scholarly journals The Filler Effect on Compressive Strength of Sulfur Concrete

2021 ◽  
Vol 2 (1) ◽  
Author(s):  
Wenwei Lin ◽  
Fan Fei ◽  
Qunjie Li
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Fly Ash ◽  
Scanning Electron Microscope ◽  
Chemical Reaction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Compressive Performance ◽  
Bonding Mode ◽  
Scanning Electron

The sulfur concrete samples were prepared by the optimized process, which were mixed with cement, fly ash and slag, respectively. The influence of the type and content of filler on the compressive strength of sulfur concrete was studied. The phase and micromorphology of filler and sulfur mixture were characterized by X-ray diffraction and scanning electron microscope, and the bonding mode was studied. The results show: the cement filler has the best effect on the compressive performance of sulfur concrete,and the compressive strength is 87.2 MPa by adding cement filler with the same quality as sulfur; there is no chemical reaction between filler and sulfur, and the filler is physically bonded to sulfur matrix.

Test Research on Preparation of New Wall Material with Iron Tailings in Tangshan Area

2011 ◽  
Vol 295-297 ◽  
pp. 535-538
Author(s):  
De Qing Gan ◽  
Chao Chen ◽  
Jin Xia Zhang
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Fly Ash ◽  
Wall Material ◽  
X Ray Diffraction ◽  
Steam Curing ◽  
X Ray ◽  
A New Technique ◽  
Scanning Electron

This paper discussed the experimental resuhs of exploiting brick materials with iron tailing materials in Tanshang area. Through preparation of iron tailing bricks, the technical flow and production proportion was obtained. The results show that a burning-and steam curing-free brick product with a compressive strength of 28.30 MPa and Flexural strength of 5.63 MPa as the following: iron tailing; fly ash; sand; CaO; gypsum; cement. And long-term properties of a burning-and steam curing-flee brick is also studied by experiments in this paper. Put forward a new technique of making materials with iron tailing. At the same time, the micro mechanism of iron tailing brick was also studied with X-Ray Diffraction (XRD) and Scanning Electron Microscope(SEM).

scholarly journals The Formation of Local Catalyst from Zeolite, Characterization and Performance in the Reaction

2020 ◽  
Vol 846 ◽  
pp. 257-261
Author(s):  
Zahrul Mufrodi ◽  
Erna Astuti ◽  
Gita Indah Budiarti
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Chemical Reaction ◽  
Natural Zeolite ◽  
X Ray Diffraction ◽  
Glycerol Conversion ◽  
Catalyst Synthesis ◽  
X Ray ◽  
And Performance ◽  
Scanning Electron

The existance of catalyst in a chemical reaction is very important. This catalyst can accelerate the chemical reaction. Currently there are local catalyst with the performance as good as commercial catalyst. One of those catalyst is zeolite. This paper determines the study of characterization of zeolite using Scanning Electron Microscope (SEM) and X-ray Diffraction (XRD), and explains the perfomance of zeolite in the synthesis of triacetin. Catalyst from zeolite was made by mixing with H2SO4 in various concentrations, neutralization and drying. From morfology analysis by using Scanning Electron Microscope (SEM), density and X-Ray Diffraction (XRD) obtain that mixing with H2SO4 of 0.5M is better than the others. From the study of catalyst synthesis from natural zeolite it can be concluded that natural zeolite before activation has fragile structure meanwhile after being activated it was formed crystal structure. The best zeolite crystal phase was obtained from zeolite activated by using 0,5 M H2SO4 with glycerol conversion of 94.45% and triacetin selectivity of 4.01%.

Utilization of Desulfuration Residues in Non-Autoclaved Aerated Concrete

2011 ◽  
Vol 250-253 ◽  
pp. 707-710
Author(s):  
Fang Xian Li ◽  
You Zhi Chen ◽  
Qi Jun Yu ◽  
Jiang Xiong Wei
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Bulk Density ◽  
Hydration Products ◽  
X Ray Diffraction ◽  
X Ray ◽  
Autoclaved Aerated Concrete ◽  
Aerated Concrete ◽  
Scanning Electron

Desulfuration residues were used as aggregate to produce Non-autoclaved aerated concrete. The effects of water-hinder ratio, casting temperature on the gas forming behavior, and those of desulfuration residue content on the compressive strength and bulk density of aerated concrete were investigated. The types of the hydration products and the microstructure of Non-autoclaved aerated concrete with desulfuration residue were investigated by means of X-ray diffraction and scanning electron microscope. Results show that the optimum replacement amount was determined as 50% and at this rate the compressive strength, bulk density of Non-autoclaved aerated concrete were measured as 2.83 MPa and 543 kg/m3. The hydration products of Non-autoclaved aerated concrete with desulfuration residue are C2SH (A) and C2SH (B) along with ettringite and hydrogarnet phases.

