Determination of Critical Stress for Dynamic Recrystallization of a High-Mn Austenitic TWIP Steel Micro-Alloyed with Vanadium

2016 ◽  
Vol 1812 ◽  
pp. 41-46
Author(s):  
Elvira García-Mora ◽  
Ignacio Mejía ◽  
Francisco Reyes-Calderón ◽  
José M. Cabrera
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Strain Hardening ◽  
Critical Stress ◽  
Twip Steel ◽  
True Strain ◽  
Compression Tests ◽  
Hollomon Parameter ◽  
Strain And Strain Rate ◽  
Twip Steels

ABSTRACTWhen high strength and high ductility are required, the Twinning Induced Plasticity steels are an excellent choice. Their mechanical advantages are perfectly known in the automotive industry. Then, they are currently deeply studied. During the deformation at high temperature, TWIP steel experiences dynamic recrystallization. This mechanism results from dislocation interactions, and it depends of temperature, stress, strain, and strain rate. Experimental data give the maximum stress reached by the material, but the critical stress which determinates the DRX onset must be calculated from the strain hardening rate. Both stress and strain change simultaneously, and this variation gives the analytic data to determine σc, which is located at the inflection point of θ-σ plot. The main purpose of this paper was to study how the chemical composition and the experimental parameters (temperature and strain rate) affect the DRX, by the calculation and analysis of the σc values. Hot compression tests were applied to a pair of TWIP steels to compare the DRX onset and its relationship with the vanadium addition. The experimental variables were temperature and strain rate. The true stress–true strain plots were used to calculate σc by cutting data up to a previous point before the σp value, then, a polynomial fit and derivation were applied. The Zener-Hollomon parameter (Z) versus the stresses (peak and critical) plots show how the micro-alloying element vanadium improves the strain hardening in the analyzed TWIP steels.

scholarly journals Effect of Trace Magnesium Additions on the Dynamic Recrystallization in Cast Alloy 825 after One-Hit Hot-Deformation

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 36
Author(s):  
Munir Al-Saadi ◽  
Wangzhong Mu ◽  
Christopher N. Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson
Keyword(s):  
Service Life ◽  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Cast Alloy ◽  
True Strain ◽  
Peak Strain ◽  
Compression Tests ◽  
Electron Backscattered Diffraction ◽  
Hollomon Parameter ◽  
Test Conditions

Alloy 825 is widely used in several industries, but its useful service life is limited by both mechanical properties and corrosion resistance. The current work explores the effect of the addition of magnesium on the recrystallization and mechanical behavior of alloy 825 under hot compression. Compression tests were performed under conditions representative of typical forming processes: temperatures between 1100 and 1250 °C and at strain rates of 0.1–10 s−1 to a true strain of 0.7. Microstructural evolution was characterized by electron backscattered diffraction. Dynamic recrystallization was found to be more prevalent under all test conditions in samples containing magnesium, but not in all cases of conventional alloy 825. The texture direction ⟨101⟩ was the dominant orientation parallel to the longitudinal direction of casting (also the direction in which the samples were compressed) in samples that contained magnesium under all test conditions, but not in any sample that did not contain magnesium. For all deformation conditions, the peak stress was approximately 10% lower in material with the addition of magnesium. Furthermore, the differences in the peak strain between different temperatures are approximately 85% smaller if magnesium is present. The average activation energy for hot deformation was calculated to be 430 kJ mol−1 with the addition of magnesium and 450 kJ mol−1 without magnesium. The average size of dynamically recrystallized grains in both alloys showed a power law relation with the Zener–Hollomon parameter, DD~Z−n, and the exponent of value, n, is found to be 0.12. These results can be used to design optimized compositions and thermomechanical treatments of alloy 825 to maximize the useful service life under current service conditions. No experiments were conducted to investigate the effects of such changes on the service life and such experiments should now be performed.

