scholarly journals Effect of Trace Magnesium Additions on the Dynamic Recrystallization in Cast Alloy 825 after One-Hit Hot-Deformation

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 36
Author(s):  
Munir Al-Saadi ◽  
Wangzhong Mu ◽  
Christopher N. Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson
Keyword(s):  
Service Life ◽  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Cast Alloy ◽  
True Strain ◽  
Peak Strain ◽  
Compression Tests ◽  
Electron Backscattered Diffraction ◽  
Hollomon Parameter ◽  
Test Conditions

Alloy 825 is widely used in several industries, but its useful service life is limited by both mechanical properties and corrosion resistance. The current work explores the effect of the addition of magnesium on the recrystallization and mechanical behavior of alloy 825 under hot compression. Compression tests were performed under conditions representative of typical forming processes: temperatures between 1100 and 1250 °C and at strain rates of 0.1–10 s−1 to a true strain of 0.7. Microstructural evolution was characterized by electron backscattered diffraction. Dynamic recrystallization was found to be more prevalent under all test conditions in samples containing magnesium, but not in all cases of conventional alloy 825. The texture direction ⟨101⟩ was the dominant orientation parallel to the longitudinal direction of casting (also the direction in which the samples were compressed) in samples that contained magnesium under all test conditions, but not in any sample that did not contain magnesium. For all deformation conditions, the peak stress was approximately 10% lower in material with the addition of magnesium. Furthermore, the differences in the peak strain between different temperatures are approximately 85% smaller if magnesium is present. The average activation energy for hot deformation was calculated to be 430 kJ mol−1 with the addition of magnesium and 450 kJ mol−1 without magnesium. The average size of dynamically recrystallized grains in both alloys showed a power law relation with the Zener–Hollomon parameter, DD~Z−n, and the exponent of value, n, is found to be 0.12. These results can be used to design optimized compositions and thermomechanical treatments of alloy 825 to maximize the useful service life under current service conditions. No experiments were conducted to investigate the effects of such changes on the service life and such experiments should now be performed.

scholarly journals Hot Deformation Behavior and Processing Maps of Fe-30Mn-0.11C Steel

Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1940 ◽  
Author(s):  
Jianmei Kang ◽  
Yuhui Wang ◽  
Zhimeng Wang ◽  
Yiming Zhao ◽  
Yan Peng ◽  
...  
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
True Strain ◽  
Peak Stress ◽  
Strain Rates ◽  
Processing Maps ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
High Deformation

Hot deformation behavior of Fe-30Mn-0.11C steel was investigated. Hot compression tests were carried out at various temperatures ranging from 800 °C to 1200 °C and at different strain rates of 0.01 s−1 to 10 s−1. The constitutive equation based on peak stress was established. Hot processing maps at different strains and recrystallization diagrams were also established and analyzed. The results show that dynamic recrystallization easily occur at high deformation temperatures and low strain rates. Safe and unstable zones are determined at the true strain of 0.6 and 0.7, and the hot deformation process parameters of partial dynamic recrystallization of the tested steel are also obtained.

Determination of Critical Stress for Dynamic Recrystallization of a High-Mn Austenitic TWIP Steel Micro-Alloyed with Vanadium

2016 ◽  
Vol 1812 ◽  
pp. 41-46
Author(s):  
Elvira García-Mora ◽  
Ignacio Mejía ◽  
Francisco Reyes-Calderón ◽  
José M. Cabrera
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Strain Hardening ◽  
Critical Stress ◽  
Twip Steel ◽  
True Strain ◽  
Compression Tests ◽  
Hollomon Parameter ◽  
Strain And Strain Rate ◽  
Twip Steels

