Micro-morphological analysis of the effect of sampling by the volumetric ring method on soil structure
This report investigates the effect of sampling by the volumetric ring method on pore size number and shape distributions. Soil porosity was analyzed using the micromorphological image analysis technique, which helped to explain soil structure changes near the border of samples collected in cylinders and provided detailed information about pore shape, number, and size distribution variations along the samples. Compaction due to sampling affects mainly large irregular and rounded pores of the soils utilized in this study. When evaluating inaccuracies in density measurements due to the compacted regions caused by the sampling device the average soil bulk density for each soil resulted in the ranges of 1.72 ± 0.05 g.cm −3 for Geric Ferralsol soil, 1.66 ± 0.03 g.cm −3 for Eutric Nitosol soil and 1.33 ± 0.05 g.cm −3 for Rhodic Ferralsol soil, respectively. When calculating the average soil bulk density over smaller regions, e.g. in the center of each sample (area of 17.14 mm 2 ) results reduced to 1.64 ± 0.05 g.cm −3 with Geric Ferralsol soil, 1.56 ± 0.03 g.cm −3 with Eutric Nitosol soil and 1.29 ± 0.10 g.cm −3 with Rhodic Ferralsol soil, respectively. These results clearly indicate the effect of sampling by the volumetric ring method. The use of image analysis was essential to explain compaction differences close to the border of the samples collected using cylinders (volumetric ring method) and provided detailed information about pore shape and size distribution variations within soil samples. The results are useful as indicators of the consequences of sampling on the quality of soil samples.