scholarly journals Fused deposition modeling of polypropylene-aluminium silicate dihydrate microcomposites

e-Polymers ◽  
2022 ◽  
Vol 22 (1) ◽  
pp. 87-98
Author(s):  
Kilole Tesfaye Chaka

Abstract Polypropylene (PP) undergoes fast crystallization and resulting in rigorous shrinkage when it is subjected to high temperature likewise of the fused deposition modeling (FDM) process. This research study focuses on the investigation of the processing parameters and factors that decrease the warpage of PP during the FDM process. Aluminium silicate dihydrate (K) microparticles of different ratios were melt blended with PP by a twin-screw extruder, and filaments of about 1.7 mm diameter were extruded in a single screw extruder. Then, the extruded filaments were used to fabricate the dumbbells structure through the FDM process. The effects of optimizing the fused deposition temperature, coating the chamber with thick papers/fabrics, and coating a printer bed with PP material were also investigated in this study. Scanning and transmission electron microscopy, differential scanning calorimetry, melt flow, and mechanical properties testing instruments are used to analyze the microparticles dispersion, crystallization, flow, and mechanical properties of resulting samples. Uniformly dispersed filler and increased printing chamber temperature result in an increase of crystallization temperature and improve the dimensional accuracy of fused deposited specimens. The fused deposited PP-K10 wt% composite showed an improvement of up to 32% in tensile modulus compared to the neat PP.

2021 ◽  
pp. 089270572110530
Author(s):  
Nagarjuna Maguluri ◽  
Gamini Suresh ◽  
K Venkata Rao

Fused deposition modeling (FDM) is a fast-expanding additive manufacturing technique for fabricating various polymer components in engineering and medical applications. The mechanical properties of components printed with the FDM method are influenced by several process parameters. In the current work, the influence of nozzle temperature, infill density, and printing speed on the tensile properties of specimens printed using polylactic acid (PLA) filament was investigated. With an objective to achieve better tensile properties including elastic modulus, tensile strength, and fracture strain; Taguchi L8 array has been used for framing experimental runs, and eight experiments were conducted. The results demonstrate that the nozzle temperature significantly influences the tensile properties of the FDM printed PLA products followed by infill density. The optimum processing parameters were determined for the FDM printed PLA material at a nozzle temperature of 220°C, infill density of 100%, and printing speed of 20 mm/s.


Author(s):  
Jiaqi Lyu ◽  
Souran Manoochehri

The dimensional accuracy of fused deposition modeling (FDM) machines is dependent on errors caused by processing parameters and machine motions. In this study, an integrated error model combining these effects is developed. Extruder temperature, layer thickness, and infill density are selected as parameters of this study for three FDM machines, namely, Flashforge Finder, Ultimaker 2 go, and XYZ da Vinci 2.0 Duo. Experiments have been conducted using Taguchi method and the interactions between processing parameters are analyzed. Based on the dimensional deviations between fabricated parts and the computer aided design (CAD) geometry, a set of coefficients for the integrated error model are calculated to characterize each machine. Based on the results of the integrated error model, the original CAD geometry is optimized for fabrication accuracy on each machine. New parts are fabricated using the optimized CAD geometries. Through comparing the dimensional deviations of parts fabricated before and after optimization, the effectiveness of the integrated error model is analyzed and demonstrated for the three FDM machines.


Polymers ◽  
2019 ◽  
Vol 11 (7) ◽  
pp. 1094 ◽  
Author(s):  
Valentina Mazzanti ◽  
Lorenzo Malagutti ◽  
Francesco Mollica

As biodegradable thermoplastics are more and more penetrating the market of filaments for fused deposition modeling (FDM) 3D printing, fillers in the form of natural fibers are convenient: They have the clear advantage of reducing cost, yet retaining the filament biodegradability characteristics. In plastics that are processed through standard techniques (e.g., extrusion or injection molding), natural fibers have a mild reinforcing function, improving stiffness and strength, it is thus interesting to evaluate whether the same holds true also in the case of FDM produced components. The results analyzed in this review show that the mechanical properties of the most common materials, i.e., acrylonitrile-butadiene-styrene (ABS) and PLA, do not benefit from biofillers, while other less widely used polymers, such as the polyolefins, are found to become more performant. Much research has been devoted to studying the effect of additive formulation and processing parameters on the mechanical properties of biofilled 3D printed specimens. The results look promising due to the relevant number of articles published in this field in the last few years. This notwithstanding, not all aspects have been explored and more could potentially be obtained through modifications of the usual FDM techniques and the devices that have been used so far.


