The wet FGD system with the characteristics of stable and mature, which had been widely used in the large thermal power plants. In this system, spray nozzle plays a key role, and the atomization performance of the spray nozzle affects the desulfurization reaction rate and efficiency directly. A new type spray nozzle, liquid beset gas nozzle was came up with in this article. It makes use of compressed gas in the internal pipeline to crush the liquid flowed out of the external pipeline into small particles. To optimize the nozzle's structure and develop its atomization performance, then considered outlet diameters of nozzle as one of the main influencing factors, sets three outlet diameters of nozzles: 4mm, 5mm and 6mm. This experiment with water for medium uses a laser particle size analyzer and a high speed camera for analysis to take atomization performance's tests of liquid beset gas nozzles under different outlet diameters and working conditions. The results of experimental studies were concluded. Firstly, when the outlet diameter is 5mm, the total spraying performance was the best. Because this outlet diameter can make the nozzle be in a balance between effective crush, fully mixing and jams preventing. Secondly, the new type nozzle had certain adaptability, when working pressures changed, and can be widely used in the wet FGD system.