STUDY INTO STRUCTURE AND PROPERTIES OF SOLDERS BASED ON ALUMINUM AND ZINC IN THE FORM OF SMALL-SECTION CAST BARS

Author(s):  
K. V. Nikitin ◽  
I. Yu. Timoshkin ◽  
V. I. Nikitin

The study covers Al–Cu–Si (A34 grade) and Zn–Al–Cu (Welco52 grade) solders. It is found that A34 solder (Al–28%Cu–6%Si) melts and crystallizes in a narrow range of temperatures (~18 °C). Solidus and liquidus temperatures of A34 solder are ~508 °С and ~526 °С, respectively. Zn–Al–Cu (Zn–4%Al–2,5% Cu) solder has a eutectic composition, so it melts and crystallizes at a constant temperature of ~389 °С. Densities of investigated solders in their liquid and solid states are studied. A34 solder has a density of 3,02 and 3,32 g/cm3 , respectively. Zinc solder density is 6,28 g/cm3 in the liquid state, and 6,69 g/cm3 in the solid state. The influence of casting conditions on the structure of cast alloys in the form of bars with cross sections of 13, 10, and 5 mm2 was investigated. Main structural components of solder alloys reduce in size as cross sections decrease. The aluminium-based solid solution dendrites and CuAl2 phase are reduced in the A34 solder microstructure. In zinc solders, the most severely reduced ones are zinc-based solid solution dendrites. The best castability is observed in melts obtained from 5 mm2 section bar solders with studied sample gaps of 2,0, 1,5 and 1,0 mm. Eutectic zinc solder features better castability in comparison with A34: castability of the melt obtained from the 5 mm2 section zinc solder rod with a sample gap width of 2,0 mm is 100 % (for A34 melt solder obtained from a rod of the same cross section it was 98 %). Experiments on soldering AK12 alloy plates and 3003 alloy sheets demonstrated that there is a tight border in the solder/base material system and no any defects such as pores or unsoldered areas. There was a slight interpenetration of solder alloys into base materials, especially when soldering AK12 cast plates.

Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 217
Author(s):  
Borut Zorc ◽  
Matija Zorc ◽  
Aleš Nagode

This article deals with an analysis of mixing and determines the admixing rate of a base S355 steel plate in single-bead surface welds by measuring the chemical composition using a plane-scan energy dispersive X-ray spectroscopy (EDXS) on metallographic cross-sections. The results show that obtaining a larger number of EDXS measurements does not necessarily lead to obtaining a more accurate admixing rate. Due to the ever-present segregations that are generally near the base material, the disadvantage of this method is the subjective influence of the SEM operator on the estimated admixing rate. To obtain relevant results, a sufficiently wide area of well-mixed melt, including segregations, must be analyzed. This study showed that by using a sufficiently large number of appropriately selected sites with a sufficiently large surface area, it is possible to estimate the admixing rate from the chemical composition with an accuracy of ≥96% for the geometrically determined admixing rate D = 30%. From several equations, the best result showed an equation which is the arithmetic mean of the two different arithmetic means and in which the artificial influencing factor of the segregations of the base material is taken into account. With this equation, the same value of admixing rate, D = 30%, was obtained using the comparative geometric method.


Coatings ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 823
Author(s):  
Danko Ćorić ◽  
Mateja Šnajdar Musa ◽  
Matija Sakoman ◽  
Željko Alar

The development of cemented carbides nowadays is aimed at the application and sintering of ultrafine and nano-sized powders for the production of a variety of components where excellent mechanical properties and high wear resistance are required for use in high temperature and corrosive environment conditions. The most efficient way of increasing the tribological properties along with achieving high corrosion resistance is coating. Using surface processes (modification and/or coating), it is possible to form a surface layer/base material system with properties that can meet modern expectations with acceptable production costs. Three coating systems were developed on WC cemented carbides substrate with the addition of 10 wt.% Co using the plasma-assisted chemical vapor deposition (PACVD) method: single-layer TiN coating, harder multilayer gradient TiCN coating composed of TiN and TiCN layers, and the hardest multilayer TiBN coating composed of TiN and TiB2. Physical and mechanical properties of coated and uncoated samples were investigated by means of quantitative depth profile (QDP) analysis, nanoindentation, surface layer characterization (XRD analysis), and coating adhesion evaluation using the scratch test. The results confirm the possibility of obtaining nanostructured cemented carbides of homogeneous structure without structural defects such as eta phase or unbound carbon providing increase in hardness and fracture toughness. The lowest adhesion was detected for the single-layer TiN coating, while coatings with a complex architecture (TiCN, TiBN) showed improved adhesion.


