Mechanical Properties and Structure of Ti-6Al-4V with Graded-Porosity Coatings Applied by Plasma Spraying for Use in Orthopedic Implants

Author(s):  
H Hahn ◽  
PJ Lare ◽  
RH Rowe ◽  
AC Fraker ◽  
F Ordway
Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3467
Author(s):  
Anna Nocivin ◽  
Doina Raducanu ◽  
Bogdan Vasile ◽  
Corneliu Trisca-Rusu ◽  
Elisabeta Mirela Cojocaru ◽  
...  

The present paper analyzed the microstructural characteristics and the mechanical properties of a Ti–Nb–Zr–Fe–O alloy of β-Ti type obtained by combining severe plastic deformation (SPD), for which the total reduction was of etot = 90%, with two variants of super-transus solution treatment (ST). The objective was to obtain a low Young’s modulus with sufficient high strength in purpose to use the alloy as a biomaterial for orthopedic implants. The microstructure analysis was conducted through X-ray diffraction (XRD), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) investigations. The analyzed mechanical properties reveal promising values for yield strength (YS) and ultimate tensile strength (UTS) of about 770 and 1100 MPa, respectively, with a low value of Young’s modulus of about 48–49 GPa. The conclusion is that satisfactory mechanical properties for this type of alloy can be obtained if considering a proper combination of SPD + ST parameters and a suitable content of β-stabilizing alloying elements, especially the Zr/Nb ratio.


2005 ◽  
Vol 502 ◽  
pp. 505-510 ◽  
Author(s):  
Masami Futamata ◽  
Xiaohui Gai ◽  
Toyokazu Mizumoto ◽  
Kimio Nakanishi

To fabricate thermal spraying coatings with good reproducibility, it is necessary to improve the process of the equalization of both thermal history and impacting behavior of the particles. In this study, the characteristics of the solution type plasma spraying using the hollow-cathode type torch are investigated. The physical and mechanical properties that are different from usual thermal spraying coatings are described. By using solutions including metal ingredients in a state of ion, colloid or sol, thinner coating that cannot be made by conventional plasma spraying methods is formed on various substrates. The coatings are uniform in appearance.


Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 421
Author(s):  
Salome Hagelstein ◽  
Sergej Zankovic ◽  
Adalbert Kovacs ◽  
Roland Barkhoff ◽  
Michael Seidenstuecker

Zinc alloys have recently been researched intensely for their great properties as bioabsorbable implants for osteosynthesis. Pure zinc (Zn) itself has relatively poor strength, which makes it insufficient for most clinical use. Research has already proven that the mechanical strength of zinc can be enhanced significantly by alloying it with silver. This study evaluated zinc silver alloys (ZnAg) as well as novel zinc silver titanium alloys (ZnAgTi) regarding their mechanical properties for the use as bioabsorbable implants. Compared to pure zinc the mechanical strength was enhanced significantly for all tested zinc alloys. The elastic properties were only enhanced significantly for the zinc silver alloys ZnAg6 and ZnAg9. Regarding target values for orthopedic implants proposed in literature, the best mechanical properties were measured for the ZnAg3Ti1 alloy with an ultimate tensile strength of 262 MPa and an elongation at fracture of 16%. Besides the mechanical properties, the corrosion rates are important for bioabsorbable implants. This study tested the corrosion rates of zinc alloys in PBS solution (phosphate buffered solution) with electrochemical corrosion measurement. Zinc and its alloys showed favorable corrosion rates, especially in comparison to magnesium, which has a much lower degradation rate and no buildup of hydrogen gas pockets during the process. Altogether, this makes zinc alloys highly favorable for use as material for bioabsorbable implants for osteosynthesis.


