scholarly journals Effects of Hot Isostatic Pressing and Heat Treatment on the Microstructure and Mechanical Properties of Cast TiAl Alloy

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1156
Author(s):  
Wen Yu ◽  
Jianxin Zhou ◽  
Yajun Yin ◽  
Xin Feng ◽  
Hai Nan ◽  
...  

Hot isostatic pressing (HIP) and subsequent heat-treatments (HT) are necessary for titanium aluminide (TiAl) casting components. But there are few studies carefully comparing the microstructure changes from the initial as-cast condition to the final heat-treated condition. In this study, the microstructures of Ti-47Al-2Cr-2Nb (at%) alloy in the as-cast, as-HIPed and as-heat-treated conditions were characterized by optical microscopy and scanning electron microscopy. The mechanical properties after HTs were determined by the tensile tests at 700 °C. The results show that after HIP and HTs, all the microstructures exhibit a nearly lamellar (NL) structure and can be divided into an edge region and a central area. The microstructure after HIP in the edge region is normal, while distorted lamellae and many fine recrystallized grains exist in the central area. The yield strengths after three HTs are nearly the same, but the elongation after the HT at 1310 °C is much more than that after HTs at 1185 °C and 1280 °C. A refinement of colony size induced by distorted lamellae in as-HIPed condition is considered responsible for the great improvement in elongation.

Metals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 753 ◽  
Author(s):  
Kanwal Chadha ◽  
Yuan Tian ◽  
John Spray ◽  
Clodualdo Aranas

In this work, the microstructural features and mechanical properties of an additively manufactured 316L stainless steel have been determined. Three types of samples were characterized: (i) as printed (AP), (ii) annealing heat treated (AHT), and (iii) hot isostatic pressed and annealing heat treated (HIP + AHT). Microstructural analysis reveals that the AP sample formed melt pool boundaries with nano-scale cellular structures. These structures disappeared after annealing heat treatment and hot isostatic pressing. The AP and AHT samples have similar grain morphologies; however, the latter has a lower dislocation density and contains precipitates. Conversely, the HIP + AHT sample displays polygon-shaped grains with twin structures; a completely different morphology compared to the first two samples. Optical micrography reveals that the application of hot isostatic pressing reduces the porosity generated after laser processing. The tensile strengths of all the samples are comparable (about 600 MPa); however, the elongation of the HIP + AHT sample (48%) was superior to that of other two samples. The enhanced ductility of the HIP + AHT sample, however, resulted in lower yield strength. Based on these findings, annealing heat treatment after hot isostatic pressing was found to improve the ductility of as-printed 316L stainless steel by as much as 130%, without sacrificing tensile strength, but the sample may have a reduced (40%) yield strength. The tensile strength determined here has been shown to be higher than that of the hot isostatic pressed, additively manufactured 316L stainless steel available from the literature.


2019 ◽  
Vol 822 ◽  
pp. 569-574
Author(s):  
Evgenii Borisov ◽  
Viktoria Vladislavovna Sokolova ◽  
Alexey Orlov ◽  
Pu Guang Ji

Geometric features of mesh structures allow them to be used as a material for medical purposes. In this paper, the study of the properties of lattice structures, performed by selective laser melting was carried out. The range of high accuracy of manufactured samples and microstructure was determinated. The results of changes in porosity and mechanical properties after hot isostatic pressing in comparison with cortical bone and heat treated material and microstructure of samples are represented.


Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 884
Author(s):  
A-Ra Jo ◽  
Ji-Seob An ◽  
Sun-Hyung Kim ◽  
Myeong-Sik Jeong ◽  
Young-Hoon Moon ◽  
...  

Tungsten carbide-cobalt (WC-Co) alloys have various mechanical properties according to their Co content and manufacturing method. High-strength materials such as WC-Co alloys are usually manufactured using various sintering methods. In this study, WC-Co was compared according to the Co content and manufacturing method using the sinter-hot isostatic pressing process. Furthermore, an additional test was performed to investigate the effect of post-hot isostatic pressing (HIP) treatment on the mechanical properties. To compare tensile strength, threaded end and shoulder end specimens are generally applied in axial tensile testing with hard metals. However, it is extremely difficult to shape WC-Co by machining. A tensile testing jig for a shoulder end specimen is, therefore, proposed. Tensile tests were conducted using the proposed jig, and microstructure, hardness, and impact tests were carried out to compare the mechanical properties. The microstructure evolution was obtained by decreasing the Co content and applying the HIP treatment, resulting in changes in Young’s modulus and strength. The results indicated that the proposed jig of the axial tensile test could be applied to the extremely hard WC-Co, and the mechanical properties of WC-Co could be modified by the Co content and HIP treatment control.


Author(s):  
Janusz Kluczynski ◽  
Lucjan Śnieżek ◽  
Krzysztof Grzelak ◽  
Artur Oziębło ◽  
Krzysztof Perkowski ◽  
...  

Industries that rely on additive manufacturing of metallic elements, especially biomedical companies, require material science-based knowledge of how process parameters and methods affect element properties, but such phenomena are incompletely understood. In this study, we investigated the influence of selective laser melting (SLM) process parameters and additional heat treatment on mechanical properties. The research included structural analysis of residual stress, microstructure, and scleronomic hardness in low-depth measurements. Tensile tests with element deformation analysis using digital image correlation (DIC) were performed as well. Experiment results showed it was possible to observe the porosity growth mechanism and its influence on material strength. Elements manufactured with 20% lower energy density had almost half the elongation, which was directly connected with porosity growth during energy density reduction. Hot isostatic pressing (HIP) treatment allowed for a significant reduction of porosity and helped achieve properties similar to elements manufactured using different levels of energy density.


2021 ◽  
pp. 22-30
Author(s):  
A.I. Vasilev ◽  
◽  
P.V. Panin ◽  
S.V. Putyrskiy ◽  
A.M. Rogalev ◽  
...  

Presents the results of the investigation of the influence of hot isostatic pressing and heat treatment on the structure and mechanical properties during tension of synthesized workpieces obtained by selective laser alloying from a metal-powder composition of VT6 alloy. The blanks were subjected to heat treatment at various temperatures in the state after synthesis, as well after HIP. The influence of different heat treatment modes was assessed by the results of tensile tests and structural researches.


2007 ◽  
Vol 336-338 ◽  
pp. 1214-1217
Author(s):  
Wen Jun Liu ◽  
Yong Zheng ◽  
Wei Hao Xiong

Several nano-composite Ti(C, N)-based cermets were produced by vacuum sintering and subsequently heat-treated with hot isostatic pressing (HIP) in Ar. The influence of nano powder additions on the microstructures and properties of cermets has been studied It was found that, with increasing nano powder additions, the microstructures became finer and even, the amount of small grains with inner-rim, outer-rim and those with “white core-gray rim” increased. When nano TiC and TiN additions accounted for 20wt% of the amount of TiC and TiN, the samples exhibited the best properties. Some nano particles were found to distribute at (along?) the grain boundaries of cermets, which strengthened the grain boundaries and improved the mechanical properties of Ti(C, N)-based cermets.


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