Reliability and Properties of Ground Y-TZP-Zirconia Ceramics

2002 ◽  
Vol 81 (7) ◽  
pp. 487-491 ◽  
Author(s):  
R.G. Luthardt ◽  
M. Holzhüter ◽  
O. Sandkuhl ◽  
V. Herold ◽  
J.D. Schnapp ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Flexural Strength ◽  
High Performance ◽  
Control Sample ◽  
Surface Grinding ◽  
Weibull Parameter ◽  
Zirconia Ceramics ◽  
Inner Surface ◽  
Cad Cam ◽  
Ceramic Restorations

Yttria-stabilized zirconia ceramics is a high-performance material with excellent biocompatibility and mechanical properties, which suggest its suitability for posterior fixed partial dentures. The hypothesis under examination is that the strength and reliability of Y-TZP zirconia ceramics are affected by the inner surface grinding of crowns, and vary with the grinding parameter. Flexural strength, surface roughness, and fracture toughness were determined on samples machined by face and peripheral grinding with varied feed velocities and cutting depths. Results have been compared with those on lapped samples. Analysis of variance and Weibull parameter were used for statistical analysis. It was found that inner surface grinding significantly reduces the strength and reliability of Y-TZP zirconia compared with the lapped control sample. Co-analysis of flexural strength, Weibull parameter, and fracture toughness showed counteracting effects of surface compressive stress and grinding-introduced surface flaws. In conclusion, grinding of Y-TZP needs to be optimized to achieve the CAD/CAM manufacture of all-ceramic restorations with improved strength and reliability.

Mechanical Properties of Machinable Zirconia Dental Composites

2007 ◽  
Vol 336-338 ◽  
pp. 1587-1589
Author(s):  
Wen Xu Li ◽  
Hua Zhao ◽  
Ying Song ◽  
Bin Su ◽  
Fu Ping Wang
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Calcium Phosphate ◽  
Flexural Strength ◽  
Dental Composite ◽  
The Other ◽  
Dental Composites ◽  
Composite Ceramics ◽  
Cad Cam ◽  
The Common

Ca3(PO4)2/ZrO2 dental composite ceramics using for CAD/CAM system were prepared and the effects of weak phases on microstructures and mechanical properties were studied. The results showed that intergranular spreads happened with the increasing Ca3(PO4)2 contents due to the discontinuity of weak interfaces between Zirconia and Calcium phosphate in matrix. So the flexural strength and hardness of the Ca3(PO4)2/ZrO2 composite ceramics were decreased effectively, which improved the machinability of the composites. On the other hand, strong interfaces between Zirconias increased the integrality of the ceramic structures. ZrO2 composite Ceramics with 15% Ca3(PO4)2 were sintered at 1350°C. The flexural strength is 300.44MPa, fracture toughness is 4.36 MPam1/2, and hardness is 6.69 GPa. The cutting exponent of the Ca3(PO4)2/ZrO2 composite ceramics is obviously lower than that of the common commercial Vita Mark II and Dicor MGC ceramics, which shows good mechanical properties and machinability.

Mechanical Properties and Microstructure of PMMA-ZrO2 Nanocomposites for Dental CAD/CAM

2013 ◽  
Vol 785-786 ◽  
pp. 533-536 ◽  
Author(s):  
Shi Bao Li ◽  
Yi Min Zhao ◽  
Jian Feng Zhang ◽  
Cheng Xie ◽  
Dong Mei Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Bending Strength ◽  
In Situ Polymerization ◽  
Zirconia Ceramics ◽  
Sem Images ◽  
The Matrix ◽  
Cad Cam ◽  
Organic Resin

A novel PMMA-ZrO2 composite (PZC) was prepared by resin infiltrated to ceramic method. The composite mechanical properties were evaluated and correlated to its microstructure. Partially sintered zirconia ceramics (PSZC) were made by isostatic pressing and partially sintering. Subsequently, the PZC was prepared by vacuum infiltrating prepolymerized MMA into PSZC, followed by in-situ polymerization. When PSZC-70% was used as the matrix, the bending strength, elastic modulus, and fracture toughness of the prepared composite i.e PZC-70% were 202.56±12.09 MPa, 58.71±3.98 GPa, and 4.60±0.26 MPa·m1/2, corresponding to 25.69%, 23.31%, and 169.01% improvement, respectively, in comparison with the control matrix. Among them, the fracture toughness improvement was the most prominent. According to SEM images of the fracture surfaces, each pore of zirconia skeleton was filled by organic resin contributing to the bending strength improvement. These weak interfaces between zirconia skeleton and organic resin absorbed energy and terminated the growth of microcracks which might be responsible for significant improvement in fracture toughness. This PZC material is anticipated to be a new member of the dental CAD/CAM family.