The Preparation and Micro Mechanism of Brick Materials with Iron Tailings in Tanshang Area

2013 ◽  
Vol 753-755 ◽  
pp. 572-575
Author(s):  
Shu Xian Liu ◽  
Shao Bo Wei
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Fly Ash ◽  
Flexural Strength ◽  
Scanning Electron Microscope ◽  
Steam Curing ◽  
X Ray ◽  
A New Technique ◽  
Scanning Electron

This paper discussed the experimental results of exploiting brick materials with iron tailing materials in Tanshang area. Through preparation of iron tailing bricks, the technical flow and production proportion was obtained. The results show that a burning-and steam curing-free brick product with a compressive strength of 28.30 MPa and Flexural strength of 5.63 MPa as the following: iron tailing; fly ash; sand; CaO; gypsum; cement. And long-term properties of a burning-and steam curing-free brick is also studied by experiments in this paper. Put forward a new technique of making materials with iron tailing. At the same time, the micro mechanism of iron tailing brick was also studied with X-Ray Diffractometer (XRD) and Scanning Electron Microscope (SEM).

Influence of Nano-SiO2 on the Strength of High Performance Concrete

2011 ◽  
Vol 686 ◽  
pp. 432-437 ◽  
Author(s):  
Bao Min Wang
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
High Performance ◽  
High Performance Concrete ◽  
Mixing Ratio ◽  
X Ray Diffraction ◽  
X Ray ◽  
Injection Experiment ◽  
Scanning Electron

The influence of Nano-SiO2 (NS) on the strength of high-performance concrete (W/B=0.24, W/B=0.29, W/B=0.34) has been studied in this paper. The results show that compressive strengths of concrete in both the early and later stage can be improved by adding Nano-SiO2 content. And the influence on the early compressive strength is greater than that on the later compressive strength. According to the results, 3%-5% Nano-SiO2can be used as the proper mixing ratio. X-ray diffraction, SEM (scanning electron microscope) and mercury injection experiment were used to analyze the action principle of Nano-SiO2 microscopically, the microscopic characteristics of concrete can be significantly improved through interfacial and filling effect effects so that the performance of concrete can be accordingly improved.

PENGGUNAAN TiO2 PARTIKEL NANO HASIL SINTESIS BERBASIS AIR MENGGUNAKAN METODA SOL-GEL PADA BAHAN KAPAS SEBAGAI APLIKASI UNTUK TEKSTIL ANTI UV

Arena Tekstil ◽  
2013 ◽  
Vol 28 (1) ◽  
Author(s):  
Maya Komalasari ◽  
Bambang Sunendar
Keyword(s):  
Fourier Transform ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Sol Gel ◽  
Crosslinking Agent ◽  
X Ray Diffraction ◽  
Nano Tio2 ◽  
X Ray ◽  
Infra Red ◽  
Scanning Electron

Partikel nano TiO2 berbasis air dengan pH basa telah berhasil disintesis dengan menggunakan metode sol-gel dan diimobilisasi pada kain kapas dengan menggunakan kitosan sebagai zat pengikat silang. Sintesis dilakukan  dengan prekursor TiCl4 pada konsentrasi 0,3 M, 0,5 M dan 1 M, dan menggunakan templat kanji dengan proses kalsinasi pada suhu 500˚C selama 2 jam. Partikel nano TiO2 diaplikasikan ke kain kapas dengan metoda pad-dry-cure dan menggunakan kitosan sebagai crosslinking agent. Berdasarkan hasil Scanning Electron Microscope (SEM),diketahui bahwa morfologi partikel TiO2 berbentuk spherical dengan ukuran nano (kurang dari 100 nm). Karakterisasi X-Ray Diffraction (XRD) menunjukkan adanya tiga tipe struktur kristal utama, yaitu (100), (101) dan (102) dengan fasa kristal yang terbentuk adalah anatase dan rutile. Pada karakterisasi menggunakan SEM terhadap serbuk dari TiO2 yang telah diaplikasikan ke permukaan kain kapas, terlihat adanya imobilisasi partikel nano TiO2 melalui ikatan hidrogen silang dengan kitosan pada kain kapas. Hasil analisa tersebut kemudian dikonfirmasi dengan FTIR (Fourier Transform Infra Red) yang hasilnya memperlihatkan puncak serapan pada bilangan gelombang 3495 cm-1, 2546 cm-1, dan 511 cm-1,  yang masing-masing diasumsikan sebagai adanya vibrasi gugus fungsi O-H, N-H dan Ti-O-Ti. Hasil SEM menunjukkan pula bahwa kristal nano yang terbentuk diantaranya adalah fasa rutile , yang berdasarkan literatur terbukti dapatberfungsi sebagai anti UV.