The Mechanical and Deformation Behavior of TWIP Steel Prepared by Directional Solidification

2014 ◽  
Vol 783-786 ◽  
pp. 761-765 ◽  
Author(s):  
Dan Wang ◽  
Kun Wang ◽  
Zi Mu Shi ◽  
Fu Sheng Han
Keyword(s):  
Mechanical Properties ◽  
Strain Hardening ◽  
Twip Steel ◽  
True Strain ◽  
Longitudinal Direction ◽  
True Stress ◽  
Grain Structure ◽  
Directionally Solidified ◽  
Twip Steels ◽  
Columnar Grain

A directionally solidified TWIP steel (Fe-25Mn-2.5Al-2.5Si) was prepared by liquid metal cooling technology. The microstructure and mechanical behavior were examined and compared with usually solidified samples. The directionally solidified TWIP steel shows a typical columnar grain structure, and the maximum true stress and true strain along the longitudinal direction of the sample are 1060MPa and 71% respectively. As a comparison, the usually solidified samples shows an equiaxed grain microstructure with the maximum true stress and true strain of only 994MPa and 58%, respectively. Moreover, the two solidification modes also lead to very different strain hardening behavior, particularly in the changes of strain hardening rate with strain. This suggests that the grain boundary plays a key role in the mechanical properties of TWIP steels, and changing the grain boundaries can be effective to improve the comprehensive mechanical properties of TWIP steels.

Effect of Strain Rate on the Microstructures and Properties of Hot–Rolled TWIP Steel in the Solution Condition

2012 ◽  
Vol 430-432 ◽  
pp. 256-259 ◽  
Author(s):  
Yang Yang ◽  
Chun Fu Li ◽  
Kai Hong Song
Keyword(s):  
Strain Rate ◽  
Strain Hardening ◽  
Twip Steel ◽  
Tensile Tests ◽  
Strain Rate Range ◽  
Strain Hardening Exponent ◽  
Solution Condition ◽  
Twip Steels ◽  
Hot Rolled ◽  
Strain Hardening Behavior

TWIP steel containing 0.21% C, 24.4% Mn, 0.9% Si, 1.84% Al, 4.61% Cr, 1.89% Ni, 0.41% Mo and 0.012% Nb was investigated. Tensile tests of this steel were performed in the strain rate range of 10−4–10−3 s−1. Results indicate that tensile properties of TWIP steel at room temperature are sensitive to strain rate in the studied range. Analyses on the relationship between strain–hardening exponent and strain rates show that the formation of twins during deformation greatly affects the strain–hardening behavior of TWIP steels.

Determination of the Onset of the Dynamic Recystallization of a 7075 Al Alloy

2013 ◽  
Vol 752 ◽  
pp. 105-114 ◽  
Author(s):  
Tamás Mikó ◽  
Peter Barkoczy
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Critical Stress ◽  
Al Alloy ◽  
Strain Rates ◽  
Compression Tests ◽  
Critical Stresses ◽  
Work Hardening Rate ◽  
Initial States

This paper presents an investigation about the occurrence of the dynamic recrystallization (DRX) during hot forming. Two 7075 aluminum alloy samples in different initial states were examined by compression tests at temperatures between 573 K and 723 K and constant strain rates ranging from 0.002 to 2 (s-1) with the maximum strain of 0.5 mm/mm. The activation energies of the examined aluminium were calculated, being 137.7 kJ/mol and 142.4 kJ/mol. The critical stresses and strains for the initiation of the dynamic recrystallization were determined using a numerical method based on the changes of the work hardening rate (θ) as a function of the flow stress (σ) or a strain (ε), respectively. Based on the micrographs taken after the deformations it was revealed that in some cases only dinamyc recovery (DRV) whereas in others DRX occurred under the applied examination conditions. The critical stress which belongs to the onset of the DRX or the DRV depend on the temperature, the strain rate, and the initial grain size. The critical and maximal stresses and the corresponding strain values at different conditions were determined. In the examined range of deformation, temperature and strain rate, the critical rations are σ_c/σ_p= (0.93-0.99) and εc/ εp = (0.3-0.74), respectively.

