on the micrometric domains in which the pores are divided. These features coupled with the wear test conditions, show to have a strong influence on the wear behavior. The thinnest sample showed also the best performance against the ceramic counterbody.


2020 ◽  
Vol 27 (11) ◽  
pp. 2050004
Author(s):  
HAMID GHANBARI ADIVI ◽  
IMAN EBRAHIMZADEH ◽  
MORTEZA HADI ◽  
MORTEZA TAYEBI

The pure iron and aluminum powders were milled with 3[Formula: see text]wt.% and 7[Formula: see text]wt.% of alumina nanoparticles in planetary ball mill in order to produce iron aluminide by mechanical alloying technique. The resulting powder mixture was sintered after the formation of iron aluminide by spark plasma sintering (SPS) method to achieve specimens with the highest densification. SPS technique was utilized on specimens under the condition of 40[Formula: see text]MPa pressure at 950∘C for 5[Formula: see text]min. The microstructures were analyzed after sintering using scanning electron microscopy and EDS analysis. The results indicated that the aluminide iron phase has been produced at high purity. The sintered specimens were treated under hardness and density tests, and it was characterized that the specimen included 3[Formula: see text]wt.% of alumina nanoparticles had the highest microhardness. Likewise, it was revealed that the unreinforced sample had a maximum relative density. The wear behavior of specimens was performed at 600∘C. The results of weight loss showed after 1000[Formula: see text]m of wear test, the weight loss of unreinforced specimen was reduced up to 0.21[Formula: see text]g while the specimen with 3[Formula: see text]wt.% of alumina nanoparticle indicated the lowest weight loss about 0.02[Formula: see text]g. The worn surfaces were evaluated by scanning electron microscopy which indicated that the main wear mechanism at high temperature included adhesive wear and delamination.


2014 ◽  
Vol 15 (2) ◽  
pp. 232-241 ◽  
Author(s):  
Masafumi Kanehira ◽  
Werner J Finger ◽  
Keiichi Sasaki ◽  
Naohiko Iwasaki ◽  
Hidekazu Takahashi ◽  
...  

ABSTRACT Purpose To analyze on scanning electron microscopy (SEM) pictures from eight composite resins, taken in the centers of the initial, the middle and the terminal thirds of in vitro produced wear tracks morphological features to explain causative mechanisms for the material wear observed under two- and three-body wear. Materials and methods In vitro wear behavior of eight composite resins, three conventional and five nanofiller containing marketed products was evaluated using a custommade Zr-ball-on-disk sliding device. The composite specimens were subjected to 50,000 one-way sliding cycles (1.2 Hz, 50 N load), either simulating two-body wear with water as the intermediate medium or three-body wear using aqueous suspensions of polymethyl methacrylate (PMMA) beads and poppy seeds, respectively. Volume loss of the materials was determined in previous study. Representative specimens were selected for inspection by scanning electron microscopy at 500-fold magnification. From each of the 24 wear tracks microphotographs were taken in the central deepest parts of the initial, middle and terminal thirds of the tracks. Results For most materials morphological differences were detected depending on the location within the wear track. As a rule, the surface deterioration found increased toward the final part of the wear scar. According to common classification in tribology abrasive wear and fatigue wear, or a combination of both mechanisms were found for all materials tested. Wear was dependent both on the testing mode and on the composition of the individual composite resin material. Conclusion The morphological assessment of wear tracks reflects the nature of the abrasive and reveals insight into the mechanism generating wear patterns. Morphological details confirmed abrasive and fatigue-related wear as main failure mechanisms. Selection of food-like slurries as third-body media, such as poppy seed suspension is mandatory to simulate wear of composite restorations in occlusal cavities where three-body wear is the dominating determinant of loss of substance and surface deterioration. How to cite this article Iwasaki N, Takahashi H, Koottathape N, Kanehira M, Finger WJ, Sasaki K. Texture of Composite Resins Exposed to Two- and Three-Body Wear in vitro. J Contemp Dent Pract 2014;15(2):232-241.


