scholarly journals 3D Characterization of Sponge Cake as Affected by Freezing Conditions Using Synchrotron X-ray Microtomography at Negative Temperature

Foods ◽  
2021 ◽  
Vol 10 (12) ◽  
pp. 2915
Author(s):  
Amira Zennoune ◽  
Pierre Latil ◽  
Fatou-Toutie Ndoye ◽  
Frederic Flin ◽  
Jonathan Perrin ◽  
...  
Keyword(s):  
Negative Temperature ◽  
Ice Formation ◽  
Analysis Method ◽  
Image Analysis Method ◽  
Sponge Cake ◽  
X Ray ◽  
Before And After ◽  
Shape Characterization ◽  
Fast Freezing

In this study, the microstructural evolution of a non-reactive porous model food (sponge cake) during freezing was investigated. Sponge cake samples were frozen at two different rates: slow freezing (0.3 °C min−1) and fast freezing (17.2 °C min−1). Synchrotron X-ray microtomography (µ-CT) and cryo-scanning electron microscopy (Cryo-SEM) were used to visualize and analyze the microstructure features. The samples were scanned before and after freezing using a specific thermostated cell (CellStat) combined with the synchrotron beamline. Cryo-SEM and 3D µ-CT image visualization allowed a qualitative analysis of the ice formation and location in the porous structure. An image analysis method based on grey level was used to segment the three phases of the frozen samples: air, ice and starch. Volume fractions of each phase, ice local thickness and shape characterization were determined and discussed according to the freezing rates.

ASSESSMENT OF OSTEOARTHRITIS INITIATIVE–KELLGREN AND LAWRENCE SCORING PROJECTS QUALITY USING COMPUTER ANALYSIS

2010 ◽  
Vol 13 (04) ◽  
pp. 197-201 ◽  
Author(s):  
Lior Shamir ◽  
David T. Felson ◽  
Luigi Ferrucci ◽  
Ilya G. Goldberg
Keyword(s):  
Image Analysis ◽  
Gold Standard ◽  
Population Studies ◽  
Detection Accuracy ◽  
X Rays ◽  
Analysis Method ◽  
Image Analysis Method ◽  
X Ray ◽  
Osteoarthritis Initiative ◽  
Kellgren And Lawrence

The detection of knee osteoarthritis (OA) is a subjective task, and even two highly experienced and well-trained readers might not always agree on a specific case. This problem is noticeable in OA population studies, in which different scoring projects provide significantly different scores for the same knee X-rays. Here we propose a method for quantitative assessment and comparison of knee X-ray scoring projects in OA population studies. The method works by applying an image analysis method that automatically detects OA in knee X-ray images, and comparing the consistency of the scores when using each of the scoring projects as "gold standard." The method was applied to compare the osteoarthritis initiative (OAI) clinic reading derived Kellgren and Lawrence (K&L) scores to central reading, and showed that when using the derived K&L scores the automatic image analysis method was able to accurately differentiate between healthy joints and moderate OA joints in ~70% of the cases. When the OAI central reading scores were used as gold standard, the detection accuracy was elevated to ~77%. These results show that the OAI central readings scores are more consistent with the X-rays, indicating that the central reading better reflects the radiographic features associated with OA, compared to the OAI K&L scores derived from clinic readings.

Aging of iron manganite negative temperature coefficient thermistors

1998 ◽  
Vol 13 (5) ◽  
pp. 1238-1242 ◽  
Author(s):  
T. Battault ◽  
R. Legros ◽  
A. Rousset
Keyword(s):  
Temperature Coefficient ◽  
Spinel Structure ◽  
Negative Temperature Coefficient ◽  
Negative Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
Octahedral Sites ◽  
Before And After ◽  
Structural Equilibrium ◽  
Electrical Data

“Aging,” defined as the drift of resistance with temperature after 1000 h, was investigated for iron manganite temperature coefficient thermistors. For these devices, aging is relatively large, about 10%. The cationic distributions before and after aging were determined by Mössbauer spectroscopy. These distributions explain all the x-ray diffraction and correlated electrical data. The origin of the aging observed on iron manganites thermistors has been identified. It is due to the migration of Fe3+ ions from tetrahedral to octahedral sites of the spinel structure in order to reach a structural equilibrium.

