scholarly journals Essential Oil Composition of Thymus × citriodorus (Pers.) Schreb. at Different Harvest Stages

2017 ◽  
Vol 45 (1) ◽  
pp. 185-189 ◽  
Author(s):  
Ozlem TONCER ◽  
Sengul KARAMAN ◽  
Emel DIRAZ ◽  
Tahsin SOGUT ◽  
Suleyman KIZIL
Keyword(s):  
Essential Oil ◽  
Essential Oil Composition ◽  
Biologically Active ◽  
Bornyl Acetate ◽  
Oil Composition ◽  
Flowering Stage ◽  
Phenological Stages ◽  
Full Flowering ◽  
Total Oil ◽  
Active Substances

Thymus is represented by 39 species (60 taxa) in Turkey and the rate of its endemism is 45% in Turkey. The herb is widely used for several purposes. Its essential oil compositions and biologically active substances are affected by the phenological stages. Therefore, the aim of this study is to evaluate the variations in the essential oil composition of Thymus × citriodorus (Pers.) Schreb. growing in Southeastern Anatolia Region of Turkey at different phenological stages (pre-flowering, full flowering, post flowering). The oils were obtained by hydrodistillation of air-dried samples. The yields of oils (w/w %) at different phenological stages was respectively 2.0% at pre-flowering state, 1.9% at flowering stage, and 1.3% at post-flowering stage. T. × citriodorus was determined mainly by using GC/MS. A total of 21 compounds, representing 93.9% in the pre-flowering stage, 98.8% in the flowering stage and 98.91% in post-flowering of the total oil, were identified. Monoterpene hydrocarbons (terpinolene) and oxygenated monoterpenes (α-terpineol) were observed to have the highest percentage in T. × citriodorus oil. The major compounds of the oil were terpinolene, α- terpineol, linalool, bornyl acetate and borneol. The highest percentage of terpinolene was determined to be 71% in flowering stages.

Effect of elevation and phenological stages on essential oil composition of Stachys

2017 ◽  
Vol 42 (6) ◽  
Author(s):  
Masomeh Alimohammadi ◽  
Mehrab Yadegari ◽  
Hamze Ali Shirmardi
Keyword(s):  
Essential Oil ◽  
Oil Content ◽  
Essential Oil Composition ◽  
Oil Composition ◽  
Flowering Stage ◽  
Natural Habitats ◽  
Phenological Stages ◽  
Methyl Chavicol ◽  
Full Flowering ◽  
Germacrene D

AbstractObjective:Determine the best elevation and phenological stages effects on essential oil content and composition inMaterials and methods:Three phenological stages (vegetative, full flowering and seeding) and three elevation ranges (2500–2700, 2700–2900 and over 2900 m), shoots of plants collected from Kallar mountain as natural habitats from Chaharmahal and Bakhtiari Province. Composition of essential oil detected by GC/MS.Results:The maximum amount of secondary metabolites of β-ocimene, methyl chavicol, germacrene-D, 1,8 cineole and phthalate had measured in vegetative stage and various of elevation ranges. The most essential oil content (0.145%) was obtained in 2700–2900 m and full flowering stage. The most components in full flowering were β-eudesmol, menthol and γ-eudesmol. The most of germacrene-D, levomenol, β-thujene, β-caryophyllene, β-sesquiphellandrene, α-eudesmol and delta-cadinene was achieved in seeding stage.Conclusion:Elevation and phenological stages had significant effect on essential oil of

scholarly journals Composition of Essential Oil of Aerial Parts of Chamomilla suaveolens from Estonia

2010 ◽  
Vol 5 (1) ◽  
pp. 1934578X1000500 ◽  
Author(s):  
Anne Orav ◽  
Janne Sepp ◽  
Tiiu Kailas ◽  
Mati Müürisepp ◽  
Elmar Arak ◽  
...  
Keyword(s):  
Essential Oil ◽  
Palmitic Acid ◽  
Essential Oil Composition ◽  
Biologically Active Compounds ◽  
Biologically Active ◽  
Oil Composition ◽  
Active Compounds ◽  
Aerial Parts ◽  
Total Oil

Variations in the essential oil composition of aerial parts of pineapple weed (Chamomilla suaveolens (Pursh) Rydb.) growing wild in Estonia, were determined using GC/FID and GC/MS. Forty-four components were identified, representing over 90% of the total oil. Nine compounds have not been mentioned in the literature before. The principal biologically active compounds in C. suaveolens oils were (Z)-en-yne-dicycloether (17.0 – 40.7%), (E)-β-farnesene (19.5– 32.2%), geranyl isovaleriate (8.4 –18.4%), palmitic acid (0.3 – 9.4%) and myrcene (1.1 – 7.9%). The investigation seems to approve the benefit of using aerial parts of pineapple weed as the substitute for flowers.