2013 ◽  
Vol 423-426 ◽  
pp. 24-27
Author(s):  
Run Guo Zheng ◽  
Xin Xing Zhang

Sliding wear behavior of the (NbSe2+SiC)/Cu composite was studied on a pin-on-disc wear tester under various electrical currents and applied loads. The worn surfaces were characterized using scanning electron microscopy and energy dispersive spectroscopy to probe the wear mechanisms. Experiment results show that the friction coefficient and wear rate of (NbSe2+SiC)/Cu composite increased with increasing of the normal load. Adhesive wear, abrasive wear and fatigue wear were the main wear mechanism during the sliding process.


2007 ◽  
Vol 336-338 ◽  
pp. 1439-1441
Author(s):  
Xiao Qing Xi ◽  
Jin Long Yang ◽  
Xin Yue Zhang ◽  
Xiao Ouyang

The composite zirconium silicate microbeads with different pretreating process were developed in this paper. The wear loss of these microbeads was compared by testing of agitation mill. These microstructures with different micro-pores were compared by scanning electron microscopy. The pore size was found have obvious influences on the mechanism of the wear. Some solutions were proposed to overcome the micro-pores in the zirconium silicate composite microbeads.


2019 ◽  
Vol 141 (8) ◽  
Author(s):  
Prosanta Biswas ◽  
Manas Kumar Mondal ◽  
Durbadal Mandal

The microstructural morphology and wear behavior of as-cast Al–X wt% Mg2Si (X = 0.0, 5.0, 10.0, 15.0, and 20.0) composites were investigated through optical microscopy (OM), energy dispersive X-ray (EDX) spectrometry, scanning electron microscopy (SEM), and field emission scanning electron microscopy (FESEM). The dry sliding wear behavior was studied against an EN 31 hardened steel disk at four different applied loads (19.6 N, 29.4 N, 39.2 N, and 49 N) with a sliding speed of 62.8 m/min for 1 h. The optical microscopy analysis exhibits that the primary Mg2Si particles average equivalent diameter and volume fraction are increased with an increase in Mg2Si (Mg and Si) concentration in the Al–Mg2Si composite. Therefore, the bulk hardness of the composites is increased, whereas the primary Mg2Si hardness decreased because the coarser primary Mg2Si particles have less compactness. The wear resistance of the commercially pure aluminum significantly improved due to Mg2Si reinforcement, and the wear resistance is increased with the increase in Mg2Si concentration up to 15.0 wt% and then decreased at 20.0 wt%. The tested composites worn surfaces and debris exhibit adhesion, delamination, microcutting-abrasion, abrasive- and oxidation-type wear mechanism.


1982 ◽  
Vol 104 (1) ◽  
pp. 9-16 ◽  
Author(s):  
M. J. Murray ◽  
P. J. Mutton ◽  
J. D. Watson

Abrasive wear tests have been carried out on three steels and a number of pure metals using a pin-on-drum instrument. Each steel was tested at several different hardness levels attained by varying the heat treatment and while the results show a relationship between abrasion resistance and hardness, this was not the linear relationship found by Kruschov and others. Single point scratch experiments and scanning electron microscopy were carried out in an attempt to elucidate the wear mechanisms in these different materials and from the results a model is suggested to account for the observed wear behavior.


2013 ◽  
Vol 750-752 ◽  
pp. 701-704
Author(s):  
Run Guo Zheng ◽  
Xin Xiu Zhang

Cu-La2O3 composite was fabricated by internal oxidation method using powder metallurgy. Its sliding behavior was studied under various electrical currents and applied loads. The worn surfaces of Cu-La2O3 composite were characterized using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) to probe the wear mechanisms. The results indicated that applied load has a significant effect on the wear rate of the Cu-La2O3 composite pins. The wear rate displayed the minimum value at the load of 50N during electrical sliding processes.


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