Mechanisms of Dynamic Recrystallization in Coarse Columnar-Grained Cu-Sn-P Alloy

2012 ◽  
Vol 715-716 ◽  
pp. 586-592
Author(s):  
Hiromi Miura ◽  
Masato Watanabe ◽  
Takashi Shirai ◽  
Akihiko Ishibashi
Keyword(s):  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Boundary Migration ◽  
True Strain ◽  
Compression Tests ◽  
Model Sample ◽  
Annealing Twins ◽  
Preferential Nucleation ◽  
Increasing Temperature

Dynamic recrystallization (DRX) behavior in a coarse columnar-grained Cu-0.65Sn-0.025P and Cu-0.025P (mass%) alloys were systematically investigated by compression tests at temperatures between 1073 K and 1253 K and at true strain rates from 2 x 10-4s-1to 2 x 10-1s-1in vacuum. As a model sample, an orientation-controlled bicrystal having [0 1 twist 18oboundary was prepared and also hot deformed. Appearance of the peaks stress, where DRX onsets, was much delayed in Cu-Sn-P alloy compared with that in Cu-0.025P alloy. The onset of DRX was, therefore, obviously impeded by the small addition of Sn to Cu-P. While nucleation of new grains took place almost at random in Cu-Sn-P when strain rate was high enough, it tended to appear more preferentially at grain boundary with decreasing strain rate and with increasing temperature. The most of new grains were annealing twins formed behind the migrating grain boundary. Because grain boundary migration took place more extensively with increasing temperature and with decreasing strain rate, the preferential nucleation at grain boundary became more significant.

Dynamic Recrystallization Behavior of Pure Titanium

2014 ◽  
Vol 852 ◽  
pp. 66-70 ◽  
Author(s):  
Juan Hua Su ◽  
Ya Wei Han ◽  
Feng Zhang Ren ◽  
Zhi Qiang Chen
Keyword(s):  
Flow Stress ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
True Strain ◽  
Pure Titanium ◽  
Avrami Equation ◽  
Test Machine ◽  
Commercially Pure Titanium ◽  
Compression Tests ◽  
Commercially Pure

The dynamic recrystallization of commercially pure titanium was investigated by compression tests on Gleeble-1500D thermal simulation test machine at temperature of 700950 °C and strain rate of 0. 015 s1. The total compression deformation is 0.7(true strain). The kinetics of dynamic recrystallization of commercially pure titanium at 950 °C was modeled by Avrami equation. The results show that the dynamic recovery and recrystallization obviously occur during compression. The flow stress increases to a peak value and gradually decreases to a steady state. The flow stress is decreased with the increase of deformation temperature and it is increased with the increase of strain rate. The Avrami kinetics model of dynamic recrystallization of commercially pure titanium at 950 °C is obtained .

scholarly journals Application of the Strain Compensation Model and Processing Maps for Description of Hot Deformation Behavior of Metastable β Titanium Alloy

Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 2021
Author(s):  
Oleksandr Lypchanskyi ◽  
Tomasz Śleboda ◽  
Aneta Łukaszek-Sołek ◽  
Krystian Zyguła ◽  
Marek Wojtaszek
Keyword(s):  
Titanium Alloy ◽  
Strain Rate ◽  
Flow Behavior ◽  
Microstructural Analysis ◽  
Calculated Data ◽  
Processing Temperature ◽  
Processing Maps ◽  
Compression Tests ◽  
Strain And Strain Rate ◽  
Average Absolute Relative Error

The flow behavior of metastable β titanium alloy was investigated basing on isothermal hot compression tests performed on Gleeble 3800 thermomechanical simulator at near and above β transus temperatures. The flow stress curves were obtained for deformation temperature range of 800–1100 °C and strain rate range of 0.01–100 s−1. The strain compensated constitutive model was developed using the Arrhenius-type equation. The high correlation coefficient (R) as well as low average absolute relative error (AARE) between the experimental and the calculated data confirmed a high accuracy of the developed model. The dynamic material modeling in combination with the Prasad stability criterion made it possible to generate processing maps for the investigated processing temperature, strain and strain rate ranges. The high material flow stability under investigated deformation conditions was revealed. The microstructural analysis provided additional information regarding the flow behavior and predominant deformation mechanism. It was found that dynamic recovery (DRV) was the main mechanism operating during the deformation of the investigated β titanium alloy.