ABSTRACTWhen high strength and high ductility are required, the Twinning Induced Plasticity steels are an excellent choice. Their mechanical advantages are perfectly known in the automotive industry. Then, they are currently deeply studied. During the deformation at high temperature, TWIP steel experiences dynamic recrystallization. This mechanism results from dislocation interactions, and it depends of temperature, stress, strain, and strain rate. Experimental data give the maximum stress reached by the material, but the critical stress which determinates the DRX onset must be calculated from the strain hardening rate. Both stress and strain change simultaneously, and this variation gives the analytic data to determine σc, which is located at the inflection point of θ-σ plot. The main purpose of this paper was to study how the chemical composition and the experimental parameters (temperature and strain rate) affect the DRX, by the calculation and analysis of the σc values. Hot compression tests were applied to a pair of TWIP steels to compare the DRX onset and its relationship with the vanadium addition. The experimental variables were temperature and strain rate. The true stress–true strain plots were used to calculate σc by cutting data up to a previous point before the σp value, then, a polynomial fit and derivation were applied. The Zener-Hollomon parameter (Z) versus the stresses (peak and critical) plots show how the micro-alloying element vanadium improves the strain hardening in the analyzed TWIP steels.

scholarly journals Hot Deformation Behaviour of Mn–Cr–Mo Low-Alloy Steel in Various Phase Regions

Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1255 ◽  
Author(s):  
Ivo Schindler ◽  
Petr Opěla ◽  
Petr Kawulok ◽  
Jaroslav Sojka ◽  
Kateřina Konečná ◽  
...  
Keyword(s):  
Flow Stress ◽  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Behaviour ◽  
True Strain ◽  
Coarse Grained ◽  
Peak Strain ◽  
Compression Tests ◽  
Wide Range ◽  
Hot Deformation Behaviour

The deformation behaviour of a coarse-grained as-cast medium-carbon steel, alloyed with 1.2% Mn, 0.8% Cr and 0.2% Mo, was studied by uniaxial compression tests for the strain rates of 0.02 s−1–20 s−1 in the unusually wide range of temperatures (650–1280 °C), i.e., in various phase regions including the region with predominant bainite content (up to the temperature of 757 °C). At temperatures above 820 °C, the structure was fully austenitic. The hot deformation activation energies of 648 kJ·mol−1 and 364 kJ·mol−1 have been calculated for the temperatures ≤770 °C and ≥770 °C, respectively. This corresponds to the significant increase of flow stress in the low-temperature bainitic region. Unique information on the hot deformation behaviour of bainite was obtained. The shape of the stress-strain curves was influenced by the dynamic recrystallization of ferrite or austenite. Dynamically recrystallized austenitic grains were strongly coarsened with decreasing strain rate and growing temperature. For the austenitic region, the relationship between the peak strain and the Zener–Hollomon parameter has been derived, and the phenomenological constitutive model describing the flow stress depending on temperature, true strain rate and true strain was developed. The model can be used to predict the forming forces in the seamless tubes production of the given steel.

Dynamic Recrystallization Behavior and Softening Kinetics in 3Mn-1.5Al TRIP Steels

2011 ◽  
Vol 287-290 ◽  
pp. 330-333 ◽  
Author(s):  
Adam Grajcar ◽  
Roman Kuziak
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Large Fraction ◽  
Solute Drag ◽  
Vacuum Induction Furnace ◽  
Compression Tests ◽  
Hollomon Parameter ◽  
Trip Steels ◽  
Dynamic Recrystallization Behavior ◽  
Parameter Values

Two 0.17C-3Mn-1.5Al-0.2Si-0.2Mo steels with and without Nb microaddition were melted in a vacuum induction furnace. The steels are characterized by bainitic-martensitic structures with large fraction of retained austenite. To design a thermomechanical treatment for steels with required multiphase structures a knowledge of their hot deformation resistance and softening kinetics is of primary importance. The paper presents the results of the compression tests carried out at various temperatures and strain rates using the Gleeble simulator. A softening kinetics was determined in a double-hit compression test. It was found that the dynamic recrystallization was a process controlling work hardening of steels except for hot deformation conditions characterized by the highest Zener-Hollomon parameter values. Nb microalloyed steel has higher flow stresses and peak strains than the steel without Nb. A solute drag effect of niobium results also in a slower recrystallization kinetics for the Nb containing steel.

