scholarly journals RESEARCH OF STRAW PYROLYSIS THERMAL EFFECTS FOR ESTIMATION OF POSSIBILITY ITS IMPLEMENTA-TION IN AUTOTHERMAL MODE

2019 ◽  
pp. 271-280 ◽  
Author(s):  
Aleksandr Vladimirovich Astafev ◽  
Roman Borisovich Tabakaev ◽  
Dias Erlanovich Musafirov ◽  
Aleksandr Sergeyevich Zavorin ◽  
Yuriy Vladimirovich Dubinin ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Thermal Effect ◽  
Thermal Effects ◽  
Raw Materials ◽  
Laser Flash ◽  
Raw Material ◽  
Exothermic Reactions ◽  
Calculation Results

The aim of the work is research of straw pyrolysis in various modes, the determination of process thermal effects and estimation of straw thermal processing possibility in the autothermal mode. Physical experiment and differential thermal analysis were used as research methods. Thermotechnical characteristics of raw materials are determined by ISO 1171:2010, GOST R 55660-2013 and a bomb calorimeter; thermal and physical characteristic are determined by the analyzer of thermal diffusivity Discovery Laser Flash DLF-1200. In result of the work is established that thermal effects occur in the straw after heating to 200 °C. The first shows of exothermic reactions are observed when the reactor is heated to 303 °C – in this case the temperature of the straw reaches 308.8 °C. By differential thermal analysis is established that the temperature range of heat input was set from 235 to 575 °C and value of the thermal effect in this range was set 1475 kJ/kg. For this range, the heat costs for the organization of pyrolysis in the autothermal mode and the total thermal effect of the process are calculated. The calculation results showed that the maximum thermal effect (398.9 kJ/kg) can be obtained at a pyrolysis temperature of 460 °C. For these conditions, the influence of the initial straw moisture content on the autothermality of pyrolysis process was evaluated and it was established that process can be organized due to its own thermal effects when the raw material moisture is less than 30.5%.

PHASE EQUILIBRIUM IN THE AS2TE3-TM2TE3 SYSTEM.

2020 ◽  
Vol 5 (8(77)) ◽  
pp. 65-68
Author(s):  
Teymur Mammad Ilyasly ◽  
Rahman Hasanaga Fatullazade ◽  
Zakir Islam Ismailov ◽  
Nigar Nadir Jafarova
Keyword(s):  
Thermal Analysis ◽  
Solid Solution ◽  
Differential Thermal Analysis ◽  
Phase Equilibrium ◽  
Physicochemical Properties ◽  
Thermal Effects ◽  
Isothermal Annealing ◽  
Intermediate Phase ◽  
Physicochemical Analysis ◽  
Two Phases

The synthesis of alloys of the system was carried out stepwise in rotary furnaces. The synthesis mode was selected based on the physicochemical properties of the elementary components. For homogenization, the alloys were subjected to isothermal annealing at 750 and 1275 K, depending on the Tm2Te3 concentration, for 250 h after homogenization of the alloys, they were subjected to physicochemical analysis. The results of differential thermal analysis showed that reversible thermal effects are observed in the alloys of the system. In alloys in a 1: 1 ratio, a new intermediate phase is formed with a composition corresponding to the TmAsTe3 compound. The homogeneity area is observed in the concentration range 52.5-47.5. It was found that in the concentration range 98.5-52.5 Tm2Te3 there are two phases - a mixture of β and of the solid solution, and in the concentration range of 47.51 mol% Tm2Te3 phases and α are in equilibrium. ) 66 The eutectic has coordinates of 11.5 mol Tm2Te3 at a temperature of 575 K.

Liquid Chromatographic Determination of Amiodarone Hydrochloride and Related Compounds in Raw Materials and Tablets

1994 ◽  
Vol 77 (6) ◽  
pp. 1447-1453 ◽  
Author(s):  
Pauline M Lacrok ◽  
Norman M Curran ◽  
Wing-Wah Sy ◽  
Dennis K J Goreck ◽  
Pierre Thibault ◽  
...  
Keyword(s):  
Raw Materials ◽  
Chromatographic Determination ◽  
Raw Material ◽  
Liquid Chromatographic Method ◽  
Limit Of Quantitation ◽  
Liquid Chromatographic Determination ◽  
Liquid Chromatographic ◽  
Amiodarone Hydrochloride ◽  
Related Compounds

Abstract A liquid chromatographic method for the determination of amiodarone hydrochloride and 10 related compounds in drug raw material and for assay of drug in tablets was developed. The method specifies a 3 jxm Hypersil nitrile column (150 × 4.6 mm), a mobile phase of 1 + 1 acetonitrile–ammonium acetate buffer (0.1 M adjusted to pH 6.0 with 0.1 M acetic acid), a flow rate of 1 mL/min, and detection at 240 nm. The lower limit of quantitation of the related compounds is 0.02% or less. Drug contents in 2 raw material samples were 100.1 and 99.9% and ranged from 98.2 to 99.4% in 3 tablet formulations. Impurity levels in 2 samples of raw material from different manufacturers were ca 0.4%. The presence of 3 of the known related compounds in these samples was confirmed by liquid chromatographymass spectrometry. The method applied to raw materials was evaluated by a second laboratory and found to be satisfactory.