Effect of the Neodymium Content on Mechanical Properties of the Electro-Brush Plated Nano-Al2O3/Ni Composite Coating

2012 ◽  
Vol 525-526 ◽  
pp. 277-280
Author(s):  
Guo Jin ◽  
Xiu Fang Cui ◽  
Er Bao Liu ◽  
Qing Fen Li
Keyword(s):  
Mechanical Properties ◽  
Rare Earth ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Composite Coating ◽  
Nanoindentation Test ◽  
X Ray Diffraction ◽  
X Ray ◽  
Small Cracks ◽  
Scanning Electron

The effect of the neodymium content on mechanical properties of the electro-brush plated nanoAl2O3/Ni composite coating was investigated in this paper. The microstructure and phase structure were studied with scanning electron microscope (SEM) and X-ray diffraction (XRD). The hardness and abrasion properties of several coatings with different neodymium content were studied by nanoindentation test and friction / wear experiment. Results show that the coatings are much finer and more compact when the neodymium was added, and the hardness and abrasion property of the coatings with neodymium were improved obviously. Besides, the small cracks conduced by the upgrowth stress in the coatings were ameliorated when the rare earth neodymium was added. The improvement mechanism was further discussed.

Effect of Briquetting Pressure on the Performance of In Situ Formed Sialon in Al2O3-C Refractory Bricks

2014 ◽  
Vol 881-883 ◽  
pp. 1049-1052 ◽  
Author(s):  
Nai Peng ◽  
Cheng Ji Deng ◽  
Hong Xi Zhu
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
X Ray Diffraction ◽  
X Ray ◽  
Z Value ◽  
Refractory Bricks ◽  
Scanning Electron

In this paper, the effects of briquetting pressure on the performance of in-situ formed Sialon in Al2O3-C refractory bricks are investigated. The phase compositions and microstructure of the Al2O3-C refractory were investigated by X-ray diffraction (XRD) and scanning electron microscope (SEM).The results show the briquetting pressure hardly has effect on the phase of the sintered specimens, two new phases of Sialon with a Z value of 2 and SiC formed. The micrographs of Sialon crystals have the shape of both column and tabular column, but with a cone tip in the specimens sintered at 200MPa and 300MPa and smooth tip in specimens sintered at 400MPa and 500MPa.

Effect of P2O5 on the Properties of Alite-Calcium Strontium Sulphoaluminate Cement

2011 ◽  
Vol 306-307 ◽  
pp. 961-965
Author(s):  
Chao Nan Yin ◽  
Ling Chao Lu ◽  
Shou De Wang
Keyword(s):  
Compressive Strength ◽  
Electron Microscope ◽  
Heat Evolution ◽  
Petrographic Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Sulphoaluminate Cement ◽  
Suitable Amount ◽  
Acceleration Period ◽  
Scanning Electron

The influence of P2O5on the properties of alite-calcium strontium sulphoaluminate cement was researched by means of X-ray diffraction, scanning electron microscope-energy dispersive spectroscopy (SEM-EDS) and petrographic analysis. The results show that the optimal content of P2O5is 0.3% and the compressive strength of the cement at 1, 3, 28d are 27.0, 59.1, 110.9MPa when the calcining temperature is 1350°C. P2O5mainly exists in the belite and a suitable amount of P2O5can promote the formation of C1.5Sr2.5A3and alite. When the content of P2O5is higher than 0.3%, the formation of C1.5Sr2.5A3and alite can be hindered. P2O5can enhance the hydration heat evolution rate in the acceleration period and the hydrate heat of cement containing P2O5increases slightly.

Effect of Nickel on Titanium Carbide Synthesized via Tungsten Inert Gas (TIG) Method

2012 ◽  
Vol 620 ◽  
pp. 384-388
Author(s):  
Sharifah Aishah Syed Salim ◽  
Julie Juliewatty Mohamed ◽  
Zainal Arifin Ahmad ◽  
Zainal Arifin Ahmad
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Powder Mixture ◽  
Raw Material ◽  
Inert Gas ◽  
X Ray Diffraction ◽  
X Ray ◽  
Arc Melting ◽  
Elemental Powder Mixture ◽  
Scanning Electron

Numerous methods have been used to produce high purity TiC. There is no previous study has been reported on the formation using single elemental powders of Titanium (Ti) and Carbon (C) with addition Nickel (Ni) by tungsten inert gas (TIG) weld method. In this work, TiC was synthesized via TIG method by arc melting elemental powder mixture of Ti and C at ~5 second (s) and 80 ampere (A). The effect Ni contents on TiC formation was investigated. The mixed raw material was ball milled for 24 hours followed by synthesis via TIG method. The arced samples were characterized by X-ray diffraction (XRD) and Scanning electron microscope (SEM). It was revealed, that small amount of Ni additive to the metal powder allows the production of dense and tough TiC.

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