Hot Deformation Behavior of Four Steels: A Comparative Study

2018 ◽  
Vol 140 (2) ◽  
Author(s):  
C. Menapace ◽  
N. Sartori ◽  
M. Pellizzari ◽  
G. Straffelini
Keyword(s):  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Rolling Process ◽  
Peak Strain ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Stress Strain ◽  
Hollomon Parameter ◽  
Experimental Values

The hot deformation behavior of four different steels in the as-cast condition was investigated by means of hot compression tests conducted at temperatures ranging from 1100 °C up to 1200 °C, and at strain rates in between 0.12 and 2.4 s−1. The primary focus of this work was to check the possibility to increase the strain rate during the rough preliminary working of the ingots, i.e., to adopt a rough rolling process in place of the more conventional rough forging. The second aim of the research was to study the influence of the different characteristics of these steels in their as-cast conditions on their hot deformation behavior. It was seen that in all deformation conditions, the stress–strain compression curves show a single peak, indicating the occurrence of dynamic recrystallization (DRX). The hot deformation behavior was studied in both the condition of dynamic recovery (DRV), modeling the stress–strain curves in the initial stage of deformation, and DRX. Data of modeling were satisfactorily employed to estimate the flow stress under different conditions of temperature and strain rate. The experimental values of the activation energy for hot deformation, QHW, were determined and correlated to the chemical composition of the steels; a power law curve was found to describe the relation of QHW and the total amount of substitutional elements of the steels. The critical strain for DRX, εc, was determined as a function of the Zener–Hollomon parameter and correlated to the peak strain, εp. A ratio εc/εp in the range 0.45–0.65 was found, which is in agreement with literature data. All this information is crucial for a correct design of the rough deformation process of the produced ingots.

The Constitutive Model for High Temperature Flow Behavior of SiC/6168Al Composite

2015 ◽  
Vol 1089 ◽  
pp. 37-41
Author(s):  
Jiang Wang ◽  
Sheng Li Guo ◽  
Sheng Pu Liu ◽  
Cheng Liu ◽  
Qi Fei Zheng
Keyword(s):  
Constitutive Model ◽  
Hot Deformation ◽  
Flow Behavior ◽  
Type Equation ◽  
Strain Rate Range ◽  
Compression Tests ◽  
Stress Strain ◽  
Hollomon Parameter ◽  
Proposed Model ◽  
Relationship Of

The hot deformation behavior of SiC/6168Al composite was studied by means of hot compression tests in the temperature range of 300-450 °C and strain rate range of 0.01-10 s-1. The constitutive model was developed to predict the stress-strain curves of this composite during hot deformation. This model was established by considering the effect of the strain on material constants calculated by using the Zenter-Hollomon parameter in the hyperbolic Arrhenius-type equation. It was found that the relationship of n, α, Q, lnA and ε could be expressed by a five-order polynomial. The stress-strain curves obtained by this model showed a good agreement with experimental results. The proposed model can accurately describe the hot flow behavior of SiC/6168Al composite, and can be used to numerically analyze the hot forming processes.

Constitutive Modeling for Flow Stress Behavior of Nimonic 80A Superalloy During Hot Deformation Process

2016 ◽  
Vol 35 (3) ◽  
pp. 327-336 ◽  
Author(s):  
Sendong Gu ◽  
Liwen Zhang ◽  
Chi Zhang ◽  
Wenfei Shen
Keyword(s):  
Flow Stress ◽  
Constitutive Model ◽  
Hot Deformation ◽  
Critical Strain ◽  
Volume Fraction ◽  
Constitutive Models ◽  
Avrami Equation ◽  
Peak Strain ◽  
Compression Tests ◽  
Nimonic 80A

AbstractThe hot deformation characteristics of nickel-based alloy Nimonic 80A were investigated by isothermal compression tests conducted in the temperature range of 1,000–1,200°C and the strain rate range of 0.01—5 s–1on a Gleeble-1500 thermomechanical simulator. In order to establish the constitutive models for dynamic recrystallization (DRX) behavior and flow stress of Nimonic 80A, the material constantsα,nand DRX activation energyQin the constitutive models were calculated by the regression analysis of the experimental data. The dependences of initial stress, saturation stress, steady-state stress, dynamic recovery (DRV) parameter, peak strain, critical strain and DRX grain size on deformation parameters were obtained. Then, the Avrami equation including the critical strain for DRX and the peak strain as a function of strain was established to describe the DRX volume fraction. Finally, the constitutive model for flow stress of Nimonic 80A was developed in DRV region and DRX region, respectively. The flow stress values predicted by the constitutive model are in good agreement with the experimental ones, which indicates that the constitutive model can give an accurate estimate for the flow stress of Nimonic 80A under the deformation conditions.

