scholarly journals Cold plasma enamel surface treatment to increase fluoride varnish uptake

2021 ◽  
Author(s):  
S. Fathollah ◽  
H. Abbasi ◽  
S. Akhoundi ◽  
A. Naeimabadi ◽  
S. Emamjome
Keyword(s):  
Cold Plasma ◽  
Tooth Enamel ◽  
Enamel Surface ◽  
Fluoride Varnish ◽  
Sodium Absorption ◽  
Tooth Decay ◽  
Fluoride Ions ◽  
Sem Images ◽  
X Ray ◽  
Group A

Abstract Enamel strengthening to prevent the first stage of caries has been an essential issue in oral health recently. Among the available methods to increase enamel strength, fluoride varnish treatment has relatively better results in preventing tooth decay. Cold plasma capabilities in sterilizing the environment, surface modification, and improving adhesion are well known. Accordingly, this study aims to increase the enamel layer's adhesion hoping that the intensity and time of enamel interaction with FV and the absorption of fluoride ions will increase. Accordingly, we randomly divided twenty bovine teeth into two groups A (consisting of four teeth) and B (composed of four subgroups, each containing four teeth). Samples of group A and one specimen of each subset B investigate the effect of using Helium-DBD (He-DBDJ), Argon (ArJ), and Air-DBD jet on the enamel surface. Other B specimens are devoted to the study of the release of FV fluoride ions from processed enamel. The scanning electron microscope (SEM) images show that although ArJ and Air-DBD have significantly damaged the enamel's hexagonal structures, they are only changed from convex to concave in the He-DBDJ case. For this reason, enamel effectively enhances the capacity to accept more FV. The energy-dispersive X-ray spectroscopy (EDX) indicates an increase in calcium ratio to phosphorus and the amount of fluoride and sodium absorption in the enamel layer in processing with He-DBDJ plasma. The latter helps restore the damaged parts of the enamel. Analysis of fluoride released from the FV did not show a significant change owing to plasma processing. The combination of Cold plasma and varnish fluoride on treatment enamel could be unique ability to improve reinforcement of tooth enamel against of tooth decay.

scholarly journals Influence of different types of whitening tooth pastes on the tooth color, enamel surface roughness and enamel morphology of human teeth

F1000Research ◽  
2019 ◽  
Vol 8 ◽  
pp. 1764
Author(s):  
Mohamed Shamel ◽  
Mahmoud M. Al-Ankily ◽  
Mahmoud M. Bakr
Keyword(s):  
Surface Roughness ◽  
Tooth Enamel ◽  
Morphological Changes ◽  
Enamel Surface ◽  
Tooth Surface ◽  
Tooth Whitening ◽  
Sem Images ◽  
Human Teeth ◽  
Tooth Color ◽  
Different Types

Background: Tooth whitening usually includes the direct use of gels containing carbamide or hydrogen peroxide on the tooth enamel surface through a wide variety of products formulas. A generally new advancement in whitening of teeth uses the significant importance of the tooth color shift from yellow to blue in delivering a general enhancement in the observation of tooth whiteness. The aim of the current work was to measure the tooth whitening effects, surface roughness and enamel morphology of six different types of blue covarine-containing and blue covarine-free toothpastes using in vitro models. Methods: A total of 70 sound extracted human premolars were randomly and equally divided into seven groups, and each subjected to tooth brushing using different toothpastes. Tooth color and enamel surface roughness were measured before and after the brushing procedure using a white light interferometer, and scanning electron microscopy (SEM) was used to assess tooth surface after the procedure. Results: Toothpaste containing blue covarine resulted in the greatest improvement in tooth color amongst all groups as well as a statistically significant color difference when compared to blue covarine-free toothpaste.  Furthermore, blue covarine-containing toothpaste resulted in fewer morphological changes to the enamel surface. This was confirmed with SEM images that showed smooth enamel surfaces with fine scratches.   Conclusions: The results from the present study show that blue covarine containing toothpastes are reliable, effective in tooth whitening and produce less surface abrasion when compared to blue covarine-free toothpastes.