scholarly journals Analysis of the essential oil composition of three cultivated Nepeta species from Iran

2020 ◽  
Vol 75 (7-8) ◽  
pp. 247-254 ◽  
Author(s):  
Fatemeh Zahra Amirmohammadi ◽  
Majid Azizi ◽  
Seyyed Hossein Nemati ◽  
Marcello Iriti ◽  
Sara Vitalini
Keyword(s):  
Gas Chromatography ◽  
Essential Oil ◽  
Mass Spectroscopy ◽  
Essential Oil Composition ◽  
Oil Composition ◽  
Flowering Stage ◽  
Plant Materials ◽  
Nepeta Cataria ◽  
Full Flowering ◽  
Main Components

AbstractEssential oils (EOs) of three Iranian cultivated Nepeta species were investigated. The oils were obtained by hydrodistillation of air-dried plant materials at full flowering stage and analyzed by gas chromatography (GC) and gas chromatography coupled to mass spectroscopy (GC/MS). In total, 89 compounds were detected. In over 2 years, a number of constituents were identified in the EO of Nepeta binaloudensis first and second years (26 and 37, respectively), Nepeta cataria (25 and 32, respectively), and Nepeta assurgens (45 and 50, respectively). In the oils of N. binaloudensis, 4a-α,7-α,7a-α-nepetalactone (NL) 59.7% and 1,8-cineole (19.6%) during the first and second years, respectively, were the main constituents. The main components of N. cataria were 4a-α,7-α,7a-β-NL (72.8%) and 4a-α,7-β,7a-α-NL (73.9%) during the first and second years, respectively, and 4a–α,7-α,7a-α-NL (55.5%) and 1,8-cineole (24.1%) during the first and second years, respectively, were the main constituents of N. assurgens. The results showed that NLs isomers and 1,8-cineole were the main components of the oils of three cultivated Nepeta species.

scholarly journals Chemical Composition of the Essential Oil of the Flowering Aerial Parts of Pimpinella monoica

2013 ◽  
Vol 8 (11) ◽  
pp. 1934578X1300801
Author(s):  
Rajesh K. Joshi
Keyword(s):  
Gas Chromatography ◽  
Essential Oil ◽  
Essential Oil Composition ◽  
Bornyl Acetate ◽  
Ionization Detector ◽  
Oil Composition ◽  
Flame Ionization ◽  
Aerial Parts ◽  
Sesquiterpene Hydrocarbons ◽  
Total Oil

The essential oil composition of the flowering aerial parts of Pimpinella monoica Dalzell was analyzed by gas chromatography equipped with flame ionization detector (GC-FID) and gas chromatography coupled with mass spectrometry (GC/MS). Fifty four compounds were identified, representing 94.7% of the total oil. The main constituents were bornyl acetate (26.2%), β-caryophyllene (24.0%), limonene (6.7%) and amorpha-4, 11-dien (4.9%). The oil was dominated by sesquiterpene hydrocarbons (40.7%), followed by oxygenated monoterpenes (27.2%), monoterpene hydrocarbons (15.6%), oxygenated sesquiterpenes (7.6%) and others (3.6%).

RESOURCE-SAVING TECHNOLOGY FOR PROCESSING MEDICINAL SAGE

2020 ◽  
Author(s):  
Т.В. ПЕЛИПЕНКО
Keyword(s):  
Essential Oil ◽  
Raw Materials ◽  
Total Yield ◽  
Dry Mass ◽  
Biologically Active ◽  
Flow Diagram ◽  
Resource Saving ◽  
Process Flow Diagram ◽  
Full Flowering ◽  
Active Substances