2021 ◽  
Vol 320 ◽  
pp. 72-76
Author(s):  
Marek Góral ◽  
Tadeusz Kubaszek ◽  
Marek Poręba ◽  
Małgorzata Wierzbińska

Plasma Spray Physical Vapour Deposition (PS-PVD) method was designed for production of ceramic layer on nickel superalloys. In typical process before deposition the base material is heated by plasma up to 900 °C. In present article the yttria stabilized zirconia (YSZ) was deposited on low melting point materials: 2017A-type aluminium alloy and Cu-ETP copper. The influence of power current, process time and powder feed rate on structure and thickness of obtained coatings was analysed. During first deposition process the overheating of Al-sample was observed and as result the power current was decreased to 1600 A. In the next experimental the approx. 5 mm thick dense coating was formed. During experimental processes of YSZ deposition on copper the thickness of coating increased from approx. 5 to 22 mm. The copper-oxide layer was formed under ceramic layer. The microscopic assessment showed the difficulties in formation of columnar ceramic layer on use base materials. The obtained coating was characterized by dense structure as a result of lower plasma energy during process. The increasing of power current is not possible in the case of overheating of base material.


2018 ◽  
Vol 165 ◽  
pp. 15004 ◽  
Author(s):  
Jochen Tenkamp ◽  
Alexander Koch ◽  
Stephan Knorre ◽  
Ulrich Krupp ◽  
Wilhelm Michels ◽  
...  

Aluminium alloys are promising candidates for energy-and cost-efficient components in automotive and aerospace industries, due to their excellent strength-to-weight ratio and relatively low cost compared to titanium alloys. As modern cast processing and post-processing, e.g. hot isostatic pressing, result in decreased frequency and size of defects, the weakest link depends on microstructural characteristics, e.g. secondary dendrite arm spacing (SDAS), Si eutectic morphology and α-Al solid solution hardness. Hereby, fatigue investigations of the effect of the microstructure characteristics on the cyclic stress-strain behaviour as well as fatigue mechanisms in the low cycle and high cycle fatigue regime are performed. For this purpose, samples of the aluminium cast alloy EN AC-AlSi7Mg0.3 with different Si eutectic morphology and α-Al solid solution hardness were investigated. To compare the monotonic and cyclic stress-strain curves, quasistatic tensile tests and incremental step tests were performed on two microstructure conditions. The results show that the cyclic loading leads to a hardening of the material compared to monotonic loading. Based on damage parameter Woehler curves, it is possible to predict the damage progression and fatigue life for monotonic and cyclic loading in hypo-eutectic Al-Si-Mg cast alloys by one power law.


2000 ◽  
Vol 625 ◽  
Author(s):  
Nicole R. Harlan ◽  
David Bourell ◽  
Seok-Min Park ◽  
Joseph J. Beaman

AbstractA combination of Selective Laser Sintering and colloidal infiltration has been used to create partially stabilized zirconia molds for titanium casting. The mold material system was chosen for its low reactivity with molten titanium and thermal shock resistance. The base material, stabilized zirconia mixed with a copolymer binder, was pre-processed before laser sintering into the desired green shape. The average density of the fired parts could be increased to twice that of the green density. Hole sizes as small as 180 m are possible in thin ceramic components.


2018 ◽  
Vol 3 (1) ◽  
pp. 41
Author(s):  
Wibowo Harso Nugroho ◽  
Nanang J.H. Purnomo ◽  
Hardi Zen ◽  
Andi Rahmadiansah

With the increasingly strict requirements of the ship classification bureau for permissible noise limits to allow passengers and crew to be more comfortable and secure a technical assessment is required to address the characteristics of the noise. A noise beyond the standard allowed in the vessel can be a problem to the ship operators. This noise problem will greatly affects the crews' comfort and passengers. One method to reduce the noise on a ship is to use sound insulation. This paper describes the method for determining the absorption coefficient α and the transmission loss (TL) through an acoustic test of a concrete insulation in the laboratory. The test was conducted by using the method of impedance tube where a speciment response measured by a microphone. In general, the properties of this insulation material remains as the main base material which is concrete. it has been found that the transmission loss value (TL) is in the range of 10 - 50 dB whereas for the base material the concrete is around 22 - 49 dB but the absorption coefficient α of the specimen material is much higher than the material of the base material especially in high frequency, which ranges from 0.15 to 0.97, whereas for concrete base materials have absorbent coefficient α ranges from 0.01 to 0.02.


2018 ◽  
Vol 15 (4) ◽  
pp. 449-454
Author(s):  
Baghdad Science Journal

This work aims to investigate the tensile and compression strengths of heat- cured acrylic resin denture base material by adding styrene-butadiene (S- B) to polymethyl methacrylate (PMMA). The most well- known issue in prosthodontic practice is fracture of a denture base. All samples were a blend of (90%, 80%) PMMA and (10%, 20%) S- B powder melted in Oxolane (Tetra hydro furan). These samples were chopped down into specimens of dimensions 100x10x2.5mm to carry out the requirements of tensile tests. The compression strength test specimens were shaped into a cylinder with dimensions of 12.7mm in diameter and 20mm in length. The experimental results show a significant increase in both tensile and compression strengths when compared to control (standard) results for the preparation material.