Remineralization of Natural Tooth Enamel in Artificial Saliva Environment

2017 ◽  
Vol 68 (3) ◽  
pp. 510-514 ◽  
Author(s):  
Agripina Zaharia ◽  
Viorica Ghisman Plescan ◽  
Irina Atkinson ◽  
Oana Catalina Mocioiu ◽  
Alina Cantaragiu ◽  
...  
Keyword(s):  
Tooth Enamel ◽  
Artificial Saliva ◽  
Dental Enamel ◽  
Hexagonal Structure ◽  
Enamel Surface ◽  
Enamel Matrix Derivative ◽  
Phosphate Solution ◽  
X Ray ◽  
Composition And Structure ◽  
Demineralized Enamel

This paper investigates in situ remineralization of the acid-etched natural enamel surface, by incubation in a phosphate solution with neutral pH, at 37 �C for 4-10 days, without using any enamel matrix derivative (EMD). We investigated the morphology, crystallinity, chemical composition and structure of the newly grown layer onto the natural enamel surface stored in contact with artificial saliva (AS) having a composition similar to natural oral environment. The crystalline phases, crystallite size and orientation, as well as the chemical and phase composition of the remineralized dental enamel samples were studied by scanning electron microscopy coupled with energy dispersive X-ray spectrometry, Fourier transform infrared spectroscopy and X-ray diffraction. The experimental results showed that the enamel crystals grown on the demineralized enamel surface are mainly Ca-deficient apatite hexagonal structure. Fluoridated hydroxyapatite and sylvite-type KCl crystallites, which amount considerable increased in the case of sample stored in AS for 10 days, were also identified.

scholarly journals Surface Enamel Remineralization: Biomimetic Apatite Nanocrystals and Fluoride Ions Different Effects

2009 ◽  
Vol 2009 ◽  
pp. 1-9 ◽  
Author(s):  
Norberto Roveri ◽  
Elisa Battistella ◽  
Claudia Letizia Bianchi ◽  
Ismaela Foltran ◽  
Elisabetta Foresti ◽  
...  
Keyword(s):  
Tooth Enamel ◽  
Acid Resistance ◽  
Enamel Surface ◽  
Fluoride Ions ◽  
Crystallinity Degree ◽  
Carbonate Hydroxyapatite ◽  
Apatite Crystals ◽  
Biomimetic Apatite ◽  
Enamel Structure ◽  
Hydroxyapatite Nanocrystals

A new method for altered enamel surface remineralization has been proposed. To this aim carbonate-hydroxyapatite nanocrystals which mimic for composition, structure, nanodimensions, and morphology dentine apatite crystals and resemble closely natural apatite chemical-physical properties have been used. The results underline the differences induced by the use of fluoride ions and hydroxyapatite nanocrystals in contrasting the mechanical abrasions and acid attacks to which tooth enamel is exposed. Fluoride ions generate a surface modification of the natural enamel apatite crystals increasing their crystallinity degree and relative mechanical and acid resistance. On the other hand, the remineralization produced by carbonate-hydroxyapatite consists in a deposition of a new apatitic mineral into the eroded enamel surface scratches. A new biomimetic mineral coating, which progressively fills and shadows surface scratches, covers and safeguards the enamel structure by contrasting the acid and bacteria attacks.

scholarly journals PERBEDAAN KEKERASAN PERMUKAAN ENAMEL SETELAH APLIKASI FLUORIDE VARNISH DAN CASEIN PHOSPO PEPTIDE-AMORPHOUS CALSIUM PHOSPHATE FLUORIDE (CPP-ACPF) (PENELITIAN IN VITRO)