The Roman Ceramics of Salobrena (Granada-Spain) and their Raw Materials

1992 ◽  
Vol 267 ◽  
Author(s):  
Ana M De Andres ◽  
Isabel MuÑOZ
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Raw Materials ◽  
Third Century ◽  
Western Coast ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Third ◽  
Good Number ◽  
Scanning Electron

ABSTRACTNineteen roman ceramic sherds found near Salobreña (Granada, Spain), in the western coast of the Mediterranean Sea, as well as different ceramic clays from the surroundingsare studied. Both clays and ceramic sherds are characterizad by X-ray diffraction and spectrometry, differential thermal analysis, and scanning electron and optical microscopies. A good number of the ceramic pieces, among which some “Terrae Sigillatae”, have a composition similar to that of the local clays and, thus, have been probably manufactured at Salobreña. Only a few of them have a foreign origin. For most of them, the firing temperature was about 800-850 °C, although some have been produced at 900-1000 °C, and some others at 1000-1100 °C. It is concluded that Salobreña appearsto have been an important settlement just in the third century of the Christian era.

Preparation of Glass-Ceramics Using Molybdenum Tailings

2011 ◽  
Vol 284-286 ◽  
pp. 1431-1434 ◽  
Author(s):  
Jin Rui Zhang ◽  
Ru Wang
Keyword(s):  
Heat Treatment ◽  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Crystalline Phase ◽  
Glass Ceramics ◽  
Chemical Properties ◽  
The Other ◽  
Raw Material ◽  
Physical Chemical ◽  
Nucleation Agents

In order to utilization the molybdenum tailings which be deposited in large quantities. Test used it to prepare glass-ceramics as main raw material, TiO2 as nucleation agents and CaO-Al2O3-SiO2 system and wollastonite as the principal crystalline phase. Heat treatment system of glass-ceramics was based on the differential thermal analysis. The crystalline phase, microstructure and characteristics of glass-ceramics were analysis by XRD, SEM and physical, chemical properties test. The result shows that the performance of glass-ceramics was superior to the other types of building decoration stone.

scholarly journals Penerapan metode fuzzy sugeno untuk prediksi persediaan bahan baku

2019 ◽  
Vol 9 (2) ◽  
pp. 12-20
Author(s):  
Julio Warmansyah ◽  
Dida Hilpiah
Keyword(s):  
Fuzzy Logic ◽  
Raw Materials ◽  
Mean Absolute Percentage Error ◽  
Raw Material ◽  
Percentage Error ◽  
Human Power ◽  
Absolute Percentage Error ◽  
Input Variables ◽  
A Company

 PT. Cahaya Boxindo Prasetya is a company engaged in the manufacture of carton boxes or boxes. The company's activities also include cutting and printing services using machinery and human power. The problem faced in this company is the difficulty of predicting the amount of inventory of raw materials that will be  included in the production. The remaining raw materials for production will be used as the final stock to get the minimum, the goal is to reduce excess stock Overcoming this problem, fuzzy logic is used to predict raw material inventories by focusing on the final stock. In this study using Fuzzy Sugeno, with three input variables, namely: initial inventory, purchase, production, while the output is the final stock. Determination of prediction results using defuzzification using the average concept of MAPE (Mean Absolute Percentage Error). The results obtained, using the Fuzzy Sugeno method can predict the inventory of raw materials with a MAPE value of 38%. 

scholarly journals PERENCANAAN BAHAN BAKU DAN HASIL PRODUKSI MENGGUNAKAN METODE LINIER PROGRAMMING SIMPLEK

2017 ◽  
Vol 12 (2) ◽  
Author(s):  
Monika Handayani ◽  
Eka Kusuma Dewi
Keyword(s):  
Linear Programming ◽  
Production Planning ◽  
Simplex Method ◽  
Raw Materials ◽  
Raw Material ◽  
Planning System ◽  
Testing System ◽  
Basic Solution ◽  
Linear Programming Method

<p>CV. Baja Utama Landasan Ulin is a business entity that manufactures various products using the basic ingredients of iron. In the management of raw materials for the production of common regulatory process raw materials into sections for further processing. This setting is often done manually without doing careful planning, so that at the end of each production process there are many remaining pieces of the raw materials that should be used in production. In addition to the determination of the production is necessary to reference how the product should be made for each type of existing products. This is often an important factor that pushed for the optimization of production planning in determining the number of products for each type of product and raw material consumption.Linear Programming is one of the methods used in production planning to regulate the use of raw materials is limited. Simplex method is part of the linear programming method that can be used in the production planning system implementation. Simplex method identifies an initial basic solution and then move systematically to other basic solution that has the potential to improve the value of the objective function.The calculation result of production planning using the simplex method can be used as a reference in the decision making production planning. By building an application using the simplex method can assist in the calculation of production peencanaan more efficiently and effectively. Accuracy testing system constructed show significant results with great value reached 94% level of accuracy.<br />Keywords: simplex, production planning, the maximum gain, linear programming</p>

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