Microstructure and strengthening mechanism of die-cast Mg–Gd based alloys

2008 ◽  
Vol 23 (5) ◽  
pp. 1269-1275
Author(s):  
Qiuming Peng ◽  
Lidong Wang ◽  
Yaoming Wu ◽  
Limin Wang

Mg–8Gd–2Y–Nd–0.3Zn (wt%) alloy was prepared by the high pressure die-cast technique. The microstructure, mechanical properties in the temperature range from room temperature to 573 K, and strengthening mechanism were investigated. It was confirmed that the Mg–Gd-based alloy with high Gd content exhibited outstanding die-cast character. The die-cast alloy was mainly composed of small cellular equiaxed dendrites and the matrix. The long lamellar-shaped stacking compound of Mg3X (X: Gd, Y, Nd, and Zn) and polygon-shaped precipitate of Mg5RE (RE: Gd, Y, and Nd) were mainly concentrated along the dendrite boundaries. Meanwhile, it was demonstrated that the Zn addition affects the formation of non-equilibrium precipitate Mg3X. The ultimate tensile strength, yield strength, and Young’s modulus were 302 MPa, 267 MPa, and 38 GPa at room temperature, respectively. The outstanding mechanical properties were mainly attributed to the small dendrite spacing, wide skin region, and some dispersed precipitates in the alloy formed by the high-pressure die-cast technique. Designing a novel die-cast Mg alloy with good heat resistance without Al element is a significant accomplishment.

2010 ◽  
Vol 150-151 ◽  
pp. 815-820
Author(s):  
Shu Jun Ji ◽  
Xue Yi Guo ◽  
Jian Xiong Dong ◽  
Peng Su

Using corundum, quartz, kaoline, etc, as base components and CeO2-rich mixed rare earth as modifier, foam ceramics were fabricated adopting the organic foam impregnation process. The mixed rare earth addition had much improving effects on the matrix mechanical properties owing to much glass phase and acerate mullite growing. While 3wt% was considered to be the optimal addition, in this case, homogeneous and compact ceramic microstructure with maximal glass condensation and minimal porosity formed, with the matrix compressive strength and the flexural strength at room temperature reached 0.87MPa and 0.66MPa respectively, which were 52.6% and 73.7% higher than the original samples respectively. As the mixed rare earth addition exceeded further, the compressive strength increased slowly and the flexural strength descended gradually. XRD and SEM were used to structure strengthening mechanism analysis.


2005 ◽  
Vol 488-489 ◽  
pp. 385-388
Author(s):  
Qiang Li ◽  
Qu Dong Wang ◽  
Xiao Qing Zeng ◽  
Wen Jiang Ding ◽  
Quanbo Tang ◽  
...  

Nd, Y and Ca containing Mg-Zn-Zr alloys are produced by electromagnetic direct-chilling casting process, and extruded at a temperature of 643K with two extrusion ratios of 38:1 and 22:1, respectively. The grain size is markedly reduced from 80µm in as-cast alloy to 2~5µm in as-extruded alloy due to dynamic recrystallization, and lamellar eutectics at grain boundaries in as-cast alloy are broken up and fine precipitates in the matrix come forth during hot extrusions. Mechanical properties of the alloys are measured by tensile test from room temperature to 523K. Nd, Y and Ca are favorable to the strength of the hot-extruded alloy, especially the elevated-temperature strength, which is above 200MPa in ultimate tensile strength at 523K.


2007 ◽  
Vol 26-28 ◽  
pp. 145-148 ◽  
Author(s):  
Shu Hei Uchida ◽  
Ippei Takeuchi ◽  
Gentaro Gonda ◽  
Kinji Hirai ◽  
Tokuteru Uesugi ◽  
...  

Twin roll casting process combines casting and hot rolling into a single process. In this study, mechanical properties at room temperature and microstructure of the twin roll cast AZ91 magnesium alloy are investigated. The alloy exhibited a good combination of high ultimate strength of 343MPa, yield stress of 224MPa and elongation to failure of 13%. The mechanical property was very excellent compared with AZ91 die-cast alloy. EPMA analysis reveals that the Al concentration in Mg matrix is higher in twin roll cast alloy than that in die-cast alloy. This high Al concentration must be the origin of the good mechanical properties of twin roll cast alloy at room temperature.