2019 ◽  
Vol 7 (2) ◽  
pp. 130
Author(s):  
Sinta Puspita ◽  
Adioro Soetojo ◽  
Sri Kunarti
Keyword(s):  
Tooth Enamel ◽  
Surface Hardness ◽  
Enamel Surface ◽  
Fluoride Varnish ◽  
Initial Surface ◽  
Surface Microhardness ◽  
Demineralized Enamel ◽  
Group 3 ◽  
Group 2 ◽  
Group 1

Background: Caries is a chronic, slowly progressing disease, with symptoms not detected at the onset of the disease but generally much later. Its initiation is associated with demineralization (calcium and phosphate loss) of subsurface tooth enamel, resulting in the formation of a subsurface lesion. To restore the natural equilibrium, either remineralization must be enhanced or demineralization must be retarded. There are some topical agents that can enhance remineralization such as topical fluor and casein phosphopeptide – amorphous calcium phosphate (CPP-ACP). Purpose: The aim of this study is to analyze the differences of the enamel surface microhardness after application of fluoride varnish and CPP-ACPF. Methode: 27 blocks bovine enamel were devided into 3 groups. Group 1 – control (No surface treatment), group 2 – fluoride varnish and group 3 – CPP-ACPF. Initial surface hardness enamel was measured for all enamel specimens. Artificial enamel carious lesions were created by immersing enamel samples to demineralization solution (pH 4,5) for 72 hours at temperature 370 C. The surface microhardness of demineralized enamel specimens was measured. A caries progression test (pH cycling) was carried out, which consisted of alternative demineralization (3 hours), remineralization with artificial saliva (21 hours) and application topical agent twice a day for 14 days. Then, the last surface enamel microhardness is measured. Result: Group 3 showed significantly highest Vickers hardness number (P<0,05) followed by group 2 and the lowest is group 1. Conclusions: This study proved that enamel surface microhardness after application of CPP-ACPF was higher than fluoride varnish.

Mosaic Mapping: A Means of Tiling Images to Shorten Acquisition Speed for Lower - Magnification SEM Images and Wavelength Dispersive Spectrometers (WDS) X-Ray Maps

1996 ◽  
Vol 54 ◽  
pp. 438-439
Author(s):  
J.D. Geller ◽  
C.R. Herrington
Keyword(s):  
Limiting Factors ◽  
X Rays ◽  
Angular Range ◽  
Acceptance Angle ◽  
Sem Images ◽  
Worst Case ◽  
X Ray ◽  
Focusing Distance ◽  
Layered Crystals ◽  
Working Distance

The minimum magnification for which an image can be acquired is determined by the design and implementation of the electron optical column and the scanning and display electronics. It is also a function of the working distance and, possibly, the accelerating voltage. For secondary and backscattered electron images there are usually no other limiting factors. However, for x-ray maps there are further considerations. The energy-dispersive x-ray spectrometers (EDS) have a much larger solid angle of detection that for WDS. They also do not suffer from Bragg’s Law focusing effects which limit the angular range and focusing distance from the diffracting crystal. In practical terms EDS maps can be acquired at the lowest magnification of the SEM, assuming the collimator does not cutoff the x-ray signal. For WDS the focusing properties of the crystal limits the angular range of acceptance of the incident x-radiation. The range is dependent upon the 2d spacing of the crystal, with the acceptance angle increasing with 2d spacing. The natural line width of the x-ray also plays a role. For the metal layered crystals used to diffract soft x-rays, such as Be - O, the minimum magnification is approximately 100X. In the worst case, for the LEF crystal which diffracts Ti - Zn, ˜1000X is the minimum.

