Evaluation of initial setting time due to superplasticizers

2017 ◽  
Vol 8 (2) ◽  
pp. 65
Author(s):  
Abhishek Singh ◽  
Shobha Ram ◽  
Alok Verma
Keyword(s):  
Water Content ◽  
Cement Paste ◽  
Setting Time ◽  
Cement Ratio ◽  
Water Cement Ratio ◽  
Initial Setting Time ◽  
Initial Setting

This paper shows how polycarboxylate based superplasticizer affects the initial setting time of cement paste. Three superplasticizers are used in this study with different properties and aiming to determine the delay in initial setting time due to superplasticizer. Initial setting time is calculated as per IS: 4031-PART 5-1988 with different SP dosages (0.5%, 0.75%, 1.0% and 1.5% of weight of cement). Superplasticizer is an admixture which reduces the water-cement ratio or increase the workability at the same water content. This paper deals with the evaluation of initial setting time due to superplasticizers.

Preliminary Study on Reaction of Fresh Concrete with Carbon Dioxide

2018 ◽  
Vol 382 ◽  
pp. 230-234
Author(s):  
Ming Ju Lee ◽  
Ming Gin Lee ◽  
Yung Chih Wang ◽  
Yu Min Su ◽  
Jia Lun Deng
Keyword(s):  
Carbon Dioxide ◽  
Compressive Strength ◽  
Fresh Concrete ◽  
Setting Time ◽  
Cement Matrix ◽  
Cement Ratio ◽  
Water Cement Ratio ◽  
Initial Setting Time ◽  
Initial Setting ◽  
Short Time

In order to let fresh concrete react with carbon dioxide sufficiently, the carbon dioxide was added to mixing concrete. The study used three water cement ratio (0.55, 0.65, 0.75), three CO2 pressures (0.2, 0.4, 0.6 MPa), and two CO2 concentration (50% and 100%) to make concrete samples, and observed the effect of carbon dioxide adsorption in the above parameters. Finally, the compressive strength and carbonation degree of concretes were tested after three curing time (7, 14 and 28 days). The research showed that concrete could be more efficient to absorb carbon dioxide by using this pressure method. The results found that the mixing concrete react with carbon dioxide in a short time, and shorten the initial setting time of concrete. But this method would greatly reduce the workability of concrete after mixing with carbon dioxide and it might be enhanced by water or superplasticizer. The bond of cement matrix might cut down after reacting with carbon dioxide. Based on the above, the compressive strength of concrete which was mixed with carbon dioxide would be impaired. The proposed CO2-mixing method has the capacity to uptake 9.5% carbon dioxide based on water cement ratio and CO2 pressure.

scholarly journals Experimental Study on Fluid Properties of Cement-Fly Ash Slurry Subjected to Multifactors

Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-17
Author(s):  
Tian Huang ◽  
Feng Huang ◽  
Huifeng Zhou
Keyword(s):  
Fly Ash ◽  
Setting Time ◽  
Factors Affecting ◽  
Cement Ratio ◽  
Water Cement Ratio ◽  
Initial Setting Time ◽  
Fluid Properties ◽  
Practical Engineering ◽  
Initial Setting ◽  
The Stability

There are many factors affecting the characteristics of cement-fly ash slurry in practical engineering. Thus, this paper studies the influence of multifactors on the fluid properties of cement-fly ash slurry based on water-cement ratio ( w / c ) (0.75, 1, 1.25, and 1.5), fly ash content (0%, 10%, 20%, 30%, 40%, and 50%) and temperature (20°C, 40°C, 60°C, and 80°C). The bleeding ratio, initial setting time, final setting time, and viscosity were analyzed under coupling conditions. It is found that the water-cement ratio ( w / c ) is the main factor that affects the rheological properties and bleeding rate of slurry. The temperature affects the stability of the slurry in terms that the bleeding ratio of the slurry decreases as the temperature increases. The addition of fly ash enhances the stability of the slurry under different temperature conditions.

scholarly journals Effect of Calcium Nitrate on the Properties of Portland–Limestone Cement-Based Concrete Cured at Low Temperature

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1611
Author(s):  
Gintautas Skripkiūnas ◽  
Asta Kičaitė ◽  
Harald Justnes ◽  
Ina Pundienė
Keyword(s):  
Compressive Strength ◽  
Cement Paste ◽  
Setting Time ◽  
Calcium Nitrate ◽  
Curing Temperature ◽  
Hardened Concrete ◽  
Cement Pastes ◽  
Initial Setting Time ◽  
Initial Setting ◽  
Early Strength

