scholarly journals Physicomechanical behavior of composites of polypropylene, and mineral fillers with different process cycles

DYNA ◽  
2018 ◽  
Vol 85 (207) ◽  
pp. 260-268 ◽  
Author(s):  
Carolina Caicedo ◽  
Aldo Rafael Vázquez-Arce ◽  
Omar Hernán Ossa ◽  
Hever De La Cruz ◽  
Alfredo Maciel-Cerda

In this work, a development of composites of polypropylene [PP] with mineral fillers [M] of talc and calcium carbonate [CaCO3] by co-extrusion and injection techniques were carried out. In the preparation of the mixtures, was used the rheometric analysis to define the optimum temperature of the extrusion process, and a weight ratio of 80:20 PP: fillers was maintained, while for the injection molding process six generations of PP and its compounds were obtained to study the rheological, thermal, morphological and mechanical properties of the new series of PPnM composites formed from a recycled matrix and the PPMn series reprocessed compounds for up to six cycles. The results allowed correlating the changes due to the thermal history and the influence of adding the mineral fillers. The mechanical characterization in the reprocessed matrix indicated a 6.0% decrease in tensile strength and an increase in flexural strength of 9.9%. Likewise, the compounds showed an increase in tensile strength of 11.7%, while flexural strength reached 35.8%. From the thermogravimetric analysis, the degradation temperature in the matrix gradually decreased from 406.5 °C to 364.3 °C, for the sixth generation with respect to the virgin material by the injection process; meanwhile, for the compounds was maintained around 410 °C indicating an optimal interaction, these results could be contrasted with the colorimetric analysis. Finally, re-injection led to a significant decrease in the size of the talc and CaCO3 particles; the sizes were estimated from microstructural analysis from Scanning Electron Microscope.

2021 ◽  
Author(s):  
Balaji Ayyanar Chninnappan ◽  
K. Marimuthu ◽  
C. Bharathiraj ◽  
B. Gayathri ◽  
S. K. Pradep Mohan

Abstract Samanea saman (SS) flower particulates were filled in Polylactic acid (PLA) composites were fabricated with different 0, 10, and 20 wt. % through the injection molding process. The elemental composition and morphology of SS PLA composites were studied through FESEM and Energy Dispersive X-ray analysis. Thermal stability of the SS PLA composites specimens was carried out through Thermo Gravimetric Analysis (TGA) and Differential Scanning Calorimeter (DSC). Crystal orientations studied through X-Ray Diffraction (XRD) showed the presence of the orthorhombic SS particulates. The properties of the composites were investigated such as tensile strength, compressive strength, flexural strength, and Shore D Hardness. It was found that 20 wt. % of SS filled PLA composites has a superior tensile strength of 43.76 MPa, the compression strength of 37.94 MPa, the flexural strength of 72.47 MPa, and Shore D Hardness of 80.1 SHN than pure PLA. SS particulates-filled PLA composites would be used for low-strength applications.


2006 ◽  
Author(s):  
Mikae¨l Chailly ◽  
Vincent Gilbert ◽  
Jean-Yves Charmeau ◽  
Yves Bereaux

Due to increasing expectings from the market, the aspect of molded parts has to be improved. Some of the defects observed such as scratches on these parts is related to the demolding stage. To limit this, we investigated the influence on demolding forces using various surface deposits on the mold surface, mainly PVD and PACVD deposits : Chromium nitrium (CrN), Titane nitrium (TiN), Diamond like Carbon (DLC), glassy deposit (SiOx), Chromium and polished steel on an cube-shaped insert in an instrumented mold (with force sensors). Injection campaign was led on three polymers which differ in terms of nature : an amorphous polymer (polycarbonate), a semi-crystalline one (polybutylene terephatalate) and one mix of copolymers (styrene acrylonitrile/ acrylonitrile butadiene styrene). We studied the evolution of these forces through the demolding stage. This allowed us to evaluate the work energy necessary to eject the part from the insert, and to correlate those data to shrinkage of the polymer part, adhesion between polymer and mold surface and friction coefficient between those surfaces during the demolding stage. We also measured the influence the surface temperature of the part just before the demolding stage thanks to an infrared camera to investigate the thermal influence of these deposits in the injection process. Our results show an influence of deposits on demolding forces which is strongly dependent on nature of the polymer (of course) but also on its chemical nature. They also have a slight influence on temperature of the part even if they are only a few microns thick. We therefore developped a method to evaluate surface deposits and their impact on demolding forces, in terms of adhesion polymer/treament and friction.


2020 ◽  
Vol 18 (11) ◽  
pp. 801-805
Author(s):  
Kyung-Soo Jeon ◽  
R. Nirmala ◽  
Seong-Hwa Hong ◽  
Yong-II Chung ◽  
R. Navamathavan ◽  
...  

This manuscript is dealt with the synthesis of short carbon fibers reinforced polycarbonate polymer composite by using injection modeling technique. Four different composite materials were obtained by varying the carbon fibers weight percentage of 10, 20, 30 and 40%. The synthesized carbon fibers/polycarbonate composites were characterized for their morphological, mechanical and thermal properties by means of scanning electron microscopy (SEM), universal testing machine (UTM) and IZOD strength test. The resultant carbon fibers/polycarbonate composites exhibited excellent interfacial adhesion between carbon fibers and polycarbonate resin. The tensile properties were observed to be monotonically increases with increasing carbon fiber content in the composite resin. The tensile strength of carbon fiber/polycarbonate composites with the carbon fiber content 40% were increased about 8 times than that of the pristine polycarbonate matrix. The carbon fibers/polycarbonate composites with 40 wt.% of short carbon fibers exhibited a high tensile strength and thermal conductivity. The incorporation of carbon fiber in to polycarbonate resin resulted in a significant enhancement in the mechanical and the thermal behavior. These studies suggested that the short carbon fiber incorporated polycarbonate composite matrix is a good candidate material for many technological applications.


