Remarks on Selecting Length of Cylindrical Sample to Determine Magnetic Properties of its Material

Author(s):  
A.V. Sandulyak ◽  
R.Yu. Tkachenko ◽  
D.A. Sandulyak ◽  
A.A. Sandulyak ◽  
M.N. Polismakova ◽  
...  

When experimentally studying magnetic properties of the ferromagnetic materials, preferences are often given to a more convenient method involving the use of sufficiently long cylindrical samples with the L length and the D diameter placed in the solenoid field as an alternative to the method based on using classical samples of the toroidal shape (to exclude manifestations of the demagnetizing factor). Currently, required justification is practically missing for specific values of the relative L/D length, which would indicate such [L/D] values (for L/D ≥ [L/D]), at which magnetic properties of a sample (already long enough) correspond to magnetic properties of its material. While the existing recommendations such as [L/D] = 50 are postulated, let us note that relevant experimental studies of magnetic properties of the cylindrical samples with the L/D parameter targeted variation were not made. An attempt was made to fill this gap. For cylindrical steel samples with the different L/D values (from 1 to 50), families of the B magnetic induction and of the μ permeability field dependencies were obtained experimentally using the ballistic method. The sought [L/D] values were determined from the B and μ dependencies on the L/D by the junction abscissa of the ascending and self-similar branches. It was established that in the accepted field strength in the range of H = 0.94--54.2 kА/m magnetizing field, the [L/D] parameter is a variable substantially depending on H (and/or μ). It varies from [L/D] = 10--15 at H = 54.2 kA/m (μ = 30) to [L/D] = 50--60 at H = 4.7 kA/m (μ = 270). And at H < 4.7 kA/m, [L/D] > 50--60, i.e., more than is commonly believed. Thus, it was stated that the data on magnetic properties obtained when using even long samples (L/D = 50) and declared as data on the magnetic properties of the corresponding material, are only close to those with H < 4.7 kA/m. Phenomenological expressions were obtained for the [L/D] determination: exponential with the H argument and logarithmic with the μ argument

2021 ◽  
pp. 014544552110540
Author(s):  
Nihal Sen

The purpose of this study is to provide a brief introduction to effect size calculation in single-subject design studies, including a description of nonparametric and regression-based effect sizes. We then focus the rest of the tutorial on common regression-based methods used to calculate effect size in single-subject experimental studies. We start by first describing the difference between five regression-based methods (Gorsuch, White et al., Center et al., Allison and Gorman, Huitema and McKean). This is followed by an example using the five regression-based effect size methods and a demonstration how these methods can be applied using a sample data set. In this way, the question of how the values obtained from different effect size methods differ was answered. The specific regression models used in these five regression-based methods and how these models can be obtained from the SPSS program were shown. R2 values obtained from these five methods were converted to Cohen’s d value and compared in this study. The d values obtained from the same data set were estimated as 0.003, 0.357, 2.180, 3.470, and 2.108 for the Allison and Gorman, Gorsuch, White et al., Center et al., as well as for Huitema and McKean methods, respectively. A brief description of selected statistical programs available to conduct regression-based methods was given.


2019 ◽  
Vol 298 ◽  
pp. 00015 ◽  
Author(s):  
Alexander Bolotov ◽  
Vladislav Novikov ◽  
Olga Novikova

The paper presents the results of theoretical and experimental studies of the magnetic properties of magnetic lubricating oils. It shows oil magnetization curves in the initial state and after tests in the boundary friction mode. Oil properties were measured by an original magnetometer with Hall sensors. It has been established that triboeffects change oil composition and structure and decrease its magnetization. The results will help determine the optimal operating conditions of magnetic oils while maintaining their magnetic and lubricating properties.


2016 ◽  
Vol 18 (24) ◽  
pp. 16457-16465 ◽  
Author(s):  
M. E. Zilm ◽  
L. Chen ◽  
V. Sharma ◽  
A. McDannald ◽  
M. Jain ◽  
...  