Author(s):  
Zainab Ahmed Alkaissi ◽  
Hassan Adnan

The estimation of elastic modulus for road bases is the primary objective of this research which is implemented a significant role in transmitting the vertical loading to the pavement foundation layers. In this study, the effect of weathering conditions on the stiffness of base course is investigated and implied the durability test by subjecting the prepared samples to a different numbers of wet-dry cycles (0,2, 4, 6, 8 and 10). A conventional base materials of local natural gravel aggregate and treated base materials with recycled concrete aggregate RCA at different percentages (0%, 25%, 50% 75% and 100%) is adopted in this research. The elastic characteristics are estimated in terms of elastic modulus. Elastic modulus are estimated by passing the ultrasonic pulse velocity through the untreated and treated base materials laboratory specimens. This test can be used to study the elastic modulus properties of base materials. A multiple linear regression analysis is used for prediction the elastic modulus using the SPSS (software ver.21). Elastic Modulus (kPa) is the dependent variable whereas the independent variable are; No. of wet- dry cycle and Percent (%) of RCA stabilizer. The obtained results for elastic modulus (Es) of granular base material layer showed increasing in elastic modulus with percentage of RCA%., results revealed that the (Es) values reached a maximum value of (6927kPa) for 100%. For the OMC’s values increases due to the percentage increment of RCA in granular base material mixture, this increment in water contents is refer to high absorption capacity of the paste clinging to the RCA. On other side the dry density decrease gradually with adding percentage of (RCA) in granular base material mixture.


2009 ◽  
Vol 410-411 ◽  
pp. 87-96 ◽  
Author(s):  
Markku Keskitalo ◽  
Kari Mäntyjärvi

The laser weldability of austenitic stainless steel (ASS) is good because of the material’s high absorptivity and favourable microstructure. There can be a slight possibility of solidification cracking at high welding speeds and low Crekv/Niekv ratios. Test welds were welded with a Yb:YAG disc laser. The test material was 3.2 mm EN 1.4404 2H C700 type stainless steel plate which was work hardened by cold rolling. The test materials were welded with different heat inputs ranging from 0.024 kJ/mm to 0.12 kJ/mm and with 300 mm and 200 mm focal lengths. The weld seams were square-groove welded as butt weld without filler material. The edges of the groove were made by mechanical or laser cutting. The hardness profiles from cross-sections of the welds were measured with a Vickers microhardness tester using 200 g weight. The mechanical properties were tested with tensile tests. The welds were classified with radiographic verification by an accredited laboratory. A number of the welds were fatigue tested with a bending fatigue tester. The mechanical properties (Rp 0.2%, Rm) of the laser welds were almost the same as in the base material except at the highest heat input. In the radiographic classification, the welds which were welded to the laser-cut edge were classified as class B (accepted). The other welds were classified as class D or C (rejected). The main reasons for the rejection of welds made on mechanically cut edges were lack of penetration or undercut of the weld. A problem with mechanically cut edges, and hence the welds, is that they can be non-square and bent edge. Fatigue tests and tensile tests gave no evidence of solidification cracking in the microstructure of the solidified parts of the welds.


Author(s):  
J. Lertthanasarn ◽  
C. Liu ◽  
M.-S. Pham

Architected lattice metamaterials offer extraordinary specific strength and stiffness that can be tailored through the architecture. Meta-crystals mimic crystalline strengthening features in crystalline alloys to obtain high strength and improved post-yield stability of lattice materials. This study investigates synergistic effects of the base material’s intrinsic crystalline microstructure and architected polycrystal-like architecture on the mechanical behavior of architected metamaterials. Four different polygrain-like meta-crystals were fabricated from 316L, Inconel 718 (IN718) and Ti6Al4V via laser powder bed fusion (L-PBF). While the elastic modulus of the meta-crystals did not vary significantly with the base material or the number of meta-grains, the strength of the meta-crystals showed strong increasing correlation with reducing the size of meta-grains. The differences between meta-crystals made by the three alloys were the most substantial in the post-yield behavior, where the 316L meta-crystals were the most stable while Ti6Al4V meta-crystals were the most erratic. The differences in the post-yield behavior were attributed to the base material’s ductility and intrinsic work-hardening. For all base materials, increasing the number of meta-grains improved the post-yield stability of meta-crystals. The tolerance to the processing defects also differed with the base material. Detrimental defects such as the high surface roughness on the downskin of the struts or the large, irregularly shaped pores near the surface of the struts led to early strut fracture in Ti6Al4V meta-crystals. In contrast, ductile IN718 was able to tolerate such defects, enabling the most significant synergistic strengthening across lengthscales to achieve architected materials of low relative density, but with a very high strength and an excellent energy absorption.


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