The effect of calcium nitrate (CN) dosages from 0 to 3% (of cement mass) on the properties of fresh cement paste rheology and hardening processes and on the strength of hardened concrete with two types of limestone-blended composite cements (CEM II A-LL 42.5 R and 42.5 N) at different initial (two-day) curing temperatures (−10 °C to +20 °C) is presented. The rheology results showed that a CN dosage up to 1.5% works as a plasticizing admixture, while higher amounts demonstrate the effect of increasing viscosity. At higher CN content, the viscosity growth in normal early strength (N type) cement pastes is much slower than in high early strength (R type) cement pastes. For both cement-type pastes, shortening the initial and final setting times is more effective when using 3% at +5 °C and 0 °C. At these temperatures, the use of 3% CN reduces the initial setting time for high early strength paste by 7.4 and 5.4 times and for normal early strength cement paste by 3.5 and 3.4 times when compared to a CN-free cement paste. The most efficient use of CN is achieved at −5 °C for compressive strength enlargement; a 1% CN dosage ensures the compressive strength of samples at a −5 °C initial curing temperature, with high early strength cement exceeding 3.5 MPa but being less than the required 3.5 MPa in samples with normal early strength cement.

scholarly journals Preparation and Performance of a New-Type Alkali-Free Liquid Accelerator for Shotcrete

2017 ◽  
Vol 2017 ◽  
pp. 1-9
Author(s):  
Yanping Sheng ◽  
Bin Xue ◽  
Haibin Li ◽  
Yunyan Qiao ◽  
Huaxin Chen ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Cement Paste ◽  
Cement Mortar ◽  
Retention Rate ◽  
Setting Time ◽  
Test Results ◽  
Initial Setting Time ◽  
Initial Setting ◽  
New Type ◽  
And Performance

A new type of alkali-free liquid accelerator for shotcrete was prepared. Specifically, the setting time and strength and shrinkage performance of two kinds of Portland cement with the accelerator were fully investigated. Moreover, the accelerating mechanism of alkali-free liquid accelerator and the hydration process of the shotcrete with accelerator were explored. Results show that alkali-free liquid accelerator significantly shortened the setting time of cement paste, where the initial setting time of cement paste with 8 wt% of the accelerator was about 3 min and the final setting time was about 7 min. Compressive strength at 1 day of cement mortar with the accelerator could reach 23.4 MPa, which increased by 36.2% compared to the strength of cement mortar without the accelerator, and the retention rate of 28-day compressive strength reached 110%. In addition, the accelerator still shows a good accelerating effect under low temperature conditions. However, the shrinkage rate of the concrete increased with the amount of the accelerator. 5~8% content of accelerator is recommended for shotcrete in practice. XRD and SEM test results showed that the alkali-free liquid accelerator promoted the formation of ettringite crystals due to the increase of Al3+ and SO42- concentration.

Study on the Early Hydration of Cement Paste Containing Sodium Chloride

2014 ◽  
Vol 621 ◽  
pp. 35-38 ◽  
Author(s):  
Rahimah Embong ◽  
Andri Kusbiantoro
Keyword(s):  
Compressive Strength ◽  
Sodium Chloride ◽  
Cement Paste ◽  
Setting Time ◽  
Chloride Ion ◽  
Strength Development ◽  
Early Hydration ◽  
Initial Setting Time ◽  
Additive Component ◽  
Initial Setting

This paper studies the effect of sodium chloride as the additive component in cement paste. Sodium chloride was included at 0.5%, 1%, 1.5%, and 2% by weight of cement content. Analysis on the performance of this reagent was conducted via setting time, compressive strength, and porosity test. Based on the setting time analysis, the inclusion of sodium chloride can extend the initial setting time of cement paste up to 24.91% longer than control specimen. Obstruction on the formation of calcium silicate hydrate gel by sodium and chloride ion was one of the possible causes to this phenomenon. Acceleration on the compressive strength development by sodium chloride was also detected. It appears that sodium chloride was able to de-flocculate the coagulated cement particles and reduced the viscosities of cement slurries; hence resulted in faster early hydration process.

scholarly journals Compressive Strength of Concrete with Nano Cement

2021 ◽  
Author(s):  
Jemimah Carmichael Milton ◽  
Prince Arulraj Gnanaraj
Keyword(s):  
Compressive Strength ◽  
Specific Surface ◽  
Surface Area ◽  
Specific Surface Area ◽  
Cement Paste ◽  
Cement Mortar ◽  
Setting Time ◽  
Replacement Level ◽  
Initial Setting Time ◽  
Initial Setting

