The mean inner potential of GaN measured from nanowires using off-axis electron holography

2005 ◽  
Vol 892 ◽  
Author(s):  
Andrew See Weng Wong ◽  
Ghim Wei Ho ◽  
Rafal E Dunin-Borkowski ◽  
Takeshi Kasama ◽  
Rachel A Oliver ◽  
...  

AbstractThe mean inner potentials of wurtzite GaN nanowires are measured using off-axis electron holography in the transmission electron microscope (TEM). The nanowires have a circular cross-section and are suspended across holes in a holey carbon film, resulting in an accurate knowledge of their thickness profiles and orientations. They are also free of the implantation and damage that is present in mechanically-polished ion-milled TEM specimens. The effect of a thin amorphous coating, which is present on the surfaces of the nanowires, on measurements of their mean inner potential is assessed. A value for the mean inner potential of GaN of (16.7 ± 0.3) V is obtained from these samples.

During the course of study, by the authors, of the flow of fluids in the small clearances which exist between the moving and fixed parts of certain machines, an accurate knowledge was desired of the range over which the equations of viscous flow could be applied. An exhaustive search revealed an absence of any record of experimental work which could be of direct assistance. An investigation was accordingly undertaken with the object of obtaining the desired information, and as the preliminary results were of an interesting and unexpected nature, the experiments were extended to cover the whole range of velocities and dimensions permitted by the apparatus. They have shown briefly that the lower critical velocity (as ordinarily understood) for flow between flat plates occurs at a value of the Reynolds number about one-half that found for pipes of circular cross section, if the linear dimension in that number is the distance between the plates and the diameter respectively. For velocities well below this limit there is evidence, however, of a distinct deviation from true viscous flow if initial disturbing factors are present, and the influence of such disturbing factors does not disappear entirely until a second well-defined limit is reached, which has a value of about one-tenth of the lower critical number. It would appear that below this limit eddies do not exist at any point in the pipe, and the flow is truly viscous. The suggestion is accordingly made that there may be three distinct types of flow: ( a ) one in which eddies cannot exist, corresponding to truly viscous flow; ( b ) one in which eddies may exist, due to an initial disturbance, but cannot be sustained in the pipe, the initial eddies therefore ultimately disappearing; and ( c ) one in which eddies once generated will be maintained without decrement throughout the pipe, corresponding to truly turbulent flow. The use of a channel of rectangular cross section for a study of the fundamental laws of the flow of fluids possesses advantages, in point of simplicity, which were recognised at once by Reynolds in his classical research into the cause of instability of flow. In the form in which this channel is used by the present writers, an additional and important advantage is obtained over the circular pipe by the fact that the controlling dimension may be varied over a wide range whilst retaining the same surfaces as boundaries. It is, in essentials, an adjustable pipe. The upper plate A (fig. 1) and the lower plate B are brass castings suitably drilled to provide inlet and outlet passages and pressure measuring points. The surfaces forming the pipe are hand scraped to a surface plate, and are separated at the ends by brass foil shims of suitable thickness, thus providing a passage between the inlet and outlet ports. The sides of this passage are closed by the plates C and D, very thin rubber insertion providing a watertight joint. All parts are sufficiently robust to reduce distortion under pressure to an amount found to be negligible.


1998 ◽  
Vol 4 (2) ◽  
pp. 146-157 ◽  
Author(s):  
Y.C. Wang ◽  
T.M. Chou ◽  
M. Libera ◽  
E. Voelkl ◽  
B.G. Frost

This study describes the use of transmission electron holography to determine the mean inner potential of polystyrene. Spherical nanoparticles of amorphous polystyrene are studied so that the effect of specimen thickness on the phase shift of an incident electron wave can be separated from the intrinsic refractive properties of the specimen. A recursive four-parameter χ-squared minimization routine is developed to determine the sphere center, radius, and mean inner potential (Φ0) at each pixel in the phase image. Because of the large number of pixels involved, the statistics associated with determining a single Φ0 value characteristic of a given sphere are quite good. Simulated holograms show that the holographic reconstruction procedure and the χ-squared analysis method are robust. Averaging the Φ0 data derived from ten phase images from ten different polystyrene spheres gives a value of Φ0PS = 8.5 V (σ) = 0.7 V). Specimen charging and electron-beam damage, if present, affect the measurement at a level below the current precision of the experiment.


Author(s):  
T. Hirayama ◽  
Q. Ru ◽  
T. Tanji ◽  
A. Tonomura

The observation of small magnetic materials is one of the most important applications of electron holography to material science, because interferometry by means of electron holography can directly visualize magnetic flux lines in a very small area. To observe magnetic structures by transmission electron microscopy it is important to control the magnetic field applied to the specimen in order to prevent it from changing its magnetic state. The easiest method is tuming off the objective lens current and focusing with the first intermediate lens. The other method is using a low magnetic-field lens, where the specimen is set above the lens gap.Figure 1 shows an interference micrograph of an isolated particle of barium ferrite on a thin carbon film observed from approximately [111]. A hologram of this particle was recorded by the transmission electron microscope, Hitachi HF-2000, equipped with an electron biprism. The phase distribution of the object electron wave was reconstructed digitally by the Fourier transform method and converted to the interference micrograph Fig 1.


