Nano Indentation Response of Various Thin Films Used for Tribological Applications

2014 ◽  
pp. 62-88
Author(s):  
Manish Roy
Keyword(s):  
Thin Films ◽  
Elastic Modulus ◽  
Nano Indentation ◽  
Lubricating Film ◽  
Indentation Response

Various thin films used for tribological applications are classified under four heads. Based on their load vs. displacement curves, which have some characteristics features, the ratio of nanohardness to elastic modulus and the ratio of cube of nanohardness to square of elastic modulus are evaluated in this chapter. It is demonstrated that depending on the type of film used, these ratios vary within a certain range. For soft self-lubricating films, these ratios are very low; whereas for hard self-lubricating film, these ratios are quite high.

Compositional and phase dependence of elastic modulus of crystalline and amorphous Hf1-xZrxO2 thin films

2021 ◽  
Vol 118 (10) ◽  
pp. 102901
Author(s):  
Shelby S. Fields ◽  
David H. Olson ◽  
Samantha T. Jaszewski ◽  
Chris M. Fancher ◽  
Sean W. Smith ◽  
...  
Keyword(s):  
Thin Films ◽  
Elastic Modulus ◽  
Phase Dependence

Direct Comparison of Three Buckling-Based Methods to Measure the Elastic Modulus of Nanobiocomposite Thin Films

2021 ◽  
Author(s):  
Taylor C. Stimpson ◽  
Daniel A. Osorio ◽  
Emily D. Cranston ◽  
Jose M. Moran-Mirabal
Keyword(s):  
Thin Films ◽  
Elastic Modulus

Determining the elastic modulus of thin films using a buckling-based method: computational study

2009 ◽  
Vol 42 (17) ◽  
pp. 175506 ◽  
Author(s):  
Xiu-Peng Zheng ◽  
Yan-Ping Cao ◽  
Bo Li ◽  
Xi-Qiao Feng ◽  
Hanqing Jiang ◽  
...  
Keyword(s):  
Thin Films ◽  
Elastic Modulus ◽  
Computational Study

Elastic Modulus of Pb/Sn Solder Joints in Microelectronics

2002 ◽  
Author(s):  
Cemal Basaran ◽  
Jianbin Jiang
Keyword(s):  
Grain Size ◽  
Elastic Modulus ◽  
Single Crystal ◽  
Solder Alloy ◽  
Ultrasonic Testing ◽  
Heterogeneous Materials ◽  
Testing Methods ◽  
Nano Indentation ◽  
Deformation Kinetics ◽  
Kinetics Of

Young’s modulus (E) values published in literature for the eutectic Pb37/Sn63 and near eutectic Pb40/Sn60 solder alloy vary significantly. One reason for this discrepancy is different testing methods for highly rate sensitive heterogeneous materials, like Pb/Sn alloys, yield different results. In this paper, we study different procedures used to obtain the elastic modulus; analytically, by single crystal elasticity and experimentally by ultrasonic testing and Nano indentation. We compare these procedures and propose a procedure for elastic modulus determination. The deformation kinetics of the Pb/Sn solder alloys is discussed at the grain size level.

Impact of Surface-Modified Nanoparticles on Glass Transition Temperature and Elastic Modulus of Polymer Thin Films

2007 ◽  
Vol 40 (22) ◽  
pp. 7755-7757 ◽  
Author(s):  
Jong-Young Lee ◽  
Kristin E. Su ◽  
Edwin P. Chan ◽  
Qingling Zhang ◽  
Todd Emrick ◽  
...  
Keyword(s):  
Thin Films ◽  
Glass Transition ◽  
Elastic Modulus ◽  
Transition Temperature ◽  
Glass Transition Temperature ◽  
Polymer Thin Films ◽  
Surface Modified ◽  
Surface Modified Nanoparticles

Growth, Structural and Mechanical Characterization and Reliability of Chemical Vapor Deposited Co and Co3O4 Thin Films as Candidate Materials for Sensing Applications

2011 ◽  
Vol 495 ◽  
pp. 108-111 ◽  
Author(s):  
Vasiliki P. Tsikourkitoudi ◽  
Elias P. Koumoulos ◽  
Nikolaos Papadopoulos ◽  
Costas A. Charitidis
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Elastic Modulus ◽  
Data Storage ◽  
Mechanical Stability ◽  
Chemical Vapor ◽  
Magnetic Sensors ◽  
Functional Coatings ◽  
Sensing Applications ◽  
Chemical Vapor Deposited

The adhesion and mechanical stability of thin film coatings on substrates is increasingly becoming a key issue in device reliability as magnetic and storage technology driven products demand smaller, thinner and more complex functional coatings. In the present study, chemical vapor deposited Co and Co3O4thin films on SiO2and Si substrates are produced, respectively. Chemical vapor deposition is the most widely used deposition technique which produces thin films well adherent to the substrate. Co and Co3O4thin films can be used in innovative applications such as magnetic sensors, data storage devices and protective layers. The produced thin films are characterized using nanoindentation technique and their nanomechanical properties (hardness and elastic modulus) are obtained. Finally, an evaluation of the reliability of each thin film (wear analysis) is performed using the hardness to elastic modulus ratio in correlation to the ratio of irreversible work to total work for a complete loading-unloading procedure.