scholarly journals Algorithms for 3D Particles Characterization Using X-Ray Microtomography in Proppant Crush Test

2018 ◽  
Vol 4 (11) ◽  
pp. 134 ◽  
Author(s):  
Ilia Safonov ◽  
Ivan Yakimchuk ◽  
Vladimir Abashkin
Keyword(s):  
Laboratory Method ◽  
X Ray ◽  
Geometric Moments ◽  
Before And After ◽  
Statistical Hypotheses ◽  
Image Processing Algorithms ◽  
A New Technique ◽  
Individual Particles ◽  
Remarkable Advantage

We present image processing algorithms for a new technique of ceramic proppant crush resistance characterization. To obtain the images of the proppant material before and after the test we used X-ray microtomography. We propose a watershed-based unsupervised algorithm for segmentation of proppant particles, as well as a set of parameters for the characterization of 3D particle size, shape, and porosity. An effective approach based on central geometric moments is described. The approach is used for calculation of particles’ form factor, compactness, equivalent ellipsoid axes lengths, and lengths of projections to these axes. Obtained grain size distribution and crush resistance fit the results of conventional test measured by sieves. However, our technique has a remarkable advantage over traditional laboratory method since it allows to trace the destruction at the level of individual particles and their fragments; it grants to analyze morphological features of fines. We also provide an example describing how the approach can be used for verification of statistical hypotheses about the correlation between particles’ parameters and their crushing under load.

Preparation and Characterization of Clays from Different Areas in Ban Bo Suak, Nan Province, Thailand

2015 ◽  
Vol 659 ◽  
pp. 127-131
Author(s):  
Usanee Malee ◽  
Sakdiphon Thiansem
Keyword(s):  
Clay Sample ◽  
X Ray Diffraction ◽  
Scientific Process ◽  
Quartz Content ◽  
Xrd Pattern ◽  
X Ray ◽  
Kiln Site ◽  
Before And After ◽  
Tone Color

The scientific process was used to explain characterization and physical properties of the clay sample close to the ancient Nan kiln site. These samples were obtained from JQA, FQB, PQC and NQD. X-ray diffraction (XRD) and X-ray fluorescence (XRF) technique were used to determine the chemical composition and phase transformation before and after fired at 800-1250 °C. XRF result was confirmed that all clay samples mainly contained SiO2(>80 wt. %) XRD pattern indicated that quartz was the majority of phase in the all of them. High amount of Fe2O3(>1.6 wt. %) was related to the red-brown tone color. The clay sample could be fired up to 1280 °C without wrapping behavior; it was found that FQB clay had the highest firing resistance due to the maximum quartz content.

scholarly journals Spatiotemporal quantification of acoustic cell patterning using Voronoï tessellation

Lab on a Chip ◽  
2019 ◽  
Vol 19 (4) ◽  
pp. 562-573 ◽  
Author(s):  
James P. K. Armstrong ◽  
Stephanie A. Maynard ◽  
Isaac J. Pence ◽  
Amanda C. Franklin ◽  
Bruce W. Drinkwater ◽  
...  
Keyword(s):  
Image Analysis ◽  
Voronoi Tessellation ◽  
Cell Patterning ◽  
Analysis Method ◽  
Image Analysis Method

A new image analysis method based on Voronoï tessellation that enables quantitative and spatiotemporal characterization of acoustic cell patterning.

scholarly journals The Synthesis and Effect of Silver Nanoparticles on the Adsorption of Cu2+ from Aqueous Solutions

2020 ◽  
Vol 10 (14) ◽  
pp. 4840
Author(s):  
Ghadah M. Al-Senani ◽  
Nada Al-Kadhi
Keyword(s):  
Aqueous Solution ◽  
Freundlich Isotherm ◽  
Spherical Particles ◽  
Convolvulus Arvensis ◽  
X Ray ◽  
Nanoparticle Surface ◽  
Before And After ◽  
Adsorption Processes ◽  
Sem Analyses