2005 ◽  
Vol 488-489 ◽  
pp. 127-130
Author(s):  
Guang Yin Yuan ◽  
Wen Jiang Ding ◽  
Kenji Amiya ◽  
Hidemi Kato ◽  
Akihisa Inoue

Mg-8Zn-4Al-xY base alloys containing an icosahedral quasicrystal phase (i-phase) as a main strengthening phase were prepared by casting into a copper mould at moderate cooling rates. The Y addition was effective for decreasing the size of i-phase and the more homogeneousness of its dispersed state. The mechanical properties at room temperature were much superior to those of AZ91 alloy. The creep tests indicated a promising high temperature creep resistance of the quasicrystal-reinforced Mg-Zn-Al-Y cast alloy. The dislocation characteristic in crept specimens which containing i-phase and no i-phase was analyzed and strengthening mechanism was discussed.


2020 ◽  
Vol 10 (3) ◽  
pp. 1159 ◽  
Author(s):  
Yingmei Xie ◽  
Hiroki Kurita ◽  
Ryugo Ishigami ◽  
Fumio Narita

Epoxy resins are a widely used common polymer due to their excellent mechanical properties. On the other hand, cellulose nanofiber (CNF) is one of the new generation of fibers, and recent test results show that CNF reinforced polymers have high mechanical properties. It has also been reported that an extremely low CNF addition increases the mechanical properties of the matrix resin. In this study, we prepared extremely-low CNF (~1 wt.%) reinforced epoxy resin matrix (epoxy-CNF) composites, and tried to understand the strengthening mechanism of the epoxy-CNF composite through the three-point flexural test, finite element analysis (FEA), and discussion based on organic chemistry. The flexural modulus and strength were significantly increased by the extremely low CNF addition (less than 0.2 wt.%), although the theories for short-fiber-reinforced composites cannot explain the strengthening mechanism of the epoxy-CNF composite. Hence, we propose the possibility that CNF behaves as an auxiliary agent to enhance the structure of the epoxy molecule, and not as a reinforcing fiber in the epoxy resin matrix.


2004 ◽  
Vol 19 (5) ◽  
pp. 1531-1538 ◽  
Author(s):  
Guangyin Yuan ◽  
Kenji Amiya ◽  
Hidemi Kato ◽  
Akihisa Inoue

The structure and mechanical properties of Mg–Zn–Al–Y base cast alloys containing an icosahedral quasicrystal phase (i-phase) as a main strengthening phase were investigated. Mg–8Zn–4Al–xY base bulk alloys containing the i-phase were prepared by casting into a copper mold at moderate cooling rates. The Y addition was effective for decreasing the size of the i-phase and the increasing the homogeneity of its dispersed state. The mechanical properties examined by compression tests at room temperature were much superior to those of a conventional AZ91 Mg alloy. The creep tests at elevated temperatures indicated a promising high temperature creep resistance of the quasicrystal-reinforced Mg–Zn–Al–Y cast alloy. The strengthening mechanism was also discussed.


2021 ◽  
Vol 1035 ◽  
pp. 925-930
Author(s):  
Ya Zhou Li ◽  
Yu Zhao ◽  
Xu Ran

To reduce the agglomeration of graphene and enhance the interface bonding between reduced graphene oxide (RGO) and copper substrate, copper plating on the graphene surface was prepared by the in-situ reduction method. To improve the strength of the copper matrix, the microalloying strategy of adding titanium to the matrix was adopted. By changing the mass fraction of titanium in the matrix, the optimum ratio of RGO was obtained( Ti mass fraction was 5:1), and the tensile strength was maximized. The results show that RGO did not agglomerate obviously in the matrix. At the same time, the composite powder could be densified rapidly by spark plasma sintering (SPS), which could effectively protect the original distribution of the additive phase in the matrix. In this paper, Cu@RGO/Cu-Ti was prepared and the strengthening mechanism of the composites discussed, providing a new insights into the interface design and carbide formation mechanism of advanced graphene/copper composites with high mechanical properties.


2021 ◽  
Vol 1023 ◽  
pp. 45-52
Author(s):  
Xiao Yan Wang ◽  
Meng Li ◽  
Zhi Xun Wen

After solid solution treatment at 1335°C for 4 hours and cooling to room temperature at different rate, the nickel-based single crystal superalloy were made into three kinds of nickel-based single crystal superalloy materials containing different size γ′ phases, respectively. The tensile test of I-shaped specimens was carried out at 980°C, and their effect of γ′ phase microstructure on the tensile properties was studied. The results show that the yielding strength of the material air-cooled to room temperature was lower than that with cooling rate at 0.15°C/s, but both of them were lower than the yielding strength of original material. Little difference was found on the elastic modulus of I-shaped specimens made of three kinds of materials. When the cubic degree of the γ′ phase is higher and the size is larger, the tensile properties of the material is better, which can be attributed to the larger size and narrower channel of the matrix phase that lead to higher dislocation resistance.


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