Modelling the nano indentation behaviour of recast layer and heat affected zone on reverse micro EDMed hemispherical feature

2021 ◽  
pp. 1-15
Author(s):  
Tribeni Roy ◽  
Anuj Sharma ◽  
Prabhat Ranjan ◽  
R. Balasubramaniam
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Heat Affected Zone ◽  
Parent Material ◽  
Recast Layer ◽  
Machined Surface ◽  
Nano Indentation ◽  
Fea Simulation ◽  
Load Displacement ◽  
Good Agreement

Abstract Electrical discharge machined surfaces inherently possess recast layer on the surface with heat affected zone (HAZ) beneath it and these have a detrimental effect on the mechanical properties viz. hardness, elastic modulus, etc. It is very difficult to experimentally characterise each machined surface. Therefore, an attempt is made in this study to numerically calculate the mechanical properties of the parent material, HAZ and the recast layer on a hemispherical protruded micro feature fabricated by reverse micro EDM (RMEDM). In the 1st stage, nano indentation was performed to experimentally determine the load-displacement plots, elastic modulus and hardness of the parent material, HAZ and the recast layer. In the 2nd stage, FEA simulation was carried out to mimic the nano indentation process and determine the load-displacement plots for all the three cases viz. parent material, recast layer and HAZ. Results demonstrated that the load'displacement plots obtained from numerical model in each case was in good agreement with that of the experimental curves. Based on simulated load-displacement plots, hardness was also calculated for parent material, HAZ and the recast layer. A maximum of 11% error was observed between simulated values of hardness and experimentally determined values.

Nanoclay-reinforced Polyacrylamide Composite: Synthesis, Structural and Mechanical Characterization

2009 ◽  
Vol 1239 ◽  
Author(s):  
Yong Sun ◽  
Zaiwang Huang ◽  
Xiaodong Li
Keyword(s):  
Thin Films ◽  
Deformation Behavior ◽  
Mechanical Characterization ◽  
Interfacial Strength ◽  
Localized Deformation ◽  
Nano Indentation ◽  
Atomic Force ◽  
Nanocomposite Thin Films ◽  
Synthesized Materials

AbstractA facile electrophoretic deposition method was successfully applied to achieve novel nanoclay-reinforced polyacrylamide nanocomposite thin films. A special curled architecture of the re-aggregated nanoclay-platelets was identified, providing a possible source for realizing the interlocking mechanism in the nanocomposites. The curled architecture could be the result from strain releasing when the thin films were peeled off from the substrates. Through micro-/nano-indentation and in situ observation of the deformation during tensile test with an atomic force microscope (AFM), the localized deformation mechanism of the synthesized materials was investigated in further details. The results implied that a localized crack diversion mechanism worked in the synthesized nanocomposite thin films, which resembled its nature counterpart-nacre. The deformation behavior and fracture mechanism were discussed with reference to lamellar structure, interfacial strength between the nanoclays and the polyacrylamide matrix, and nanoclay agglomeration.

scholarly journals Structural and Mechanical Properties of Nanostructured C-Ag Thin Films Synthesized by Thermionic Vacuum Arc Method

2018 ◽  
Vol 2018 ◽  
pp. 1-10 ◽  
Author(s):  
Rodica Vladoiu ◽  
Aurelia Mandes ◽  
Virginia Dinca-Balan ◽  
Vilma Bursikova
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Mechanical Properties ◽  
Elastic Modulus ◽  
Silicon Substrate ◽  
Vacuum Arc ◽  
Average Roughness ◽  
Thermionic Vacuum Arc ◽  
Induced Aggregation ◽  
Ag Film

Nanostructured C-Ag thin films of 200 nm thickness were successfully synthesized by the Thermionic Vacuum Arc (TVA) method. The influence of different substrates (glass, silicon wafers, and stainless steel) on the microstructure, morphology, and mechanical properties of nanostructured C-Ag thin films was characterized by High-Resolution Transmission Electron Microscopy (HRTEM), Scanning Electron Microscopy (SEM), Atomic Force Microscopy (AFM), and TI 950 (Hysitron) nanoindenter equipped with Berkovich indenter, respectively. The film’s hardness deposited on glass (HC-Ag/Gl = 1.8 GPa) was slightly lower than in the case of the C-Ag film deposited on a silicon substrate (HC-Ag/Si = 2.2 GPa). Also the apparent elastic modulus Eeff was lower for C-Ag/Gl sample (Eeff = 100 GPa) than for C-Ag/Si (Eeff = 170 GPa), while the values for average roughness are Ra=2.9 nm (C-Ag/Si) and Ra=10.6 (C-Ag/Gl). Using the modulus mapping mode, spontaneous and indentation-induced aggregation of the silver nanoparticles was observed for both C-Ag/Gl and C-Ag/Si samples. The nanocomposite C-Ag film exhibited not only higher hardness and effective elastic modulus, but also a higher fracture resistance toughness to the silicon substrate compared to the glass substrate.

Transmission electron microscopy studies and simulation of the indentation response of superelastic fullerenelike carbon nitride thin films

2008 ◽  
Vol 103 (12) ◽  
pp. 123515 ◽  
Author(s):  
J. Neidhardt ◽  
C. Walter ◽  
J. M. Molina-Aldareguia ◽  
M. Herrmann ◽  
W. J. Clegg ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Transmission Electron Microscopy ◽  
Carbon Nitride ◽  
Transmission Electron ◽  
Indentation Response
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