The control of material surface condition for plasma technology to fabricate advanced packaging

Author(s):  
Daisuke Hironiwa ◽  
Yasuhiro Morikawa ◽  
Tsuyoshi Kagami ◽  
Takashi Kurimoto ◽  
Kazumasa Horita ◽  
...  
2010 ◽  
Vol 158 (4) ◽  
pp. 84-99
Author(s):  
Leszek DZICZKOWSKI ◽  
Andrzej BUCHACZ

As the relationship between some important parameters of materials and their electric conductivity really exists, it makes it possible to use the eddy current method to measure conductivity of material in a non-destructive manner and then infer about the desired properties of materials, their continuous or non-continuous structure or some geometrical parameters. However, the substantial impact of surface condition demonstrated by examined materials onto test results is a significant drawback of the eddy current method. This is why, a new and innovative method for compensation of material surface roughness onto results of conductance measurements is proposed. The presented method is based on the double calibration process applied to the measuring kit of the conductometer and the measuring probe.


2013 ◽  
Vol 212 ◽  
pp. 45-48 ◽  
Author(s):  
Anna J. Dolata ◽  
Jakub Wieczorek

In manufacturing of air compressors, piston engines and guides, lubricants are used to result in formation of a continuous oil film that separates the friction surfaces. The continuity of this film within the entire operating range of the friction pair, from starting to steady state, is the guarantee of proper operation. The surface geometry of friction elements plays significant role in maintaining continuity of the oil film. The widely used method for obtaining proper surface condition of the structural components of piston systems is the honing process. This method consists of shaping the microgeometry of the surface of friction pair elements by material removal processing methods (turning, grinding, laser processing) to prevent rapid spreading of lubricant, and thus to prevent breaking of the oil film. In case of Al-MMCs using for manufacturing the parts of machines working under friction with lubrication conditions the shaping of their working surface by honing is limited by the machining efficiency. The investigations on surface geometry of elements made of composites including ceramic reinforcement revealed that presence of reinforcement particles on the working surface bring the changes which can be used for shaping the correct oil film. The investigations presented in this article can be used for evaluation of lubricant propagation process on the composite material surface.


1969 ◽  
Vol 91 (4) ◽  
pp. 785-791 ◽  
Author(s):  
L. H. Kirschler ◽  
R. C. Andrews

The mechanical properties of 316 stainless steel were measured at room temperature and at 1200 F during exposure to environments of air, helium and “clean” sodium. The test results were: Test: Cyclic strain / Environment: Air - Least cycles to failure; Environment: Helium - Most cycles to failure; Environment: Sodium - Between air and helium values. Test: Rupture / Environment: Air/Helium - No significant difference in rupture strenth; Environment: Sodium - Possible increase in ductility compared to air. Test: Creep / Environment: Air - Lowest rate; Environment: Helium - Highest rate; Environment: Sodium - Between air and helium values. Test: Tensile / Environment: Air/Helium/Sodium - 5 percent or less difference in tensile strength; 6 percent or less difference in yield strength. The small changes seen in the rupture, creep, and tensile tests, due to different environments, are considered insignificant when compared to overall variations between heats of stainless steel. The differences seen in cyclic strain tests reflect changes in material surface condition produced by environment.


2007 ◽  
Vol 361-363 ◽  
pp. 755-758
Author(s):  
Junji Ikeda ◽  
Fumiaki Miyaji ◽  
Masaru Ueno ◽  
Giuseppe Pezzotti

Phase stability of 3 mol% yttria stabilized polycrystalline zirconia ceramics (3Y-TZP) was evaluated by aging test in water vapor environment and Raman spectroscopic technique. In our previous study, it has been confirmed that phase stability was improved by controlling sintering temperature. In this study, we pointed our attention and evaluated the influence of surface conditions related to machining and to heat treatment, thus monitoring the changes in phase transformation fraction and residual stress on the material surface. From the results of aging test, an increase in monoclinic fraction was observed for grinded surfaces as compared with polished surfaces. Samples subjected to heat treatment after machining showed improved phase stability. A Vickers indentation print was also introduced on a 3Y-TZP surface, and the relationship between surface condition and low temperature aging was evaluated in the neighborhood of the print. We found that the residual stress fields induced in phase-transformed areas were enhanced during low temperature aging, and that phase stability was improved by heat treatment.