Study on Dynamic Recrystallization Behavior in Deformed Austenite of 52100 Steel by Using JMAK-Model

2013 ◽  
Vol 275-277 ◽  
pp. 1833-1837
Author(s):  
Ke Lu Wang ◽  
Shi Qiang Lu ◽  
Xin Li ◽  
Xian Juan Dong
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Volume Fraction ◽  
True Strain ◽  
Strain And Strain Rate ◽  
Average Grain Size ◽  
Dynamic Recrystallization Behavior ◽  
Simulation And Experiment ◽  
Good Agreement

A Johnson-Mehl-Avrami-Kolmogorov (JMAK)-model was established for dynamic recrystallization in hot deformation process of 52100 steel. The effects of hot deformation temperature, true strain and strain rate on the microstructural evolution of the steel were physically studied by using Gleeble-1500 thermo-mechanical simulator and the experimental results were used for validation of the JMAK-model. Through simulation and experiment, it is found that the predicted results of DRX volume fraction, DRX grain size and average grain size are in good agreement with the experimental ones.

Critical Strain for the Initiation of Dynamic Recrystallization in a Ni-Fe Base Alloy

2004 ◽  
Vol 449-452 ◽  
pp. 577-580
Author(s):  
Young Sang Na ◽  
Young Mok Rhyim ◽  
J.Y. Lee ◽  
Jae Ho Lee
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Critical Strain ◽  
Base Alloy ◽  
Strain Rate Range ◽  
Boundary Phase ◽  
Alloy 718 ◽  
Compression Tests ◽  
Temperature Range ◽  
Critical Strains

In order to quantitatively analyze the critical strain for the initiation of dynamic recrystallization in Ni-Fe-based Alloy 718, a series of uniaxial compression tests was conducted in the temperature range 927°C - 1066°C and the strain rate range 5 x 10-4s-1- 5 s-1with varying initial grain size. The critical strains were graphically determined based on one parameter approach and microscopically confirmed. The effect of γ'' (matrix-hardening phase) and δ (grain boundary phase)on the critical strain was simply discussed. The constitutive model for the critical strain of Alloy 718 was constructed using the experimental data obtained from the higher strain rate and the temperature range between 940°C and 1040°C.

scholarly journals Hot Deformation Behavior of a Ni-Based Superalloy with Suppressed Precipitation

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 605
Author(s):  
Franco Lizzi ◽  
Kashyap Pradeep ◽  
Aleksandar Stanojevic ◽  
Silvana Sommadossi ◽  
Maria Cecilia Poletti
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Hot Deformation ◽  
Strain Rates ◽  
Compression Tests ◽  
Deformation Bands ◽  
Stress Softening ◽  
Relative Stress ◽  
The Matrix ◽  
Thermomechanical Processes

Inconel®718 is a well-known nickel-based super-alloy used for high-temperature applications after thermomechanical processes followed by heat treatments. This work describes the evolution of the microstructure and the stresses during hot deformation of a prototype alloy named IN718WP produced by powder metallurgy with similar chemical composition to the matrix of Inconel®718. Compression tests were performed by the thermomechanical simulator Gleeble®3800 in a temperature range from 900 to 1025 °C, and strain rates scaled from 0.001 to 10 s−1. Flow curves of IN718WP showed similar features to those of Inconel®718. The relative stress softening of the IN718WP was comparable to standard alloy Inconel®718 for the highest strain rates. Large stress softening at low strain rates may be related to two phenomena: the fast recrystallization rate, and the coarsening of micropores driven by diffusion. Dynamic recrystallization grade and grain size were quantified using metallography. The recrystallization grade increased as the strain rate decreased, although showed less dependency on the temperature. Dynamic recrystallization occurred after the formation of deformation bands at strain rates above 0.1 s−1 and after the formation of subgrains when deforming at low strain rates. Recrystallized grains had a large number of sigma 3 boundaries, and their percentage increased with strain rate and temperature. The calculated apparent activation energy and strain rate exponent value were similar to those found for Inconel®718 when deforming above the solvus temperature.

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