scholarly journals Effect of heat treatment on the tensile properties of incrementally processed modified polylactide

Polimery ◽  
2021 ◽  
Vol 66 (6) ◽  
pp. 357-361
Author(s):  
Bogdan Kozik ◽  
Mariusz Dębski ◽  
Piotr Bąk ◽  
Małgorzata Gontarz ◽  
Małgorzata Zaborniak

The article presents the results of strength tests in the form of a static tensile test on the INSTRON 5967 testing machine. Samples were made with the use of the Prusa i3 MK3 3D printer, by modeling with a plasticized material (FFF) made of ABS copolymer, polylactide and its modified variant. According to the information provided by the manufacturer, heat-treated modified polylactide has mechanical properties similar to ABS copolymer filament. The publication also discusses the method of manufacturing elements subjected to the tests, the heat treatment process, as well as changes in material properties as a result of this treatment. Based on the test results, it was found that the annealing process increased the proportion of the crystalline phase, which significantly improved the strength properties of the modified polylactide.

2018 ◽  
Vol 204 ◽  
pp. 05020
Author(s):  
Aminnudin Aminnudin ◽  
Moch. Agus Choiron

Metal matrix composite (MMC) is a combination of two or more materials using metal as a matrix. In this paper we used brass as the matrix and fly ash as for the particle. The fly ash used is fly ash which is produced from coal combustion in the Paiton power plant. Fly ash composition in the MMC are 5% and 10%. The MMC was produced with gas furnace. Heat tratment to MMC was done at 350 and 400 °C.Hard testing process, tensile test and impack test are carried out at MMC before heat treatment and after heat treatment. From the test results showed an increase in hardness, tensile strength and impact test showed the heat treatment process at a temperature of 350 °C. Heat treatment at a temperature of 400 °C does not improve the mechanical properties of MMC


2005 ◽  
Vol 495-497 ◽  
pp. 907-912 ◽  
Author(s):  
Suk Hoon Kang ◽  
Hee Suk Jung ◽  
Woong Ho Bang ◽  
Jae Hyung Cho ◽  
Kyu Hwan Oh ◽  
...  

This paper studies the microstructure of drawn gold wires to equivalent strain of 10 and to equivalent strain of 8.5 then heat-treated. The texture of gold wire drawn to strain of 10 is mainly composed of <100> and <111> fibers. Tensile strength of the gold wire increases with <111> fiber fraction, while the grain size does not appear to affect the tensile property. With an exception at heat treatment at 600oC, the texture of gold wire drawn the strain of 8.5 is replaced with <100> fiber component by heat treatment process at 400~700oC. Heat treatment at 600oC produces <110> fiber or <112> fiber, depending upon annealing time.


2016 ◽  
Vol 61 (1) ◽  
pp. 405-410
Author(s):  
M. Bigaj ◽  
S. Boczkal ◽  
J. Żelechowski ◽  
M. Gawlik ◽  
M. Mitka

The results of studies carried out on the heat treated AZ61 magnesium alloy extruded by two methods, i.e. direct extrusion and continuous rotary extrusion, were presented. As part of the work, parameters of the T6 heat treatment were proposed and aging curves were plotted. The solution heat treatment process was accompanied by the grain growth. During artificial aging, due to the decomposition of solid solution, the β-Mg17Al12 phase was precipitated from the supersaturated α solution. It precipitated in a coagulated form at the grain boundaries and in the form of fine-dispersed plates arranged in a preferred direction relative to the grain orientation. Rods obtained by continuous rotary extrusion, unlike those made by the direct process, exhibited a low degree of texturing and lack of anisotropic properties.


2014 ◽  
Vol 59 (4) ◽  
pp. 1637-1640 ◽  
Author(s):  
J. Dworecka ◽  
E. Jezierska ◽  
K. Rozniatowski ◽  
W. Swiatnicki

Abstract The aim of the work was to produce a nanobainitic structure in the commercial bearing steel - 100CrMnSi6-4 and to characterize its structure and mechanical properties. In order to produce this structure the austempering heat treatment was performed, with parameters that have been selected on the basis of dilatometric measurements of phase transformation kinetics in steel. The heat treatment process was performed in laboratory as well as in industrial furnaces. The obtained structure was characterized using transmission electron microscopy. In order to investigate the effect of the microstructure parameters on the material’s mechanical properties, the hardness, impact strength and static tensile tests have been conducted.


2017 ◽  
Vol 898 ◽  
pp. 1705-1711 ◽  
Author(s):  
Jun Zhe Li ◽  
Xun Sun ◽  
Hai Tao Liu ◽  
Hai Feng Cheng ◽  
Xiao Shan Zhang

The composition and microstructure of silicon nitride fibers after heat-treatment at elevated temperatures were investigated by XRD, NMR, XPS, SEM and TEM analyses. The results show that as-received fibers consisted of amorphous silicon nitride, and a little Si-C-O structure. During heat-treatment process, α-Si3N4 and β-Si3N4 formed resulting from the crystallization of amorphous silicon nitride, and the formation of β-SiC derived from the decomposition of Si-C-O structure. As heat-treated temperature increased from 1400oC to 1600oC, the above phenomenon become obvious, indicating that the fiber would possess high serving life with serving temperature lower than 1400oC. The tensile strength of fibers stays stable when heat-treated temperature was below 1200oC, while the strength retention of fibers sharply decreased to 50% after heat-treatment at 1400°C.