1984 ◽  
Vol 106 (1) ◽  
pp. 252-257 ◽  
Author(s):  
D. E. Metzger ◽  
C. S. Fan ◽  
S. W. Haley

Modern high-performance gas turbine engines operate at high turbine inlet temperatures and require internal convection cooling of many of the components exposed to the hot gas flow. Cooling air is supplied from the engine compressor at a cost to cycle performance and a design goal is to provide necessary cooling with the minimum required cooling air flow. In conjunction with this objective, two families of pin fin array geometries which have potential for improving airfoil internal cooling performance were studied experimentally. One family utilizes pins of a circular cross section with various orientations of the array with respect to the mean flow direction. The second family utilizes pins with an oblong cross section with various pin orientations with respect to the mean flow direction. Both heat transfer and pressure loss characteristics are presented. The results indicate that the use of circular pins with array orientation between staggered and inline can in some cases increase heat transfer while decreasing pressure loss. The use of elongated pins increases heat transfer, but at a high cost of increased pressure loss. In conjunction with the present measurements, previously published results were reexamined in order to estimate the magnitude of heat transfer coefficients on the pin surfaces relative to those of the endwall surfaces. The estimate indicates that the pin surface coefficients are approximately double the endwall values.


1997 ◽  
Vol 3 (S2) ◽  
pp. 1055-1056
Author(s):  
Y.C. Wang ◽  
T.M. Chou ◽  
M. Libera

The phase shift imparted to an incident high-energy electron wave in a TEM is related to the specimen’s electron-refractive properties. These, in turn, are related to the electrostatic potential and, by Fourier transform (1), to the electron scattering factors fei(s) for the various atom species i in the specimen and scattering vectors s. The average refractive index is determined by the mean electrostatic (inner) potential, Φo, and can be modelled as Φo = (C/Ω) Σfei(s0) [equation 1] where C = 47.878 (V-Å2) and the summation runs over all of the atoms in the unit volume Ω (2). Calculated fei(s) data are available from the literature (e.g. 3). These calculations have only been done for neutral atoms and some fully ionized cations and anions. They do not account for electron redistribution due to covalent bonding to which Φo is quite sensitive (4).This research is making Φo measurements using transmission electron holography. Holograms were collected using a 200keV Philips CM20 FEG TEM equipped with a non-rotatable biprism (5) and a Gatan 794 Multiscan camera.


Author(s):  
Q. Ru ◽  
J. Endo ◽  
A. Tonomura

Compared with the wavefront-divided electron holography obtained by an electron biprism, the amplitude-divided one proposed by Matteucci et al. has some essential advantages: less necessary coherency, wide interference area and available to most of transmission electron microscopes. In order to confirm and achieve these advantages in practical use, we introduce some improvements in both hologram formation and reconstruction steps. Two electron-optical setups and experimental results are presented for small objects (<1 μm) and much large objects (>1 μm), respectively.The electron-optics for taking the holograms of small objects is illustrated in Figure 1. A single crystal thin film (gold film of 0.2nm lattice spacing is used in our experiment) is placed on the objects (latex particles of 120 nm on a thin carbon film are used here) with a certain gap. In fact, the gap is spontaneously made by the microgrids of the specimen film and the crystal film.


Author(s):  
A.E. Curzon

The heating effect of an incident electron beam may cause a material to be radiation-sensitive. For example, the adsorption behaviour of inert gases on graphite observed in a transmission electron microscope depends critically on the temperature of the substrate. Early consideration of beam heating dealt with a circular film illuminated at the centre by an electron beam of circular cross-section. In practice, however, the film is often supported across a square aperture and is not centrally illuminated. It has recently been shown that the method of images may be used to solve the problem of the heating of a square film of thermal conductivity k by a beam whose cross-section is entirely within the film. This solution has the advantage that it applies regardless of where the incident electron beam strikes the film. The general solution involves an infinite sum over a two dimensional lattice of heat sources and sinks. Though the sum is readily evaluated by means of a computer, it is helpful to consider a particular limiting case which is readily understood in terms of three images and the main beam. This case is illustrated in Figure 1.


1968 ◽  
Vol 46 (20) ◽  
pp. 2325-2329 ◽  
Author(s):  
Janet S. Merritt ◽  
R. E. Green

The 2200 m/s neutron activation cross section of 59Co has been determined with respect to 197Au by irradiating gold and cobalt foils in a thermal neutron flux. The result for the production of 5.261-year 60Co both directly and through 60Com is[Formula: see text]based on a value of σ0 = 98.7 b for, 197Au. Allowing for the 60Com that decays directly to levels in 60Ni yields a value for the 2200 m/s capture cross section of[Formula: see text]The standard deviation of the mean value of seven determinations was ± 0.06 %. The quoted error of ± 0.27 b has been derived from estimates of systematic errors that are discussed.


1975 ◽  
Vol 34 (01) ◽  
pp. 223-235 ◽  
Author(s):  
M. J. S King ◽  
M. S Morris ◽  
M Tager

SummaryFibrin induced by the action of thrombin and by staphylocoagulase was studied by transmission electron microscopy.Periodic striations were consistently observed in the negatively stained preparations of both fibrins. When 4200 major periods in the thrombin fibrin system were measured the mean length was 228 Å. For 3666 major periods in the coagulase fibrin system the mean length was 223 Å. While the T test analysis of these values gave a value of 10, it is noteworthy that the differences are well within the scatter of periodicity reported in the literature for thrombin-induced fibrin.Gross inspection of the preparations indicated that the coagulase-induced fibrin had a knottier appearance and was accompanied by a greater amount of background debris than the thrombin-induced fibrin.


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