Priorities for development of standard test methods to support the commercialization of cellulose nanomaterials

TAPPI Journal ◽  
2019 ◽  
Vol 18 (4) ◽  
pp. 245-260 ◽  
Author(s):  
STEPHANIE BECK ◽  
COLLEEN WALKER ◽  
WARREN BATCHELOR

With the growing number of producers and users of cellulose nanomaterials (CNMs), there is an increasing need to develop standard test methods to control production and quality of CNMs. In 2014, a Task Group was formed within the ISO Technical Committee 6 Paper, board and pulps to begin addressing the need for standards. This Task Group, TG 1, was tasked with reviewing existing standards and identifying the need for additional standards to characterize CNMs. In March 2018, TG 1 launched a survey to ask CNM producers around the world about the importance of having standard procedures to measure and quantify a variety of CNM properties, both physical and chemical. Producers were asked to identify the type(s) of CNM they produced and their scale of production, and to rank the properties for which they felt standard test methods were most important. In this paper, we summarize the survey responses and identify those properties of highest interest for producers of both cellulose nanocrystals (CNCs) and cellulose nano- and microfibril-based materials (CNFs/CMFs). Properties of importance can be divided into three broad groups: i) a standard has either been developed or is under development, ii) a currently used standard could be adapted for use with CNMs, or iii) no standard is currently available and further R&D and consultation with industry is needed before a suitable and well-validated standard can be developed. The paper also examines the challenges of developing new standard methods for some of the key properties—as well as the feasibility and limitations of adapting exiting standards—to CNMs.

2021 ◽  
Vol 11 (11) ◽  
pp. 5294
Author(s):  
Peer Decker ◽  
Ines Zerbin ◽  
Luisa Marzoli ◽  
Marcel Rosefort

Two different intergranular corrosion tests were performed on EN AW-6016 sheet material, an ISO 11846:1995-based test with varying solution amounts and acid concentrations, and a standard test of an automotive company (PV1113, VW-Audi). The average intergranular corrosion depth was determined via optical microscopy. The differences in the intergranular corrosion depths were then discussed with regard to the applicability and quality of the two different test methods. The influence of varying test parameters for ISO 11846:1995 was discussed as well. The determined IGC depths were found to be strongly dependent on the testing parameters, which will therefore have a pronounced influence on the determined IGC susceptibility of a material. In general, ISO 11846:1995 tests resulted in a significantly lower corrosion speed, and the corrosive attack was found to be primarily along grain boundaries.


2019 ◽  
Vol 21 (4) ◽  
pp. 317 ◽  
Author(s):  
B.B. Teltayev ◽  
A.A. Kalybai ◽  
G.G. Izmailova ◽  
S.R. Rossi ◽  
E.D. Amirbayev ◽  
...  

Physical and chemical indicators of bitumen quality of grade BND 70/100 with the added carbon nanopowder 2% by weight have been studied by laboratory test methods and analysis. High reaction ability of nanopowder particles and concentration of excess surface and internal energy in them have been determined, which provide the increase of low-temperature resistance, aggregate strength, and improvement of rheological properties of nanostructured bitumen. Essential structure variation has been proved: the increase of asphaltenes and oils content for 9% and 7.2% respectively due to the decrease of resins for 16.2% by weight. Methods have been discussed for preparing a liquid nanocarbon mix, adding of the mix into bitumen and homogenization of the bitumen. Some economic indicators have been represented which influence essentially the reduction for the cost value of the nanostructure bitumen.


2016 ◽  
Vol 13 (3) ◽  
pp. 77-94
Author(s):  
Glenn Oliver ◽  
Jonathan Weldon ◽  
Chudy Nwachukwu ◽  
John Andresakis ◽  
John Coonrod ◽  
...  

Currently, there is no industry standard test method for measuring dielectric properties of circuit board materials at frequencies greater than ~10 GHz. Various material vendors and test laboratories apply different approaches to determine these properties. It is common for these different approaches to yield varying values of key properties such as permittivity and loss tangent. The D-24C Task Group of IPC has developed this round-robin program to assess these various methods from the “bottom up” to determine if standardized methods can be agreed upon to provide the industry with more accurate and valid characteristics of dielectrics used in high-frequency and high-speed applications.


2009 ◽  
Vol 1207 ◽  
Author(s):  
Lynn Davis ◽  
Seth Coe-Sullivan ◽  
Oleg Shchekin ◽  
K.C. Mishra ◽  
Madis Raukas ◽  
...  

AbstractLuminescent nanoparticles such as quantum dots (QDs) are beginning to appear in SSL devices and other commercial products. The allure of QDs in SSL these applications is the potential to provide enhanced device performance (e.g., improved energy efficiency, better color rendering properties, etc.) than is possible with conventional technologies. When used in SSL and other applications, QDs are typically incorporated into or coated onto a solid organic or inorganic matrix and then are excited using external stimuli (e.g., blue light with a maximum wavelength of 450 nm). This structure is vastly different from the colloidal environment in which QDs are typically synthesized and characterized. Bridging the gap between the measurements typically acquired by QD providers and those needed by potential end-users is currently difficult due to the absence of agreed upon standard test methods. Measurements taken in colloidal QD suspensions often do not translate to solid-phase material characterizations due to a variety of factors including sample preparation methods (e.g., temperature, solvents, etc), QD concentrations, and effects arising from the presence of the solid matrix. Additionally, solid samples are more likely to exhibit diffuse reflectance and/or diffuse transmittance necessitating the use of an integrating sphere and a computer-controlled spectrometer to acquire accurate readings. This paper discusses the development of a standard test method to measure the quantum efficiency of QDs contained in solid organic and inorganic matrices. This standard is being developed under the auspices of the International Electrotechnical Commission, Technical Committee 113 on Nano-electrotechnologies.