In vitro Evaluation of Enamel Surface Treated with Fluoride After Bleaching and Etching Erosive Processes

2018 ◽  
Vol 69 (7) ◽  
pp. 1714-1717
Author(s):  
Roxana Ionela Vasluianu ◽  
Norina Consuela Forna ◽  
Elena Raluca Baciu ◽  
Mirela Zaltariov ◽  
Lavinia Vasiliu ◽  
...  
Keyword(s):  
Enamel Surface ◽  
Spectroscopy Analysis ◽  
X Ray ◽  
Fluoride Treatment ◽  
Enamel Structure ◽  
Erosion Effect ◽  
Enamel Composition ◽  
Morphology Changes ◽  
Scanning Electron

The anti-erosion effect of fluoride on the enamel surface was investigated by ATR-FTIR, SEM and EDX techniques. Four extracted teeth (two incisors and two premolars) were initially bleached with carabamide peroxide and etched with ortho-phosphoric acid then fluoride treatment was applied. Significant differences in enamel composition and morphology were observed providing the effect of fluoride application in remineralization of teeth. Infrared spectroscopy was employed to probe the changes in enamel structure. Scanning electron microscopy/energy dispersive X-ray spectroscopy analysis revealed higher content in F of teeth enamel. Morphology changes revealed a re-mineralization of enamel surface after the treatment with fluoride gel.

Evaluating of oral and salivary conditions of two specific groups of workers

RSBO ◽  
2016 ◽  
Vol 12 (1) ◽  
pp. 50
Author(s):  
Eduardo Pizzatto ◽  
Nicolae Carvalho de Paula ◽  
Carolina Dea Bruzamolin ◽  
Paulo H. Tomazinho ◽  
Luciane Variani Pizzatto ◽  
...  
Keyword(s):  
Oral Microbiota ◽  
Tooth Decay ◽  
Oral Diseases ◽  
Industrial Countries ◽  
Group A ◽  
Dmft Index ◽  
Saliva Collection ◽  
The Mean ◽  
Group B ◽  
Lactobacillus Spp

Introduction and Objective: Tooth decay is one of the most common chronic oral diseases found in industrial countries and is a multifactorial disease which has sugar as a key dietary factor. The amount of saliva concentration and presence of cariogenic bacteria will favor the development of caries. Because of this, the aim of this study was to collect and analyze data on oral alterations referred to tooth decay, oral pH changes, and changes of the oral microbiota in two distinct groups of workers. Material and methods: 30 individuals belonging to two different groups of workers: group A (GA) – workers who maintain daily contact with the confectionery; group B (GB) – workers who do not have such contact. Saliva collection was done by analysis of the salivary pH in both groups, as well as cultivation of Lactobacillus spp and S. mutans. We also evaluate the dental status of individuals belonging to the two groups through the DMFT index. Results: After the examinations of 30 workers (17 from the GA [9 men and 8 women] and 13 in the GB [7 men and 6 women]), the mean DMFT of the individuals in the group A and group B, was 7.41 (SD 5.14) 7.08 (SD 5.56), respectively, without statistically significant differences (p < 0.05). The count of S. mutans and Lactobacillus spp, was not statistically significant. Conclusion: There was no statistically significant relationship between presence of dental caries and the fact that workers are in contact with sugar because they work on candy food industry, but new studies are needed for more precise research.

scholarly journals Hydrochloric Acid Modification and Lead Removal Studies on Naturally Occurring Zeolites from Nevada, New Mexico, and Arizona

Processes ◽  
2021 ◽  
Vol 9 (7) ◽  
pp. 1238
Author(s):  
Garven M. Huntley ◽  
Rudy L. Luck ◽  
Michael E. Mullins ◽  
Nick K. Newberry
Keyword(s):  
New Mexico ◽  
Surface Area ◽  
Bet Surface Area ◽  
Lead Removal ◽  
X Ray Diffraction ◽  
Sem Images ◽  
X Ray ◽  
Naturally Occurring ◽  
27Al Mas Nmr ◽  
Modified Zeolites