Исследованы потенциальные возможности ресурсосберегающей технологии переработки шалфея лекарственного (ШЛ). Объектом исследования были образцы эфирномасличного сырья – свежеубранные надземные части ШЛ в фазе полного цветения растения и сухие листья ШЛ. Предложенная схема переработки включает следующие стадии: получение эфирного масла; извлечение конкрета из обезэфиренных отходов экстракцией углеводородным растворителем и последующей его отгонкой; получение абсолютного масла и очищенных восков из конкрета отходов; извлечение дитерпеновых соединений экстракцией этиловым спиртом из отходов сырья после обработки гексаном. В результате исследований фракционного состава сырья и особенностей локализации эфирного масла установлено, что массовая доля эфирного масла составляет, % к сухой массе исследуемых фракций: в листьях и соцветиях 2,75, в стеблях 0,31. Рекомендовано введение ограничительных норм по соотношению технически ценной фракции – листьев и соцветий и балластной – стеблей. Полученное из ШЛ эфирное масло имеет высокое содержание туйонов (31,50%), камфоры (21,0%) и 1,8-цинеола (18,80%). Выход дитерпеновых соединений при комплексной переработке эфирномасличного сырья ШЛ на 38,0% ниже, чем из сухих листьев растения. Однако при расчете на сухую массу листьев и соцветий, составляющих 62,3% от массы сырья, показатели отличаются незначительно. Общий выход продуктов, содержащих комплекс биологически активных веществ, составил 15,53 %, что подтверждает целесообразность использования комплексной переработки шалфея лекарственного. The potential of resource-saving technology for processing medicinal sage (MS) has been studied. Samples of essential oil raw materials-freshly harvested aboveground parts of MS in the phase of full flowering of the plant and dry leaves of MS were the object of research. The proposed process flow diagram includes the following stages: obtaining essential oil; recovering a particular from deester waste by extraction with a hydrocarbon solvent and its subsequent distillation; obtaining absolute oil and refined waxes from a specific waste; extraction of diterpene compounds from raw waste after treatment with hexane by extraction with ethyl alcohol. As a result of studies of the fractional composition of raw materials and the features of localization of essential oil, it was found that the mass fraction of essential oil is, % of the dry mass of the studied fractions: 2,75 in leaves and inflorescences, and 0,31 in stems. The introduction of restrictive norms on the ratio of technically valuable fraction – leaves and inflorescences and ballast – stems is recommended. The essential oil obtained from MS has a high content of tuyons (31,50%), camphor (21,0%) and 1,8-cineol (18,80%). The yield of diterpene compounds in the complex processing of essential oil raw materials MS is 38,0% lower than from dry leaves of the plant. However when calculating the dry mass of leaves and inflorescences, which make up 62,3% of the mass of raw materials, the indicators differ slightly. The total yield products containing a complex of biologically active substances amounted to 15,53%, which confirms the feasibility of complex processing of medicinal sage.

scholarly journals Chemical Composition of the Essential Oil of Baccharoides lilacina from India

2013 ◽  
Vol 8 (3) ◽  
pp. 1934578X1300800
Author(s):  
Rajesh K. Joshi
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Essential Oil ◽  
Essential Oil Composition ◽  
Gas Chromatography Mass Spectrometry ◽  
Caryophyllene Oxide ◽  
Oil Composition ◽  
Aerial Parts ◽  
Sesquiterpene Hydrocarbons ◽  
Total Oil

The essential oil composition from the aerial parts of Baccharoides lilacina (Dalzell & A. Gibson) M. R. Almeida was analyzed by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). A total of 41 compounds have been identified, representing 97.4% of the total oil. The main constituents were identified as β-caryophyllene (27.7%), epi-α-cadinol (25.1%), caryophyllene oxide (9.9%), α-muurolol (7.6%), α-cadinene (6.1%) and α-cadinol 4.5%). The oil was found to be rich in oxygenated sesquiterpenes (47.1%) and sesquiterpene hydrocarbons (46.2%).

Antimicrobial Activity, Essential Oil Composition and Micromorphology of Trichomes of Satureja laxiflora C. Koch from Iran

2004 ◽  
Vol 59 (11-12) ◽  
pp. 777-781 ◽  
Author(s):  
Ali Sonboli ◽  
Alireza Fakhari ◽  
Mohammad Reza Kanani ◽  
Morteza Yousefzadi
Keyword(s):  
Antimicrobial Activity ◽  
Essential Oil ◽  
Glandular Trichomes ◽  
Antimicrobial Property ◽  
Reproductive Organs ◽  
Essential Oil Composition ◽  
Geranyl Acetate ◽  
Native Plant ◽  
Oil Composition ◽  
Total Oil