Experimental studies and theoretical predictions have been conducted to investigate magnetic properties of transition metal-substituted hydroxyapatite.


Geophysics ◽  
1956 ◽  
Vol 21 (4) ◽  
pp. 1100-1110 ◽  
Author(s):  
V. Bhaskara Rao

Hysteresis characteristics of a magnetite sample from Gudur area in South India have been studied up to a maximum magnetizing field of 375 oersteds. The apparatus used was the same as developed by Bruckshaw and Rao. The studies have shown that the susceptibilities of rocks are mainly dependent on the magnetite contained in them. Variations of susceptibility of magnetite with its grain size, its purity and its distribution in an inert matrix provide the explanation for the enormous range of rock susceptibilities usually encountered.


Materials ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 7037
Author(s):  
Piotr Krysiak ◽  
Aleksander Błachut ◽  
Jerzy Kaleta

This paper analyses the issues relative to the modelling of tubular (cylindrical) composite structures. This paper aims to describe the design of a multi-layer structure of filament-wound composite pipes where, after loading, the hoop-stress distribution would be as uniform as possible. That would allow the mass of the composite to decrease while maintaining the proper mechanical strength. This publication presents the development of a calculation model dedicated to mono- and multi-layered tubular composite structures. The equations describing the stress pattern were based on the Lamé Problem, whereas to describe the modelled structures, an anisotropy coefficient was introduced and interlayer pressures values were determined. To verify the calculations, experimental studies were performed. The test specimens were fabricated by winding fibre bundles around a steel core (as rings with an internal diameter of 113 mm and a height of 30 mm). For the test, the method of pressing a conical ring into a split ring, which acts on the internal surface of the tested cylindrical sample, was selected. The operation of the test rig (test stand) was simulated using the Finite Element Method (FEM). Measurements with strain gauges were conducted during the experiments.


2020 ◽  
Vol 27 (2) ◽  
pp. 472-476
Author(s):  
Mirko Holler ◽  
Johannes Ihli ◽  
Esther H. R. Tsai ◽  
Fabio Nudelman ◽  
Mariana Verezhak ◽  
...  

A simple two-spindle based lathe system for the preparation of cylindrical samples intended for X-ray tomography is presented. The setup can operate at room temperature as well as under cryogenic conditions, allowing the preparation of samples down to 20 and 50 µm in diameter, respectively, within minutes. Case studies are presented involving the preparation of a brittle biomineral brachiopod shell and cryogenically fixed soft brain tissue, and their examination by means of ptychographic X-ray computed tomography reveals the preparation method to be mainly free from causing artefacts. Since this lathe system easily yields near-cylindrical samples ideal for tomography, a usage for a wide variety of otherwise challenging specimens is anticipated, in addition to potential use as a time- and cost-saving tool prior to focused ion-beam milling. Fast sample preparation becomes especially important in relation to shorter measurement times expected in next-generation synchrotron sources.


2021 ◽  
Author(s):  
◽  
Simon Granville

<p>Materials that combine the useful properties of magnetic and semiconducting behaviours are sought for new and developing applications in electronics. In this thesis experimental studies of the properties of disordered thin films of several potentially magnetic semiconducting materials are presented. Previous research on the diluted magnetic semiconductor GaMnN is reviewed as an introduction to a study of GaMnN thin films grown with an ion-assisted deposition technique. Several complementary compositional and structural analysis techniques are used to determine that films can be grown with as much as 18 at. % Mn content and that contain no impurity phases, as are often detected in single crystalline GaMnN preparations with high Mn concentrations. The effects of varying Mn contents on the resistive, optical and magnetic properties of the thin films are investigated. The structural, electronic and magnetic properties of thin films of the potential impurity phase MnN have also been investigated and compared with band structure calculations. Recent predictions that the rare earth nitrides may have extremely useful electronic properties have been almost untested in the literature. A procedure for growing rare earth nitride thin films and capping them to protect from reaction with water vapour allows their resistivity, structural and magnetic properties to be established. The results on GdN, SmN, ErN and DyN support the recent predictions, and a more thorough study on GdN reveals that this material is a ferromagnetic semiconductor below 69 K.</p>


2020 ◽  
pp. 26-32
Author(s):  
A. V. Sandulyak ◽  
◽  
R. Yu. Tkachenko ◽  
A. A. Sandulyak ◽  
V. A. Ershova ◽  
...  