Nano technology plays a very vital role in all the areas of research. The incorporation of nano materials in concrete offers many advantages and improves the workability, the strength and durability properties of concrete. In this study an attempt has been made to carry out an experimental investigation on concrete in which cement was replaced with nano sized cement. Ordinary Portland cement of 53 grade was ground in a ball grinding mill to produce nano cement. The characterization of nano cement was studied using Scanning Electron Microscope (SEM), Brunauer Emmett–Teller (BET), Energy Dispersive X ray microanalysis (EDAX) and Fourier Transform Infrared Spectroscopy (FTIR). From the characterization studies, it was confirmed that particles were converted to nano size, the specific surface area increased and the chemical composition remained almost the same. The properties of cement paste with and without nano cement were found. For the experimental study, cement was replaced with 10%, 20%, 30%, 40% and 50% of nano cement. Cement mortar of ratio 1:3 and concrete of grades M20, M30, M40 and M50 were used. Compressive strength of cement mortar and concrete with different percentages of nano cement was found. The cement mortar was also subjected to micro structural study. It was found that the strength increased even up to the replacement level of 50%. Further increase in the replacement is not possible since the addition of nano cement reduces the initial and final setting time of cement paste. At 50% replacement level, the initial setting time got reduced to 30 minutes which the least permitted value as per IS 12269: 2013. The increase in strength was due to the fact that nano cement acts not only as a filler material but also the reactivity increased due to the higher specific surface area. The SEM image shows the formation of additional C-S-H gel. The percentage increase in compressive strength was found to increase up to 32%. The workability of concrete with nano cement was found to be significantly more than that of the normal cement concrete.

The Influence of Alcohol Amine Admixtures on the Macroscopic Properties of Portland Cement Paste

2014 ◽  
Vol 525 ◽  
pp. 573-579
Author(s):  
Tian Yong Huang ◽  
Dong Min Wang ◽  
Ze Liu
Keyword(s):  
Compressive Strength ◽  
Flexural Strength ◽  
Portland Cement ◽  
Cement Paste ◽  
Setting Time ◽  
Initial Setting Time ◽  
Final Setting Time ◽  
Cement Mortars ◽  
Macroscopic Properties ◽  
Initial Setting

It is studied the influence of triethanolamine (TEA), diethylenetriamine (DEA), Triisopropanolamine (TIPA), aminoethyl ethanolamine (AE), and polyvinyl alcohol ammonium phosphate (PAAP) at different dosages on the properties of fresh and hardened cement pastes and mortars prepared by Portland cement, including standard consistency water, setting time, the cement paste fluidity, and compressive and flexural strength. It is showed that the high polarity alcohol amine molecules exhibit strong chemical interactions with cement matrix, which are reflected in modified macroscopic properties of the cement system. All alcohol amine admixtures increased the standard consistency water and decreased cement paste fluidity of Portland cement. TEA significantly shortened the initial setting time and final setting time of Portland cement. On the other hand, TIPA, DEA, AE and PAAP extended the initial setting time of cement but shortened the cement final setting time. All alcohol amine admixtures except TIPA at 0.2 and 0.5 dosage increased the compressive and flexural strength of the Portland cement mortars at 3 days. Especially when the dosage of PAAP is 1, the compressive strength of the Portland cement mortars at 3 days is increased 10.5MPa. All alcohol amine admixtures except AE at 0.2 and 0.5 dosage increase the compressive and flexural strength of the Portland cement mortars at 28 days, Especially when the dosage of TIPA is 1, the compressive strength of the Portland cement mortars at 28 days is increased 8.8MPa.

scholarly journals Non-Dispersive Anti-Washout Grout Design Based on Geotechnical Experimentation for Application in Subsidence-Prone Underwater Karstic Formations

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1587
Author(s):  
Khaqan Baluch ◽  
Sher Q Baluch ◽  
Hyung-Sik Yang ◽  
Jung-Gyu Kim ◽  
Jong-Gwan Kim ◽  
...  
Keyword(s):  
Fractured Rock ◽  
Setting Time ◽  
Visual Assessment ◽  
Initial Setting Time ◽  
Permeable Sediments ◽  
Coarse Aggregates ◽  
Saturated Rock ◽  
Initial Setting ◽  
Level 3 ◽  
Grey Relational

A new non-dispersive, anti-washout grout consisting of ordinary Portland cement, slag, superplasticizer, and methylbenzyl cellulose is proposed herein for the treatment of open karst, jointed and fractured rock, open-work gravel, and permeable sediments. A series of laboratory experiments were performed to design an anti-wash out grout suitable for grout injection of coarse aggregates depicting partially and open-jointed saturated rock mass and grouting concrete aggregates for underwater construction. The Taguchi orthogonal array was used to obtain nine different grout mix ratios. A total of four variables were considered, each with three different levels of the water–cement ratio, slag, and dosage of additives such as the superplasticizer and methyl benzyl cellulose. The laboratory determination of grout characteristics recording of mini slump, temperature, pH, visual assessment of grout dispersion, bleeding, and initial setting time and as well as uniaxial compressive strengths and permeabilities of the hardened grout samples were tested. To evaluate the suitability of the grout mixes, an analysis of variance was used for factor analysis and Grey relational analysis (GRA) was used to determine the optimal grout mix design. Based on the GRA, the following levels of the factors afforded the best results: water level 1 (0.3%), SP level 3 (0.01%), methylbenzyl cellulose level 2 (0.002%), and slag level 3 (0.1%). This paper describes the research methodology, detailed research observations, and analyses involved in designing the appropriate concrete mix. Based on the conclusions, relevant commendations regarding the suitability of grout testing equipment and grout mix designs are presented.

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