2020 ◽  
Vol 28 (04) ◽  
pp. 2050032
Author(s):  
Hoang Minh Khoa Nguyen ◽  
Dong-Wook Oh

Short-fiber reinforced polymer composites have been widely used in industrial applications due to high strength-to-weight ratio, versatile manufacturing process, and etc. The alignment of fiber type additives plays an important role in the mechanical properties of a composite material. In this paper, an injection molding process was imitated with a liquid polymer composite flow inside a [Formula: see text] elbow channel. We performed a flow visualization experiment and analyzed the additive alignment of carbon fiber flowing in the polydimethylsiloxane (PDMS) medium. By analyzing the flow visualization images, the angle changes at the corner region of the elbow channel were calculated. At the corner region, the change of passage direction leads to the change of fiber orientation. It was observed that near to the convex region, fibers have angle change values larger than the fibers traveling near to the concave region.


2014 ◽  
Vol 609-610 ◽  
pp. 681-686
Author(s):  
Chun Bo Liu ◽  
Jian Ye Sun

In order to broaden the application range of LCP, the simulation of the LCP Hele-Shaw flow in the square cavity was conducted. The temperature of the cavity was constant 300°C. In the simulation the Leslie-Ericksen and TIF theories were used. With this simulation results, we can predict the position of the flow front at any time during the whole injection process and grasp the change of the pressure field and the velocity field. The change of the pressure and the velocity fields were very slow, there was no distortion point in the whole flow field. In the layer near the wall, the directors arranged evenly according to the direction of the flow and in the center layer it was decided by the shear rate in the X-Y plane.


2014 ◽  
Vol 607 ◽  
pp. 65-69 ◽  
Author(s):  
M. Ibrahim ◽  
N.S. Badrishah ◽  
Nasuha Sa'ude ◽  
Mohd Halim Irwan Ibrahim

This paper presents the development of a new Wood Plastic Composite (WPC) material for Fused Deposition Modeling (FDM) feedstocks. In this study, a biodegradable polymer matrix (POLYACTIDE, PLA) was mixed with natural wood flour (WF) by Brabender mixer, and the samples produced by injection molding machine. The effect of wood was investigated as a filler material in composite FDM feedstock and the detailed formulations of compounding ratio by weight percentage. Based on results obtained, it was found that, compounding ratio of PLA80%:WF20% has a goods result on the tensile strength and PLA60% : WF40% gave a higher value of flexural strength. An increment of 20% to 40% WF filler affected the flexural strength, and hardness results. The highly filled WF content in PLA composites increases the mechanical properties of PMC material through the injection molding process. The potential of development of a sustainable composite material will be explored as the FDM feedstocks in the rapid prototyping process.


2015 ◽  
Vol 786 ◽  
pp. 210-214
Author(s):  
M.S. Rusdi ◽  
Mohd Zulkifly Abdullah ◽  
A.S. Mahmud ◽  
C.Y. Khor ◽  
M.S. Abdul Aziz ◽  
...  

Computational Fluid Dynamic (CFD) was used to simulate the injection molding process of a tray. The study focuses on pressure distribution and velocity drop during the injection process. CFD simulation software ANSYS FLUENT 14 was utilized in this study. The melt front pressure in the mold cavity shows that it was affected by the shape of mold cavity and filling stage. The melt front pressure will decrease as the flow move further than the sprue but it will increase rapidly when the mold was about to be fully filled. The slight pressure drop was detected when the molten flow meets the rib of the tray. The velocity of higher injection pressure was greater than the lower injection pressure but the velocity rapidly dropped when the melt front fully filled the cavity. The current predicted flow profile was validated by the experimental results, which demonstrates the excellent capability of the simulation tool in solving injection-molding problems.


1999 ◽  
Vol 14 (7) ◽  
pp. 2871-2880 ◽  
Author(s):  
Gary G. Tibbetts ◽  
John J. McHugh

This article discusses the mechanical properties of vapor-grown carbon fiber (VGCF)/nylon and VGCF/polypropylene composites. Fibers in the as-produced condition yielded composites with marginally improved mechanical properties. Microscopic examination of these composites clearly showed regions of uninfiltrated fibers, which could account for the unsatisfactory mechanical properties. The infiltration of the fibers by both polymers was improved by carefully ball milling the raw fiber so as to reduce the diameter of the fiber clumps to less than 300 μm. Properties of composites made with ball-milled material were improved in every respect. VGCF reinforcement in nylon slightly improved the tensile strength and doubled the modulus, while VGCF in polypropylene doubled the tensile strength and quadrupled the modulus compared to unreinforced material. Moreover, the composites were sufficiently improved that differences in fiber surface preparation became important. For example, air-etched fibers and fibers covered with low concentrations of aromatics produced polypropylene composites with significantly better mechanical properties than did fibers whose surfaces were heavily coated with aromatics. Both the tensile strength and the modulus of the composites fabricated with clean fibers exceeded theoretical values for composites made with fibers randomly oriented in three dimensions, indicating that the injection-molding process oriented the fibers to some extent.


Sign in / Sign up

Export Citation Format

Share Document