scholarly journals Elastically Graded Titanium Alloy Produced by Mechanical Surface Deformation

2021 ◽  
Vol 8 ◽  
Author(s):  
Stéphanie Delannoy ◽  
Sarah Baïz ◽  
Pascal Laheurte ◽  
Laurence Jordan ◽  
Frédéric Prima

The objective of this study was to develop a thermo-mechanical strategy to create a radial elasticity gradient in a β metastable Ti-Nb-Zr alloy, and to characterize it in terms of microstructural and mechanical properties. A first investigation was conducted on thin samples of Ti-20Nb-6Zr (at.%) submitted to various thermo-mechanical treatments. Microstructure-properties relationships and elastic variability of this alloy were determined performing uniaxial tensile tests, X-ray diffraction and scanning and transmission electron microscopies. Based on these preliminary results, mechanical deformation was identified as a potential way to lower the elastic modulus of the alloy. In order to create elastically graded pieces, shot-peening was therefore carried out on thicker samples to engender surface deformation. In this second part of the work, local mechanical properties were evaluated by instrumented micro-indentation. Experimental observations demonstrated that shot-peening enabled to locally induce martensitic transformation on surface, and a decrease in indentation elastic modulus from 85 to 65 GPa over 400 μm was highlighted. Surface deformation proved to be an efficient way of creating an elasticity gradient in β metastable titanium alloys. This combination of material and process could be suitable to produce dental implants with mechanically enhanced biocompatibility.

2014 ◽  
Vol 543-547 ◽  
pp. 3733-3736
Author(s):  
Rong Hua Zhang ◽  
Biao Wu ◽  
Xiao Ping Zheng

In this study, 8009 heat resistant aluminum alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using transmission electron microscopy, X-ray diffraction, and tensile tests. The secondary phases in the microstructure of the spray-deposited alloy were examined. The tensile test results indicate that the spray-deposited 8009 alloy both at room and elevated temperature displays superior tensile strength due to the presence of the thermally stable Al12(Fe,V)3Si particles.


2021 ◽  
Vol 11 (4) ◽  
pp. 1517
Author(s):  
Silvia Todros ◽  
Carlo Biz ◽  
Pietro Ruggieri ◽  
Piero G. Pavan

Plantar Fascia (PF) is a fibrous tissue that plays a key role in supporting the foot arch; it can be affected by several pathologies that can alter foot biomechanics. The present study aims at investigating the mechanical behavior of PF and evaluating possible correlations between mechanical properties and specific pathologies, namely diabetes and plantar fibromatosis (Ledderhose syndrome). PF samples were obtained from 14 human subjects, including patients with Ledderhose syndrome, patients affected by diabetes and healthy subjects. Mechanical properties of PF tissues were evaluated on three samples from each subject, by cyclic uniaxial tensile tests up to 10% of maximum strain and stress relaxation tests for 300 s, in hydrated conditions at room temperature. In tensile tests, PF exhibits non-linear stress–strain behavior, with a higher elastic modulus (up to 25–30 MPa) in patients affected by Ledderhose syndrome and diabetes with respect to healthy subjects (elastic modulus 10 ÷ 14 MPa). Stress-relaxation tests show that PF of patients affected by Ledderhose syndrome and diabetes develop more intense viscous phenomena. The results presented in this work represent the first experimental data on the tensile mechanical propertied of PF in subjects with foot diseases and can provide an insight on foot biomechanics in pathological conditions.


2014 ◽  
Vol 783-786 ◽  
pp. 503-508
Author(s):  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yon Gan Zhang ◽  
Zhi Hui Li ◽  
Hong Wei Liu ◽  
...  

In this study, Mg-6.8Gd-4.5Y-0.5Zr alloy was fabricated by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using optical microscopy, scanning/transmission electron microscopy, X-ray diffraction, and tensile tests. The secondary phases in the microstructure of the spray-deposited alloy were examined. The tensile test results indicate that the spray-deposited Mg-6.8Gd-4.5Y-0.5Zr alloy displays superior tensile strength due to grain refinement and the presence of precipitating strengthening phases.