2004 ◽  
Vol 58 (2) ◽  
pp. 55-63
Author(s):  
Maja Radetic ◽  
Zoran Petrovic

Plasma treatment is based on the physico-chemical changes of the material surface and as an ecologically and economically acceptable process it can be an attractive alternative to conventional modifications. The possibilities of plasma technology application to the modification of polymer and textile materials are discussed. Different specific properties of the material can be achieved by plasma cleaning, etching, functionalization or polymerization. The final effects are strongly influenced by the treatment parameters (treatment time, pressure, power, gas flow), the applied gas and nature of the material. The plasma treatment of polymers is predominantly focused on cleaning and activation of the surfaces to increase adhesion, binding, wettability, dye ability and printability. Current studies deal more with plasma polymerization where an ultra thin film of plasma polymer is deposited on the material surface and, depending on the applied monomer, different specific properties can be obtained (i.e. chemical and thermal resistance, abrasion resistance, antireflexion, water repellence, etc.). Plasma application to textiles is mostly oriented toward wool and synthetic fibres, though some studies also consider cotton, hemp, flax and silk. The main goal of plasma treatment is to impart a more hydrophilic fibre surface and accordingly increase wettability, dye ability, printability and particularly, shrink resistance in the case of wool. Recent studies have favored technical textiles, where plasma polymerization can offer a wide range of opportunities.


2013 ◽  
Vol 303-306 ◽  
pp. 2704-2707
Author(s):  
Kai Way Li ◽  
Chan Chi Lin

A laboratory study was conducted to measure the coefficient of friction between the foot and the floor under three surface and two foot sliding speed conditions. A force platform was adopted to measure the ground reaction force (GRF) of the foot on the floor. The coefficient of friction was calculated as the ratio of vertical and horizontal GRF. Five male subjects were recruited. They were requested to slide their right foot on the tested floor which was mounted on the force platform. The results indicated that floor material, surface condition, and foot sliding speed were all significant factor affecting the COF. Ceramic tile had lower COF under all surface and sliding speed conditions as compared to steel, wood, and vinyl tiles.


Author(s):  
J. M. Walsh ◽  
J. C. Whittles ◽  
B. H. Kear ◽  
E. M. Breinan

Conventionally cast γ’ precipitation hardened nickel-base superalloys possess well-defined dendritic structures and normally exhibit pronounced segregation. Splat quenched, or rapidly solidified alloys, on the other hand, show little or no evidence for phase decomposition and markedly reduced segregation. In what follows, it is shown that comparable results have been obtained in superalloys processed by the LASERGLAZE™ method.In laser glazing, a sharply focused laser beam is traversed across the material surface at a rate that induces surface localized melting, while avoiding significant surface vaporization. Under these conditions, computations of the average cooling rate can be made with confidence, since intimate contact between the melt and the self-substrate ensures that the heat transfer coefficient is reproducibly constant (h=∞ for perfect contact) in contrast to the variable h characteristic of splat quenching. Results of such computations for pure nickel are presented in Fig. 1, which shows that there is a maximum cooling rate for a given absorbed power density, corresponding to the limiting case in which melt depth approaches zero.


Author(s):  
P. A. Molian ◽  
K. H. Khan ◽  
W. E. Wood

In recent years, the effects of chromium on the transformation characteristics of pure iron and the structures produced thereby have been extensively studied as a function of cooling rate. In this paper, we present TEM observations made on specimens of Fe-10% Cr and Fe-20% Cr alloys produced through laser surface alloying process with an estimated cooling rate of 8.8 x 104°C/sec. These two chromium levels were selected in order to study their phase transformation characteristics which are dissimilar in the two cases as predicted by the constitution diagram. Pure iron (C<0.01%, Si<0.01%, Mn<0.01%, S=0.003%, P=0.008%) was electrodeposited with chromium to the thicknesses of 40 and 70μm and then vacuum degassed at 400°F to remove the hydrogen formed during electroplating. Laser surface alloying of chromium into the iron substrate was then performed employing a continuous wave CO2 laser operated at an incident power of 1200 watts. The laser beam, defocussed to a spot diameter of 0.25mm, scanned the material surface at a rate of 30mm/sec, (70 ipm).


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