The adsorption of Cu2+ ions from an aqueous solution using AgNPs synthesized from Convolvulus arvensis leaf extract was investigated. The characterization of AgNPs was investigated before and after the adsorption of Cu2+ ions via Fourier-transform infrared spectroscopy (FTIR), energy-dispersive X-ray spectroscopy (EDS), and scanning electron microscopy (SEM) analyses. The adsorbent contained various functional groups in addition to the AgNPs, which contributed to the Cu2+ ions adsorption. The silver nanoparticle surface consisted of spherical particles and deep pores, which adsorbed numerous Cu2+ ions. The influences of dosage, pH, and contact time on adsorption of 10 and 50 mg/L Cu2+ at 298 K, and initial Cu2+ concentrations at 298 and 323 K were studied. It was found that the highest percentage of Cu2+ ions adsorbed from an aqueous solution was 98.99%; the aqueous solution had 10 mg/L of Cu2+ ions and 0.2 g of AgNPs, at pH 12 and 298 K. A pseudo-second kinetics model offered the most accurate description of the process of adsorption. The process of Cu2+ adsorption more resembled a Langmuir rather than a Freundlich isotherm model, including chemical and physical mixed adsorption (mixed adsorption) processes, and was exothermic and spontaneous.

Characterization of silica polymorphs in kaolins by X-ray diffraction before and after phosphoric acid digestion and thermal treatment

2005 ◽  
Vol 552 (1-2) ◽  
pp. 201-206 ◽  
Author(s):  
Sibel Kahraman ◽  
Müşerref Önal ◽  
Yüksel Sarıkaya ◽  
İhsan Bozdoğan
Keyword(s):  
Thermal Treatment ◽  
Phosphoric Acid ◽  
Acid Digestion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Before And After

scholarly journals Characterization Of Microstructure And Selected Properties of SnSbCu Alloy After FSP

2021 ◽  
Author(s):  
Joanna Hrabia-Wiśnios ◽  
Beata Leszczyńska-Madej ◽  
Marcin Madej ◽  
Aleksandra Węglowska
Keyword(s):  
Flexural Strength ◽  
Diffraction Method ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
Linear Speed ◽  
X Ray ◽  
Friction Stir ◽  
Before And After ◽  
Bearing Alloy

Abstract The paper presents the results of research on the microstructure and selected mechanical properties of the SnSbCu bearing alloy after friction stir processing (FSP). The Whorl tool was used for modification; the process was carried out using two rotational speeds of the tool: 280 and 450 RPM and a constant linear speed of 355 mm/min. Microstructure studies were performed employing the techniques of light microscopy and scanning electron microscopy along with analysis of the chemical composition of micro-areas. Additionally, the phase composition was investigated by means of the X-ray diffraction method and statistical analysis of the precipitates present in the investigated alloy. In addition, hardness, flexural strength and uniaxial compression tests were performed before and after FSP modification. It was proved that using FSP to modify the SnSbCu alloy promotes refinement and homogenization of the microstructure, as well as improvement of the flexural strength, whereas no changes in the hardness level were found.

scholarly journals Image analysis method for heterogeneity and porosity characterization of biomimetic hydrogels

F1000Research ◽  
2020 ◽  
Vol 9 ◽  
pp. 1461
Author(s):  
Maryam Jamshidi ◽  
Cavus Falamaki
Keyword(s):  
Kernel Density ◽  
Analysis Method ◽  
Image Analysis Method ◽  
Morphological Transformation ◽  
Sem Images ◽  
Density Plot ◽  
Processing Procedure ◽  
Cryogenic Scanning Electron Microscopy ◽  
Porosity Characterization

This work presents an image processing procedure for characterization of porosity and heterogeneity of fully hydrated hydrogels based on the analysis of cryogenic scanning electron microscopy (cryo-SEM) images. An algorithm consisting of different filtering, morphological transformation, and thresholding steps to denoise the image whilst emphasizing the hydrogel fibres edges for extracting the pores features is explained. Finally, the information of hydrogel porosity and heterogeneity is presented in form of pore size distribution, spatial contours maps and kernel density dot plots. The obtained results reveal that a non-parametric kernel density plot effectively determines the spatial heterogeneity and porosity of the hydrogel.

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