Four naturally occurring zeolites were examined to verify their assignments as chabazites AZLB-Ca and AZLB-Na (Bowie, Arizona) and clinoptilolites NM-Ca (Winston, New Mexico) and NV-Na (Ash Meadows, Nevada). Based on powder X-ray diffraction, NM-Ca was discovered to be mostly quartz with some clinoptilolite residues. Treatment with concentrated HCl (12.1 M) acid resulted in AZLB-Ca and AZLB-Na, the chabazite-like species, becoming amorphous, as confirmed by powder X-ray diffraction. In contrast, NM-Ca and NV-Na, which are clinoptilolite-like species, withstood boiling in concentrated HCl acid. This treatment removes calcium, magnesium, sodium, potassium, aluminum, and iron atoms or ions from the framework while leaving the silicon framework intact as confirmed via X-ray fluorescence and diffraction. SEM images on calcined and HCl treated NV-Na were obtained. BET surface area analysis confirmed an increase in surface area for the two zeolites after treatment, NM-Ca 20.0(1) to 111(4) m2/g and NV-Na 19.0(4) to 158(7) m2/g. 29Si and 27Al MAS NMR were performed on the natural and treated NV-Na zeolite, and the data for the natural NV-Na zeolite suggested a Si:Al ratio of 4.33 similar to that determined by X-Ray fluorescence of 4.55. Removal of lead ions from solution decreased from the native NM-Ca, 0.27(14), NV-Na, 1.50(17) meq/g compared to the modified zeolites, 30 min HCl treated NM-Ca 0.06(9) and NV-Na, 0.41(23) meq/g, and also decreased upon K+ ion pretreatment in the HCl modified zeolites.

scholarly journals Toxicity and Biological Effects of Beauveria brongniartii Fe0 Nanoparticles against Spodoptera litura (Fabricius)

Insects ◽  
2020 ◽  
Vol 11 (12) ◽  
pp. 895
Author(s):  
Jing Xu ◽  
Kaihui Zhang ◽  
Andrew G. S. Cuthbertson ◽  
Cailian Du ◽  
Shaukat Ali
Keyword(s):  
Spodoptera Litura ◽  
Insect Pests ◽  
Growth Parameters ◽  
Uv Spectroscopy ◽  
Biological Effects ◽  
Fungal Treatment ◽  
Beauveria Brongniartii ◽  
Sem Images ◽  
X Ray ◽  
Infection Period

Nanotechnology has clear potential in the development of innovative insecticidal products for the biorational management of major insect pests. Metal-based nanoparticles of different microbial pest control agents have been effective against several pests. Synthesis of Beauveria brongniartii based Fe0 nanoparticles (Fe0NPs) and their bio-efficacy against Spodoptera litura was observed during this study. Beauveria brongniartii conidia were coated with Fe0NPs and characterized by applying a selection of different analytical techniques. Ultraviolet (UV) spectroscopy showed the characteristic band of surface plasmon at 430 nm; Scanning electron microscopy (SEM) images showed spherical shaped nanoparticles with a size ranging between 0.41 to 0.80 µm; Energy-dispersive X-ray (EDX) spectral analysis revealed characteristic Fe peaks at 6.5 and 7.1 Kev; the X-ray diffractogram showed three strong peaks at 2θ values of 45.72°, 64.47°, and 84.05°. The bioassay studies demonstrated that mortality of 2nd instar S. litura larvae following Fe0NPs treatment increased with increasing concentrations of Fe0NPs at different time intervals. The median lethal concentration (LC50) values of Fe0NPs against S. litura after seven days of fungal treatment was 59 ppm, whereas median survival time (LT50) values for 200 and 500 ppm concentrations of Fe0NPs against S. litura seven days post-treatment were 5.1 and 2.29 days, respectively. Beauveria brongniartii-Fe0NPs caused significant reductions in feeding and growth parameters (relative growth rate, relative consumption rate, and efficiency of conversion of ingested food) of S. litura. Beauveria brongniartii Fe0NPs induced reduction in glutathione-S-transferase activities throughout the infection period whereas activities of antioxidant enzymes decreased during later periods of infection. These findings suggest that B. brongniartii Fe0NPs can potentially be used in biorational S. litura management programs.

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