Author(s):  
Halima Brima Gama Tigaidi ◽  
Dr. Mohammed Ismail Humaida ◽  
Dr.Kubra Ali Ebrahim Hammad

This study was conducted in El-Obied City, North Kordofan State.The study comprised of 54 samples of water selected from houses, animal carts (karo), tankers, gerbas and main source of water bara basin and El-khazan (surface water )in El-Obied. The sample was divided over these sources following a process of stratified sampling combined with simple random samples with probability proportional to size of sample over the selected blocks where selection was at random in each stage. Physical and chemical testing of water was done using standard procedures. Two Samples of water were collected from the main sources of water in the City for physical and chemical analysis and 52 samples collected from blocks. The data were analyzed by computer. This study showed that 50% of the samples were without residual chlorine, and only 1.8% of samples were soft water. The study showed that 3.7% of samples had pH above WHO and SSMO Standard and also showed 18.5% of samples had turbidity above 5 NTU. KEY WORDS: Assessment, physical, chemical, drinking water, El-Obied


Author(s):  
V. Ilienko ◽  
O. Isachenko ◽  
A. Los ◽  
M. Gerashchenko ◽  
S. Rudnichenko

Considering the lack of standard test methods for communication channels of modern unmanned aerial systems (UAS) class I and II, according to the UAS classification of the Armed Forces of Ukraine, it was decided to work out the basic approaches for determining indicators, conditions and procedure for conducting tests in this direction. The suggested methodological recommendations will improve the quality of the parameters and characteristics assessment for communication channels of UAS I and II classes. One of the distinctive trends in the development of modern forms and methods of conducting armed combat at all stages of the armed conflict is the widespread use of the UASs by opposing parties. UASs are capable of significant increasing the effectiveness of accomplishing aerial reconnaissance tasks, organizing electronic warfare, and providing real-time delivery of target pinpointing to fire means for the destruction of enemy’s manpower and material. A distinctive feature of UAS is that its external crew, as a rule, accomplish its mission at a considerable distance from the objects of attack. This fact significantly reduces the security risks and threats associated with performing combat missions under conditions of active enemy counteraction. Due to this feature, considerable attention is paid to the development of a reliable communication system that would be able to ensure task accomplishment at the maximum distance from command and control site. During the tests of UAS Class I and II, the specialists of the State Scientific Research Institute of Armament and Military Equipment Testing and Certification used testing methods of radio channels assessment, which will allow to improve the quality of UAS research of this type and give the manufacturers recommendations for increasing their capabilities.


2019 ◽  
Author(s):  
Emel Islamzada ◽  
Kerryn Matthews ◽  
Quan Guo ◽  
Aline T. Santoso ◽  
Simon P. Duffy ◽  
...  

AbstractA fundamental challenge in the transfusion of red blood cells (RBCs) is that a subset of donated RBC units may not provide optimal benefit to transfusion recipients. This variability stems from the inherent ability of donor RBCs to withstand the physical and chemical insults of cold storage, which ultimately dictate their survival in circulation. The loss of RBC deformability during cold storage is well-established and has been identified as a potential biomarker for the quality of donated RBCs. While RBC deformability has traditionally been indirectly inferred from rheological characteristics of the bulk suspension, there has been considerable interest in directly measuring the deformation of RBCs. Microfluidic technologies have enabled single cell measurement of RBC deformation but have not been able to consistently distinguish differences between RBCs between healthy donors. Using the microfluidic ratchet mechanism, we developed a method to sensitively and consistently analyze RBC deformability. We found that the aging curve of RBC deformability varies significantly across donors, but is consistent for each donor over multiple donations. Specifically, certain donors seem capable of providing RBCs that maintain their deformability during two weeks of cold storage in standard test tubes. The ability to distinguish between RBC units with different storage potential could provide a valuable opportunity to identify donors capable of providing RBCs that maintain their integrity, in order to reserve these units for sensitive transfusion recipients.


2008 ◽  
Vol 589 ◽  
pp. 439-444
Author(s):  
Márton Takács

There is no doubt that concrete makes a massive contribution to sustaining the quality of life. Properties of concrete can be expediently modified by adding special chemical materials called admixtures. Admixtures for concrete are now widely accepted as materials that contribute to the production of durable and cost-effective concrete structures [1]. Plasticizing admixtures reduce water needed to achieve a given workability of the fresh mix. This main effect can be utilized in three ways: increased strength, increased workability, or economies in mix design [2]. In this research work effect of type and dosage of different plasticizing admixtures available in Hungary were investigated in detail. Standard test methods such as flow table test, compressive test, and shrinkage test were applied to obtain effectiveness of the admixtures. Results were compared with the requirements of the harmonized admixture standard MSZ EN 934-2:2002.


2019 ◽  
Vol 119 ◽  
pp. 122-126
Author(s):  
P. O. Kushchenko ◽  
O. V. Dunikov ◽  
V. V. Varganov

For many years, the refractory and refractory raw materials have been successfully tested at the Testing centre of the JSC “The URIR named after A. S. Berezhnoy” for the orders of manufacturers and consumers of refractory products and for the institute’s own needs. Testing of refractory products is carried out in order to determine the physicochemical, physico­mechanical, thermophysical and thermomechanical properties and assess the quality of refractories and refractory raw materials. When conducting tests of refractories in the Testing centre of institute, standard test methods are used in accordance with the current standards in Ukraine and the methods developed at the institute. In this article, features of the measurement management system in Testing centre of the JSC “The URIR named after A. S. Berezhnoy” and results of the appraisal of Testing centre of the institute are adduced.


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