scholarly journals Effects of Different Air Particle Abrasion Protocols on the Biaxial Flexural Strength and Fractography of High/Ultra-Translucent Zirconia

Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 244
Author(s):  
Reem AlMutairi ◽  
Hend AlNahedh ◽  
Ahmed Maawadh ◽  
Ahmed Elhejazi
Keyword(s):  
Standard Deviation ◽  
Flexural Strength ◽  
Control Sample ◽  
Zirconia Ceramic ◽  
Air Abrasion ◽  
Zirconia Ceramics ◽  
Biaxial Flexural Strength ◽  
Monolithic Zirconia ◽  
The Mean ◽  
Post Hoc

In this study, the biaxial flexural strength (BFS) and fractography of high/ultra-translucent monolithic zirconia ceramics subjected to different mechanical surface pretreatments were evaluated. A total of 108 disc-shaped samples (12 mm diameter, 1.2 mm thickness) of three zirconia materials (5Y-ZP KATANA Zirconia UTML (ML), 3Y-TZP DD Bio ZX2 (DB), and 5Y-ZP DD cube X2 (DC)) were used. The BFS was investigated after subjecting the samples to surface treatment using air abrasion particles of two types (aluminum oxide or glass microbeads). The data were analyzed using two-way analysis of variance, followed by Scheffe’s post hoc test for multiple comparisons. The mean ± standard deviation BFS for DB was highest after treatment with 50 µm Al2O3 (1626.05 ± 31.9 MPa), with lower values being observed following treatment with 50 µm glass microbeads (1399.53 ± 24.2 MPa) and in the control sample (1198.51 ± 21.1 MPa). The mean ± standard deviation (SD) BFSs for DC and ML were the highest in the control groups. Surface air abrasion with 50 µm Al2O3 particles and 2 bar pressure is recommended for 3Y-TZP translucent zirconia, while no abrasion of 5Y-ZP translucent zirconia ceramic.

scholarly journals Effect of Pressure and Particle Size During Aluminum Oxide Air Abrasion on the Flexural Strength of Disperse-Filled Composite and Polymer-Infiltrated Ceramic Network Materials

Polymers ◽  
2020 ◽  
Vol 12 (6) ◽  
pp. 1396
Author(s):  
Jong-Eun Kim ◽  
Jung-Hwa Lim ◽  
You-Jung Kang ◽  
Jee-Hwan Kim ◽  
June-Sung Shim
Keyword(s):  
Particle Size ◽  
Flexural Strength ◽  
Surface Treatment ◽  
Computer Aided Design ◽  
High Performance ◽  
High Pressures ◽  
Defect Formation ◽  
Air Abrasion ◽  
Computer Aided ◽  
Cad Cam

Esthetic dental computer-aided design/computer-aided manufacturing (CAD/CAM) polymers such as disperse-filled composites (DFC) and polymer-infiltrated ceramic networks (PICN) should be subjected to surface treatment before bonding. However, such treatment can lead to defect formation and a decrease in strength. Therefore, in this study, we compared the flexural strengths of DFC and PICN materials air-abraded with alumina particles of different sizes at different pressures. In addition to Weibull analysis, the samples (untreated and treated) were characterized by scanning electron microscopy and atomic force microscopy. Both DFC and PICN exhibited the lowest flexural strength at large particle sizes and high pressures. Therefore, we optimized the air abrasion parameters to maintain the flexural strength and significantly increase surface roughness. In the case of DFC, the optimal particle size and pressure conditions were 50 µm at 2 bar and 110 µm at 1 bar, while for PICN, the best performance was obtained using Al2O3 particles with a size of 50 µm at 1 bar. This study reveals that optimization of the surface treatment process is crucial in the fabrication of high-performance clinical materials for dental restorations.

scholarly journals Saliva Influence on the Mechanical Properties of Advanced CAD/CAM Composites for Indirect Dental Restorations

Polymers ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 808
Author(s):  
Teresa Palacios ◽  
Sandra Tarancón ◽  
Cristian Abad ◽  
José Ygnacio Pastor
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Elastic Modulus ◽  
Flexural Strength ◽  
Mechanical Performance ◽  
Artificial Saliva ◽  
Fluorescence Analysis ◽  
Dental Restoration ◽  
Global Approximation ◽  
Cad Cam