Constitutive Equation for 3104 Alloy at High Temperatures in Consideration of Strain

2016 ◽  
Vol 35 (6) ◽  
pp. 599-605 ◽  
Author(s):  
Fuqiang Zhen ◽  
Jianlin Sun ◽  
Jian Li
Keyword(s):  
Hot Deformation ◽  
Flow Behavior ◽  
Temperature Correction ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Element Analysis ◽  
Hollomon Parameter ◽  
The Finite Element Analysis ◽  
Effects Of Temperature

AbstractThe flow behavior of 3104 aluminum alloy was investigated at temperatures ranging from 250°C to 500°C, and strain rates from 0.01 to 10 s−1 by isothermal compression tests. The true stress–strain curves were obtained from the measured load–stroke data and then modified by friction and temperature correction. The effects of temperature and strain rate on hot deformation behavior were represented by Zener–Hollomon parameter including Arrhenius term. Additionally, the influence of strain was incorporated considering the effect of strain on material constants. The derived constitution equation was applied to the finite element analysis of hot compression. The results show that the simulated force is consistent with the measured one. Consequently, the developed constitution equation is valid and feasible for numerical simulation in hot deformation process of 3104 alloy.

Study on Dynamic Recrystallization Behavior in Deformed Austenite of 52100 Steel by Using JMAK-Model

2013 ◽  
Vol 275-277 ◽  
pp. 1833-1837
Author(s):  
Ke Lu Wang ◽  
Shi Qiang Lu ◽  
Xin Li ◽  
Xian Juan Dong
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Volume Fraction ◽  
True Strain ◽  
Strain And Strain Rate ◽  
Average Grain Size ◽  
Dynamic Recrystallization Behavior ◽  
Simulation And Experiment ◽  
Good Agreement

A Johnson-Mehl-Avrami-Kolmogorov (JMAK)-model was established for dynamic recrystallization in hot deformation process of 52100 steel. The effects of hot deformation temperature, true strain and strain rate on the microstructural evolution of the steel were physically studied by using Gleeble-1500 thermo-mechanical simulator and the experimental results were used for validation of the JMAK-model. Through simulation and experiment, it is found that the predicted results of DRX volume fraction, DRX grain size and average grain size are in good agreement with the experimental ones.

Characteristics of Dynamic Recrystallization during Hot Deformation for High Nitrogen Stainless Steels

2012 ◽  
Vol 715-716 ◽  
pp. 115-121
Author(s):  
Hai Wen Luo ◽  
Xu Dong Fang ◽  
Rui Zhen Wang ◽  
Zhan Yin Diao
Keyword(s):  
Dynamic Recrystallization ◽  
Stainless Steels ◽  
Hot Deformation ◽  
Strain Rates ◽  
Peak Strain ◽  
High Nitrogen ◽  
Flow Curves ◽  
Grain Sizes ◽  
Nitrogen Contents ◽  
High Nitrogen Stainless Steel

Dynamic recrystallization was studied for the stainless steels with nitrogen contents of 0.56% to 1.08% during hot deformation at temperatures of 900~1200 with strain rates ranging from 0.003 to 42 s-1. It was found that flow stress could increase remarkably with increasing nitrogen content. Flow curves during the deformation by 0.1~42/s at temperatures of 900~1200°C show a single peak, indicating the occurrence of dynamic recrystallization during deformation. The peak strain seems to decrease with increasing N content, suggesting that higher content of N facilitates dynamic recrystallization. The quenched microstructures were analyzed by optical microscopy, EBSD and TEM. The recrystallized grain sizes on the quenched specimens were measured and its dependence on temperature and strain rate was analyzed. At high temperature, continuously dynamically recrystallized microstructures were observed; whilst at low temperature, necklace-like partially recrystallized microstructures were found. Key words: High nitrogen stainless steel; dynamic recrystallization; stress-strain curves

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