2014 ◽  
Author(s):  
V. S. Brooks ◽  
Y. B. Guo

Magnesium-Calcium (Mg-Ca) alloy is an emerging metallic biomaterial for manufacturing biodegradable orthopedic implants. However, very few studies have been conducted on mechanical properties of the bi-phase Mg-Ca alloy, especially at the high strain rates often encountered in manufacturing processes. The mechanical properties are critical to design and manufacturing of Mg-Ca implants. The objective of this study is to study the microstructural and mechanical properties of Mg-Ca0.8 (wt %) alloy. Both elastic and plastic behaviors of the Mg-Ca0.8 alloy were characterized at different strains and strain rates in quasi-static tension and compression testing as well as dynamic split-Hopkinson pressure bar (SHPB) testing. It has been shown that Young’s modulus of Mg-Ca0.8 alloy in quasi-static compression is much higher than those at high strain rates. Yield strength and ultimate strength of the material are very sensitive to strain rates and increase with strain rate in compression. Strain softening also occurs at large strains in dynamic compression. Furthermore, quasi-static mechanical behavior of the material in tension is very different from that in compression. The stress-strain data was repeatable with reasonable accuracy in both deformation modes. In addition, a set of material constants for the internal state variable plasticity model has been obtained to model the dynamical mechanical behavior of the novel metallic biomaterial.


1994 ◽  
Vol 186 (1-2) ◽  
pp. 105-112 ◽  
Author(s):  
Kenji Murakami ◽  
Yoshitaka Fujii ◽  
Hiroshi Matsumoto ◽  
Tsuyoshi Irisawa ◽  
Taira Okamoto ◽  
...  

2011 ◽  
Vol 295-297 ◽  
pp. 1361-1368
Author(s):  
Wen Feng Yang

To meet the requirements of integrative mechanical properties and shielding effectiveness of nuclear radiations shielding materials, the boron-rich shielding coating (Fe67.5Ni23.5B9, in wt. %) were produced onto 321 stainless steel substrate (SS) by the air-plasma spraying technology. This type of coating-SS laminated composite will be likely to be used as protection against neutrons and γ rays from radiation shielding systems. The microstructure was characterized by scanning electron microscope (SEM), energy-dispersive spectrometry (EDS) and X-rays diffraction (XRD). The mechanical properties of Fe67.5Ni23.5B9 coatings were investigated, including adhesion strength, tensile properties and residual stress. The shielding effectiveness of the coating-SS laminated composite, including the slowing down of fast-speed neutrons, absorption for 0.4ev below thermal neutrons and the attenuation against 60Co and 137Cs γ rays were investigated. The results show that the produced Fe67.5Ni23.5B9 coatings-SS laminated composite possess homogeneous microstructure, satisfactory integrative mechanical properties and shielding effectiveness which testify the possible application in radiation shielding systems.


2001 ◽  
Vol 711 ◽  
Author(s):  
Elizabeth A. Massa ◽  
Elliott B. Slamovich ◽  
Thomas J. Webster

ABSTRACTHydroxyapatite (HA) is a bone-like ceramic used as a coating for dental and orthopedic implants. It is well known for its good cytocompatibility properties, but is limited in use due to its high solubility within the body and mechanical properties that differ from surrounding tissue and bone. The present in vitro study investigated a variety of dopants as a way to further enhance the good cytocompatibility properties of HA as well as address these problematic properties. The dopants investigated were divalent (magnesium and zinc) and trivalent (yttrium, lanthanum, indium, and bismuth) ions. Of the trivalent ions, yttrium and indium have smaller ionic radii than calcium. The present study showed osteoblast adhesion to be statistically greater (p < 0.1) on yttrium-doped HA and indium-doped HA than on undoped HA. Since yttrium and indium are both trivalent ions of a smaller ionic radius than calcium, and other ions of different size and charge did not show significant changes in osteoblast adhesion, these results suggest that substituting divalent calcium with a trivalent ion of smaller size encourages osteoblast adhesion.


2012 ◽  
Vol 22 (2-3) ◽  
pp. 125-130 ◽  
Author(s):  
Leszek Łatka ◽  
Andrea Cattini ◽  
Didier Chicot ◽  
Lech Pawłowski ◽  
Stefan Kozerski ◽  
...  

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