2012 ◽  
Vol 706-709 ◽  
pp. 264-267
Author(s):  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yon Gan Zhang ◽  
Hong Wei Liu ◽  
Zhi Hui Li ◽  
...  

In this study, Zn-30Al-1Cu alloy was synthesized by the spray atomization and deposition technique. The microstructure and mechanical properties of the alloy were studied using optical microscopy, scanning electron microscopy, transmission electron microscopy, X-ray diffraction and tensile tests. It can be seen that the microstructure of spray-deposited Zn-30Al-1Cu alloy is composed of the Zn/Al eutectoids and few compounds. The Zn/Al eutectoids were shown lamellar, particle and Chinese script morphologies. The compound phases in the microstructure of the spray-deposited alloy were examined. The property test results indicate that the spray-deposited Zn-30Al-1Cu alloy displays superior tensile strength.


2020 ◽  
Vol 299 ◽  
pp. 716-722 ◽  
Author(s):  
S.A. Shalnova ◽  
O.G. Klimova-Korsmik ◽  
G.A. Turichin ◽  
M.O. Gushchina

In this paper, the effect of process parameters on quality of fabricated wall, the phase composition, microhardness, and mechanical properties of the Ti-6Al-4V titanium sample, obtained by direct laser deposition, was considered. To determine the characteristics of the samples the X-ray diffraction, scanning electron microscopy, Vickers microhardness measurements, and uniaxial tensile tests were used. It is shown that the process parameters with the same speed, oscillation amplitude and peak value of heat flux have a similar wall thickness but different waviness with high mechanical properties.


2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Sebastián Tognana ◽  
Susana Montecinos ◽  
Rosana Gastien ◽  
Walter Salgueiro

Abstract Commonly used 3D printed samples are partially infilled to reduce time and cost of printing, with mechanical properties dependent on the infill. In this work, the influence of the percentage and pattern of infill in PLA printed samples on the elastic modulus and characteristic stresses was analyzed. The elastic modulus, E, and characteristic stresses (σ 0.2, σ 4 and the maximum tensile stress) were determined for each sample using impulse excitation technique, IET, and uniaxial tensile tests. An apparent density was calculated for each pattern and infill percentage, and the mechanical parameters were studied as a function of such density. The results of IET obtained in different modes of vibration were analyzed and an apparent value of E was calculated. FEM simulations were carried out and the results were compared with the experimental ones. The mechanical properties for different infill percentages and infill patterns were studied by comparing the specific values of E and the stresses. Samples with higher infill percentages exhibit the best specific values of maximum stress and E, but the sample with 20% infill has the highest specific yield stress and a good value of the specific E from flexural vibrations.


2021 ◽  
pp. 073168442110204
Author(s):  
Bin Yang ◽  
Yingying Shang ◽  
Zeliang Yu ◽  
Minger Wu ◽  
Youji Tao ◽  
...  

In recent years, coated fabrics have become the major material used in membrane structures. Due to the special structure of base layer and mechanical properties, coated biaxial warp-knitted fabrics are increasingly applied in pneumatic structures. In this article, the mechanical properties of coated biaxial warp-knitted fabrics are investigated comprehensively. First, off-axial tensile tests are carried out in seven in-plane directions: 0°, 15°, 30°, 45°, 60°, 75°, and 90°. Based on the stress–strain relationship, tensile strengths are obtained and failure modes are studied. The adaptability of Tsai–Hill criterion is analyzed. Then, the uniaxial tensile creep test is performed under 24-h sustained load and the creep elongation is calculated. Besides, tearing strengths in warp and weft directions are obtained by tearing tests. Finally, the biaxial tensile tests under five different load ratios of 1:1, 2:1, 1:2, 1:0, and 0:1 are carried out, and the elastic constants and Poisson’s ratio are calculated using the least squares method based on linear orthotropic assumption. Moreover, biaxial specimens under four load ratios of 3:1, 1:3, 5:1, and 1:5 are further tensile tested to verify the adaptability of linear orthotropic model. These experimental data offer a deeper and comprehensive understanding of mechanical properties of coated biaxial warp-knitted fabrics and could be conveniently adopted in structural design.


Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 218
Author(s):  
Xianjie Yuan ◽  
Xuanhui Qu ◽  
Haiqing Yin ◽  
Zaiqiang Feng ◽  
Mingqi Tang ◽  
...  

This present work investigates the effects of sintering temperature on densification, mechanical properties and microstructure of Al-based alloy pressed by high-velocity compaction. The green samples were heated under the flow of high pure (99.99 wt%) N2. The heating rate was 4 °C/min before 315 °C. For reducing the residual stress, the samples were isothermally held for one h. Then, the specimens were respectively heated at the rate of 10 °C/min to the temperature between 540 °C and 700 °C, held for one h, and then furnace-cooled to the room temperature. Results indicate that when the sintered temperature was 640 °C, both the sintered density and mechanical properties was optimum. Differential Scanning Calorimetry, X-ray diffraction of sintered samples, Scanning Electron Microscopy, Energy Dispersive Spectroscopy, and Transmission Electron Microscope were used to analyse the microstructure and phases.


Author(s):  
G. S. Zakharova ◽  
E. Thauer ◽  
A. N. Enyashin ◽  
L. F. Deeg ◽  
Q. Zhu ◽  
...  

AbstractThe potential battery electrode material V2O3/C has been prepared using a sol–gel thermolysis technique, employing vanadyl hydroxide as precursor and different organic acids as both chelating agents and carbon sources. Composition and morphology of resultant materials were characterized by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, physical sorption, and elemental analysis. Stability and electronic properties of model composites with chemically and physically integrated carbon were studied by means of quantum-chemical calculations. All fabricated composites are hierarchically structured and consist of carbon-covered microparticles assembled of polyhedral V2O3 nanograins with intrusions of amorphous carbon at the grain boundaries. Such V2O3/C phase separation is thermodynamically favored while formation of vanadium (oxy)carbides or heavily doped V2O3 is highly unlikely. When used as anode for lithium-ion batteries, the nanocomposite V2O3/C fabricated with citric acid exhibits superior electrochemical performance with an excellent cycle stability and a specific charge capacity of 335 mAh g−1 in cycle 95 at 100 mA g−1. We also find that the used carbon source has only minor effects on the materials’ electrochemical performance.


2013 ◽  
Vol 762 ◽  
pp. 551-555 ◽  
Author(s):  
Marek Stanislaw Węglowski ◽  
Marian Zeman ◽  
Miroslaw Lomozik

In the present study, the investigation of weldability of new ultra-high strength - Weldox 1300 steel has been presented. The thermal simulated samples were used to investigate the effect of welding cooling time t8/5 on the microstructure and mechanical properties of the heat affected zone (HAZ). In the frame of these investigation the microstructure was studied by the light (LM) and transmission electron microscopies (TEM). It has been shown that the microstructure of the Weldox 1300 steel is composed of tempered martensite, and inside the laths the minor precipitations mainly V(CN) and molybdenum carbide Mo2C were observed. Mechanical properties of parent material were analysed by the tensile, impact and hardness tests. In details the influence of cooling time in the range of 2,5 - 300 s. on hardness, impact toughness and microstructure of simulated HAZ was studied by using welding thermal simulation test. The results show that the impact toughness and hardness decrease with the increase of t8/5 under the condition of a single thermal cycle in simulated HAZ. The continuous cooling transformation diagrams (CCT-W for welding conditions) of Weldox 1300 steel for welding purposes was also elaborated. The steel Weldox 1300 for cooling time in the range of 2,5 - 4 s showed martensite microstructure, for time from 4 s to 60 s mixture of martensite and bainite, and for longer cooling time mixture of ferrite, bainite and martensite. The results indicated that the weldability of Weldox 1300 steel is limited and to avoid the cold cracking the preheating procedure or medium net linear heat input should be used.


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