2017 ◽  
Vol 904 ◽  
pp. 15-18
Author(s):  
Bo Bo Meng ◽  
Quan An Li ◽  
Xiao Ya Chen

The effects of heat treatment on microstructure and mechanical properties of Mg-9Gd-4Y-0.5Zr alloy were studied by XRD, OM, SEM and tensile testing machine. The results show that the alloy mainly consists of α-Mg matrix, Mg5Gd and Mg24Y5. Through solid solution and aging heat treatment process, the tensile strength, yield strength and elongation rate respectively achieves 263.1MPa, 235.2MPa and 3.11%.


2018 ◽  
Vol 284 ◽  
pp. 1101-1106
Author(s):  
Irina V. Starostina

The iron ore raw materials refinement waste is not virtually used after the wet magnetic separation and is accumulated in special hydraulic constructions – tailing dumps. This work considers the opportunity of using the heat-treated tailings as loading pigments for through-dyed autoclaved silicate concretes production. The heat-treated tailings were added to the raw mix instead of quartz sand. The concrete samples of light-pink shades of color were obtained. It has been demonstrated that the activation processes, taking place at heat treatment of tailings, as well as the influence of iron oxides acting as a mineralizer at high temperatures, create the increased imperfection of the quartz component’s structure. This increases the synthesis rate of new formations – the low-basic calcium silicate hydrates – and increases the strength properties of the samples with optimal compositions by 70-75% as compared to the control sample.


2012 ◽  
Vol 624 ◽  
pp. 208-211
Author(s):  
Hua Tang ◽  
Yu Tian Wang ◽  
Wei Jun Zhang ◽  
Li Shen ◽  
Yun Biao Duan ◽  
...  

Abstract: The lithium orthosilicate pebbles was fabricated by melt spraying method with lithium carbonate (Li2CO3) and silicon dioxide (SiO2). By alter heat treatment temperature to study different particle sizes of lithium orthosilicate pebbles of strength and phase. Lithium orthosilicate pebbles which were heat treated by vacuum tube type furnace study change of phase ,by XRD to study the change of phase after the heat treatment and tested strength by universal testing machine. Heat treatment would alter strength and phase by vacuum tube type furnace.


2008 ◽  
Vol 55-57 ◽  
pp. 245-248 ◽  
Author(s):  
Nattiree Chiranavanit ◽  
Anak Khantachawana ◽  
N. Anuwongnukroh ◽  
Surachai Dechkunakorn

Ni-Ti alloy wires have been widely used in clinical orthodontics because of their properties of superelasticity (SE) and shape memory effect (SME). The purpose of this study was to assess the mechanical properties and phase transformation of 50.7Ni-49.3 Ti (at%) alloy (NT) and 45.2Ni-49.8Ti-5.0Cu (at%) alloy (NTC), cold-rolled with various percent reductions. To investigate SE and SME, heat-treatment was performed at 400°C and 600°C for 1 h. The specimens were examined using an Energy-Dispersive X-ray Spectroscope (EDS), Differential Scanning Calorimeter (DSC), Universal Testing Machine (Instron), Vickers Hardness Tester and Optical Microscope (OM). On the three-point bending test, the superelastic load-deflection curve was seen in NTC heat-treated at 400°C. Furthermore, NT heat-treated at 400°C with 30% reduction produced a partial superelastic curve. For SME, no conditions revealed superelasticity at the oral temperature. Micro-hardness value increased with greater percentage reduction. The average grain size for all specimens was typically 55-80 µm. The results showed that locally-made Ni-Ti alloys have various transformation behaviors and mechanical properties depending on three principal factors: chemical composition, work-hardening (the percent reduction) and heat-treatment temperature.


2014 ◽  
Vol 1061-1062 ◽  
pp. 454-459
Author(s):  
An Min Li ◽  
Ding Ma ◽  
Qi Feng Zheng ◽  
Ruo Huai Chen ◽  
Qiang Li ◽  
...  

The as-cast grate bar structure used in sintering trolley is primarily comprised of austenite and eutectic (eutectic austenite and eutectic carbide).The austenite is dendrite, while the carbides are reticular and chrysanthemum-like. The failed grate bar structure primarily consists of ferrite, carbide, martensite and residual austenite; cavity shrinkage and shrinkage porosity exist in the structure, and the fracture exhibits typical cleavage fracture characteristics. The primary means of failure are abrasion and fracture. The secondary carbides precipitated in the sample (quenching (1050°C+2.5h)+ tempering (390°C+2.5h)) and the other one (quenching (1050°C+2.5h)+ tempering (420°C+2.5h) ) are dispersed and refined. Compared with the as-cast one, their relative abrasion resistance performances respectively are 0.8645 and 0.8752.The values of hardness and impact toughness of the samples heat-treated are greater than those of the as-cast grate bar. The optimum heat treatment process is as follows: quenching (1050°C,2.5h) + tempering (390°C~420°C,2.5h)


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