The antimicrobial activity, essential oil composition and micromorphology of trichomes of Satureja laxiflora C. Koch, a native plant from Iran, were studied. The essential oil was obtained from the aerial parts at the flowering stage by hydrodistillation, and analyzed by GC and GC/MS. Thirty-three compounds representing 99.1% of the total oil were characterized. The major compounds were thymol (63.9%) and γ-terpinene (11.9%) followed by carvacrol (4.8%), p-cymene (3.9%), geraniol (3.2%) and geranyl acetate (3.1%). Furthermore, the essential oil and its three main components were tested against two bacteria and three fungi. The result of the bioassays has been shown that the oil possesses potent antimicrobial property. Chemical studies confirmed that a major portion of this antimicrobial activity is due to thymol present in the oil. Micromorphological analysis by SEM of both vegetative and reproductive organs revealed the presence of abundant sessile capitate and sparse short-stalked glandular trichomes along with retrorse eglandular hairs, giving useful diagnostic characters for identification of this medicinal plant.

scholarly journals Antibacterial Activity and Essential Oil Composition of Satureja spicigera from Iran

2009 ◽  
Vol 64 (1-2) ◽  
pp. 20-24 ◽  
Author(s):  
Fereshteh Eftekhar ◽  
Fereshteh Raei ◽  
Morteza Yousefzadi ◽  
Samad Nejad Ebrahimi ◽  
Javad Hadian
Keyword(s):  
Antibacterial Activity ◽  
Essential Oil ◽  
Essential Oil Composition ◽  
Diffusion Method ◽  
Resistant Organism ◽  
Disc Diffusion ◽  
Oil Composition ◽  
Bacterial Strains ◽  
Full Flowering

The aerial parts of Satureja spicigera were collected at full flowering stage at Gazvin, Iran. The essential oil was isolated by hydrodistillation and analyzed by a combination of capillary GC and GC-MS. Fourteen compounds were identified, of which carvacrol (53.74%) and thymol (36.03%) were the main constituents, representing 99.12% of the total oil. The in vitro antibacterial activity of the essential oil was determined against six ATCC standard bacterial strains (Bacillus subtilis, Enterococcus faecalis, Staphylococcus aureus, Escherichia coli, Klebsiella pneumoniae and Pseudomonas aeruginosa) using disc diffusion as well as measurement of minimum inhibitory concentrations. The disc diffusion results and MIC values indicated high inhibitory activity against the test bacteria. The most susceptible organisms were the Gram-positive B. subtilis and S. aureus followed by E. faecalis, usually resistant to most common antibiotics. Among the Gram-negative bacteria, E. coli and K. pneumoniae were highly sensitive to the different oil concentrations in the disc diffusion method. Finally, P. aeruginosa, a highly resistant organism to most antibiotics, showed moderate susceptibility to Satureja spicigera essential oil.

scholarly journals Essential Oil Composition of Three Species of Thymus Growing Wild in Mazandaran, Iran

2016 ◽  
Vol 49 (2) ◽  
pp. 107-113 ◽  
Author(s):  
H. Ghelichnia
Keyword(s):  
Gas Chromatography ◽  
Essential Oil ◽  
Essential Oils ◽  
Geographical Location ◽  
Ecological Factors ◽  
Essential Oil Composition ◽  
Gas Chromatography Mass Spectrometry ◽  
Geranyl Acetate ◽  
Bornyl Acetate ◽  
Oil Composition

Abstract The genus Thymus has a wide distributional range and chemical composition of the essential oils varies with geographical location of collection site, climate and other ecological factors. The essential oils of the aerial parts were obtained by hydrodistillation and analyzed by gas chromatography (GC) and gas chromatography/mass spectrometry (GC-MS). Twenty seven components were characterized in the essential oil of T. fedtschenkoi. The major constituents of the oil were carvacrol (69.04%), thymol (5.95%), borneol (5.21%), p-cymene (4.20%), bornyl acetate (2.97%) and 1,8- cineole (2.72%). Twenty two components were characterized in the essential oil of T. trauveterri. The major constituents of the oil were carvacrol (54.02%), thymol (9.29%), borneol (3.51%), p-cymene (18.64%) and γ- terpinene (2.97%). Twenty six components were characterized in the essential oil of T. pubescens. The major constituents of the oil were carvacrol (13.85%), α-terpineol (11.49%), thymol (10%), geraniol (9.48%), α-pinene (8.52%), p-cymene (7.66%), camphor (4.66%), γ-terpinene (3.15%) and myrcene (2.22%). Twenty four components were characterized in the essential oil of T. fallax. The major constituents of the oil were carvacrol (41.84%), p-cymene (12.18%), α-terpineol (11.49%), thymol (10%), γ-terpinene (8.68%), borneol (5.11%), geraniol (4.35%) and geranyl acetate (2.16%).

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