It has been noted that the information on magnetic properties of specific magnets available in the design and operation of magnetic separators/analyzers using magnetic fillers in the form of balls as the working body (polygradient type) is extremely limited, especially for magnets with varying sphericity coefficients (mutual ratios of characteristic sizes). Experiments using cylindrical samples (porous) as a ferromagnetic matrix rendered the induction data subsequently applied to establish the magnetic permeability, susceptibility, and magnetization values for the samples at various values of the length-todiameter ratio of φ = 1–16. The demagnetizing factor N was obtained and analyzed for the «short» samples (1 ≤ φ [φ]) in the range of magnetizing field strengths of 9–47 kA/m, taking into account the established transient value of φ = [φ] = 10–12 (when, at φ ≥ [φ], the magnetic properties of the sample correspond to the magnetic properties of its quasi-solid material). The analysis results for these data, required when assessing the actual magnetic properties of «short» working bodies, characteristic of polygradient magnetic separators/ analyzers, demonstrate the validity of the exponential dependence (decreasing with increasing) of their demagnetizing factor. The research was carried out with the financial support of the Ministry of Education and Science of the Russian Federation within the framework of the State Assignment in the field of science (project No. 0706-2020-0024) and of the Russian Foundation for Basic Research and the Royal Society of London under research project No. 20-52-10006.


1999 ◽  
Vol 577 ◽  
Author(s):  
H.A. Davies ◽  
C.L. Harland ◽  
R.J.I. Betancour ◽  
S.G. Mendoza

ABSTRACTThe magnetic properties of nanophase exchange enhanced RE-Fe-B based alloys ribbons prepared by melt spinning are presented and discussed. The alloy systems investigated include NdyFe94−yB6 and PryFe94−yB6, for y within the range 6-20 at%, and the data are compared in the context of the larger anisotropy field for the Pr2Fe14B phase in comparison with Nd2Fe14B. Experimental studies are also reported for nanophase (Nd-Pr)- Fe-B alloys with various proportions of Nd:Pr, to investigate the increase in coercivity of NdFeB by partial substitution of Nd by Pr, and for (Nd, Pr)-(Fe-Co)-B-based systems, to study the degree to which the remanence enhancement can be maintained for alloys in which Co substitutes for Fe to increase the thermal stability.


2017 ◽  
Vol 31 (09) ◽  
pp. 1750094
Author(s):  
R. Mardani ◽  
M. R. Kazerani ◽  
H. Shahmirzaee

Cobalt-based amorphous alloys, in particular CoFeBSi, have been widely used to study the response of ac-impedance to the external dc magnetic field, i.e., the so-called Giant Magneto Impedance (GMI) effect. The utility of CoFeBSi in different applications such as field-sensitive sensors is known and practiced. Despite the wealth of experimental studies on GMI properties of CoFeBSi alloys, no computational approach has yet been addressed on electronic and magnetic properties of these systems at nanoscales. In this study, we have computed electronic and magnetic properties of amorphous CoFeBSi alloys using a combined Molecular Dynamics (MD) and Density Functional Theory (DFT) approach. MD is used to provide a physically realistic sampling of different atomic configurations while the properties such as dipole moments and magnetic susceptibilities are computed using DFT. Our study shows a wide spectrum of electronic as well as magnetic properties for nanoclusters of different sizes having implications for rational design of Co-based ferromagnetic alloys.


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