2018 ◽  
Vol 33 (5) ◽  
pp. 581-598 ◽  
Author(s):  
Piyush Bedi ◽  
Rupinder Singh ◽  
IPS Ahuja

In this work, multifactor optimization of fused deposition modeling (FDM) process parameters has been reported for in-house prepared feedstock filament comprising of SiC/Al2O3 reinforced in recycled low-density polyethylene (LDPE) matrix with different particle sizes (i.e. single particle size (SPS), double particle size (DPS), and triple particle size (TPS) in different proportions). This study has been conducted on Al2O3-based DPS reinforcement in LDPE, which came out as a better solution during pilot experimentation in comparison to SPS, TPS, and SiC reinforcement, for printing of functional prototypes as rapid tooling (RT). The result of study suggests that infill angle in the FDM process is the most significant process parameter (contributing around 93%) for preparation of RT as regards dimensional accuracy and hardness is concerned. The RT so prepared is thermally stable as evident from differential scanning calorimetry analysis. Further, the photomicrographs observed in different planes suggest that, at the proposed settings, RT has a uniform distribution of reinforcement in LDPE matrix and can be gainfully used in light machining applications.


2021 ◽  
pp. 095400832110036
Author(s):  
Bin Hu ◽  
Zehua Xing ◽  
Weidong Wu ◽  
Xiaojun Zhang ◽  
Huamin Zhou ◽  
...  

Short-carbon-fiber (SCF)–reinforced poly-ether-ether-ketone (PEEK) is a promising polymer composite material with good biocompatibility, a high strength-to-weight ratio, and low friction properties. In artificial-bone fabrication and other applications with more flexible fabrication demands, fused-deposition modeling (FDM) technology enables the rapid and low-cost fabrication of SCF/PEEK parts with sophisticated structures. Owing to the high viscosity of melting PEEK composites, great challenges, associated with the poor internal interface, need to be overcome before enhanced mechanical properties can be obtained. In this study, key processing parameters and various SCF amounts were studied to investigate their effects on the mechanical properties of PEEK composites. It was revealed that the existence of voids and gaps between the SCF and PEEK led to a decrease in the strength of the composite systems. The FDM processing parameters were tuned to eliminate these defects in the PEEK composites. The tensile strength of the 2% SCF/PEEK sample reached 96.4 MPa, which is comparable to that of PEEK parts prepared by injection molding. Meanwhile, its elastic modulus reached 2.6 GPa, which is 169% higher than that of the bare PEEK sample.


2021 ◽  
pp. 002199832098856
Author(s):  
Marcela Piassi Bernardo ◽  
Bruna Cristina Rodrigues da Silva ◽  
Luiz Henrique Capparelli Mattoso

Injured bone tissues can be healed with scaffolds, which could be manufactured using the fused deposition modeling (FDM) strategy. Poly(lactic acid) (PLA) is one of the most biocompatible polymers suitable for FDM, while hydroxyapatite (HA) could improve the bioactivity of scaffold due to its chemical composition. Therefore, the combination of PLA/HA can create composite filaments adequate for FDM and with high osteoconductive and osteointegration potentials. In this work, we proposed a different approache to improve the potential bioactivity of 3D printed scaffolds for bone tissue engineering by increasing the HA loading (20-30%) in the PLA composite filaments. Two routes were investigated regarding the use of solvents in the filament production. To assess the suitability of the FDM-3D printing process, and the influence of the HA content on the polymer matrix, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) and scanning electron microscopy (SEM) were performed. The HA phase content of the composite filaments agreed with the initial composite proportions. The wettability of the 3D printed scaffolds was also increased. It was shown a greener route for obtaining composite filaments that generate scaffolds with properties similar to those obtained by the solvent casting, with high HA content and great potential to be used as a bone graft.


2017 ◽  
Vol 23 (4) ◽  
pp. 804-810 ◽  
Author(s):  
Shiqing Cao ◽  
Dandan Yu ◽  
Weilan Xue ◽  
Zuoxiang Zeng ◽  
Wanyu Zhu

Purpose The purpose of this paper is to prepare a new modified polybutylene terephalate (MPBT) for fused deposition modeling (FDM) to increase the variety of materials compatible with printing. And the printing materials can be used to print components with a complex structure and functional mechanical parts. Design/methodology/approach The MPBT, poly(butylene terephalate-co-isophthalate-co-sebacate) (PBTIS), was prepared for FDM by direct esterification and subsequent polycondensation using terephthalic acid (PTA), isophthalic acid (PIA), sebacic acid (SA) and 1,4-butanediol (BDO). The effects of the content of PIA (20-40 mol%) on the mechanical properties of PBTIS were investigated when the mole per cent of SA (αSA) is zero. The effects of αSA (0-7mol%) on the thermal, rheological and mechanical properties of PBTIS were investigated at nPTA/nPIA = 7/3. A desktop wire drawing and extruding machine was used to fabricate the filaments, whose printability and anisotropy were tested by three-dimensional (3D) printing experiments. Findings A candidate content of PIA introducing into PBT was obtained to be about 30 per cent, and the Izod notched impact strength of PBTIS increased with the increase of αSA. The results showed that the PBTIS (nPTA/nPIA = 7/3, αSA = 3-5mol%) is suitable for FDM. Originality/value New printing materials with good Izod notched impact strength were obtained by introducing PIA and SA (nPTA/nPIA = 7/3, αSA = 3-5 mol%) into PBT and their anisotropy are better than that of ABS.


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