This study aims to evaluate the microstructural and mechanical properties of three commercial resin-based materials available for computer-aid design and manufacturing (CAD/CAM)-processed indirect dental restoration: LavaTM Ultimate Restorative (LU), 3M ESPE; Brilliant Crios (BC), COLTENE and CerasmartTM (CS), GC Dental Product. The three types of resin-based composite CAD/CAM materials were physically and mechanically tested under two conditions: directly as received by the manufacturer (AR) and after storage under immersion in artificial saliva (AS) for 30 days. A global approximation to microstructure and mechanical behaviour was evaluated: density, hardness and nanohardness, nanoelastic modulus, flexural strength, fracture toughness, fracture surfaces, and microstructures and fractography. Moreover, their structural and chemical composition using X-ray fluorescence analysis (XRF) and field emission scanning electron microscopy (FESEM) were investigated. As a result, LU exhibited slightly higher mechanical properties, while the decrease of its mechanical performance after immersion in AS was doubled compared to BC and CS. Tests of pristine material showed 13 GPa elastic modulus, 150 MPa flexural strength, 1.0 MPa·m1/2 fracture toughness, and 1.0 GPa hardness for LU, 11.4 GPa elastic modulus; 140 MPa flexural strength, 1.1 MPa·m1/2 fracture toughness, and 0.8 GPa hardness for BC; and 8.3 GPa elastic modulus, 140 MPa flexural strength, 0.9 MPa·m1/2 fracture toughness, and 0.7 GPa hardness for CS. These values were significantly reduced after one month of immersion in saliva. The interpretation of the mechanical results could suggest, in general, a better behaviour of LU compared with the other two despite it having the coarsest microstructure of the three studied materials. The saliva effect in the three materials was critically relevant for clinical use and must be considered when choosing the best solution for the restoration to be used.

Mechanical Properties and Microstructure of Partially Sintered Zirconia Ceramics

2008 ◽  
Vol 368-372 ◽  
pp. 1252-1254 ◽  
Author(s):  
Shi Bao Li ◽  
Zhao Hui Chen ◽  
Yi Min Zhao ◽  
Zhong Yi Wang ◽  
Li Hui Tang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Grain Size ◽  
Bending Strength ◽  
Target Material ◽  
Dental Restoration ◽  
Diameter Distribution ◽  
Zirconia Ceramics ◽  
Grain Sizes ◽  
Cad Cam

Partially sintered zirconia ceramics (PSZCs) for dental uses were prepared from zirconia nanopowder via isostatic pressing and partially sintering. The open porosities, pore diameters, grain sizes and mechanical properties of the ceramics with different densities were studied. The results show that the pores formed in the PSZCs are all open pores, with a diameter distribution of 60nm~130nm and a grain size distribution of 120~170nm. The machinability becomes worse when the density of PSZC is higher than 75% of the theoretical density, so a ceramic named PSZC-70% with density of 70%TD was selected as the target material. Its bending strength is 168 MPa and fracture toughness is 1.8 MPa·m1/2. A dental restoration framework can be obtained via machining the PSZC-70% on a dental CAD/CAM system.

Effect of in vitro aging on the flexural strength and probability to fracture of Y-TZP zirconia ceramics for all-ceramic restorations

2014 ◽  
Vol 30 (12) ◽  
pp. e306-e316 ◽  
Author(s):  
Eleni Siarampi ◽  
Eleana Kontonasaki ◽  
Konstantinos S. Andrikopoulos ◽  
Nikolaos Kantiranis ◽  
George A. Voyiatzis ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Zirconia Ceramics ◽  
In Vitro Aging ◽  
All Ceramic ◽  
Ceramic Restorations

ARMCO PH 13-8Mo

Alloy Digest ◽  
1990 ◽  
Vol 39 (2) ◽  
Keyword(s):  
Fracture Toughness ◽  
Corrosion Resistance ◽  
High Temperature ◽  
Physical Properties ◽  
Stress Corrosion ◽  
Tensile Properties ◽  
High Performance ◽  
High Strength ◽  
Heat Treating ◽  
Temperature Performance

Abstract ARMCO PH 13-8Mo is designed for high-performance applications requiring high strength coupled with excellent resistance to corrosion and stress corrosion. It has excellent toughness, good transverse properties and excellent forgeability. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness. It also includes information on low and high temperature performance, and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: SS-224. Producer or source: Baltimore Specialty Steels Corporation. Originally published May 1969, revised February 1990.

BETHLEHEM LUKENS PLATE HPS-70W

Alloy Digest ◽  
2000 ◽  
Vol 49 (12) ◽  
Keyword(s):  
Fracture Toughness ◽  
Corrosion Resistance ◽  
Tensile Properties ◽  
High Performance ◽  
Iron And Steel ◽  
Cooperative Agreement ◽  
Federal Highway ◽  
High Performance Steel ◽  
Department Of The Navy ◽  
Steel Institute

Abstract BETHLEHEM LUKENS PLATE HPS-70W is a high-performance steel (HPS) developed through a cooperative agreement among the Federal Highway Administration (FHWA), the American Iron and Steel Institute (AISI), and the Department of the Navy. This steel is an improved version of ASTM A 709 grade 70W. This datasheet provides information on composition and tensile properties as well as fracture toughness. It also includes information on corrosion resistance as well as forming and joining. Filing Code: SA-506. Producer or source: Bethlehem Lukens Plate.

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