On the Performance of 17Ni/(10NiO-NiFe2O4) Cermet by Hot-Press Sintering Technology: Sintering Temperature Effects

2013 ◽  
Vol 457-458 ◽  
pp. 152-155
Author(s):  
Wen Zheng Dong ◽  
Qi Quan Lin ◽  
Tao Jiang ◽  
Zhi Gang Wang
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Great Influence ◽  
Sintering Behavior ◽  
Hot Press ◽  
Three Point Bending ◽  
Strength Tests ◽  
Hot Press Sintering

The sintering behavior and the resulting of cermet are influenced not only by the characteristics and impurities of the raw materials but also are found to be dependent on the thermal history during the fabrication process. Our work is concerned with the effect of sintering temperature on the mechanical properties of 17Ni/(10NiO-NiFe2O4) cermet. The nickel ferrite based cermet were prepared by hot-press sintering technology at 16MPa and sintered at temperatures ranging from 900 to 1200°C. The microstructure, phase compositions and mechanical properties were studied by SEM, XRD and three point bending strength tests respectively. It has been found that, the relative density, hardness and bending strength of NiFe2O4 based cermet have a great influence upon the sintering temperature, and an optimal sintering temperature, e.g. 1100°C is chosen through our experiments. The highest bending strength of 125.89Mpa could be obtained under the sintering temperature of 1100°C. Meanwhile, the thermal shock resistance increases as the sintering temperature increases.

scholarly journals Effect of Sintering Temperature on Microstructure and Mechanical Properties of Hot-Pressed Fe/FeAl2O4 Composite

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 422
Author(s):  
Kuai Zhang ◽  
Yungang Li ◽  
Hongyan Yan ◽  
Chuang Wang ◽  
Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Hot Press ◽  
Microstructure And Mechanical Properties ◽  
Powder Particles ◽  
Hot Press Sintering ◽  
Sintering Method

An Fe/FeAl2O4 composite was prepared with Fe-Fe2O3-Al2O3 powder by a hot press sintering method. The mass ratio was 6:1:2, sintering pressure was 30 MPa, and holding time was 120 min. The raw materials for the powder particles were respectively 1 µm (Fe), 0.5 µm (Fe2O3), and 1 µm (Al2O3) in diameter. The effect of sintering temperature on the microstructure and mechanical properties of Fe/FeAl2O4 composite was studied. The results showed that Fe/FeAl2O4 composite was formed by in situ reaction at 1300 °C–1500 °C. With the increased sintering temperature, the microstructure and mechanical properties of the Fe/FeAl2O4 composite showed a change law that initially became better and then became worse. The best microstructure and optimal mechanical properties were obtained at 1400 °C. At this temperature, the grain size of Fe and FeAl2O4 phases in Fe/FeAl2O4 composite was uniform, the relative density was 96.7%, and the Vickers hardness and bending strength were 1.88 GPa and 280.0 MPa, respectively. The wettability between Fe and FeAl2O4 was enhanced with increased sintering temperature. And then the densification process was accelerated. Finally, the microstructure and mechanical properties of the Fe/FeAl2O4 composite were improved.

Effects of TiN Content on Mechanical Properties and Microstructure of ATN Materials

2013 ◽  
Vol 589-590 ◽  
pp. 590-593 ◽  
Author(s):  
Min Wang ◽  
Jun Zhao
Keyword(s):  
Mechanical Properties ◽  
Mechanical Property ◽  
Fracture Toughness ◽  
Vickers Hardness ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Ceramic Materials ◽  
Hot Press ◽  
Hot Press Sintering ◽  
Tin Content

In order to investigate the effects of TiN content on Al2O3/TiN ceramic material (ATN), the ATN ceramic materials were prepared of TiN content in 30%, 40%, 50%, 60% in the condition of hot press sintering. The sintering temperature is 1700°C, the sintering press is 32MPa, and the holding time are 5min, 10min, 15min. The effects of TiN content on mechanical properties and microstructure of ATN ceramic materials were investigated by analyzing the bending strength, hardness, fracture toughness. The results show that ATN50 has the best mechanical property, its bending strength is 659.41MPa, vickers hardness is 13.79GPa, fracture toughness is 7.06MPa·m1/2. It is indicated that the TiN content has important effect on microstructure and mechanical properties of ATN ceramic materials.

Effect of Iron Additive on the Sintering Behavior of Hot-Pressed ZrC-W Composites

2008 ◽  
Vol 368-372 ◽  
pp. 1764-1766 ◽  
Author(s):  
Yu Jin Wang ◽  
Lei Chen ◽  
Tai Quan Zhang ◽  
Yu Zhou
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Sintering Behavior ◽  
Hot Press ◽  
Sintering Additive ◽  
Microstructure And Mechanical Properties ◽  
Hot Press Sintering

The ZrC-W composites with iron as sintering additive were fabricated by hot-press sintering. The densification, microstructure and mechanical properties of the composites were investigated. The incorporation of Fe beneficially promotes the densification of ZrC-W composites. The relative density of the composite sintered at 1900°C can attain 95.3%. W2C phase is also found in the ZrC-W composite sintered at 1700°C. The content of W2C decreases with the increase of sintering temperature. However, W2C phase is not identified in the composite sintered at 1900°C. The flexural strength and fracture toughness of the composites are strongly dependent on sintering temperature. The flexural strength and fracture toughness of ZrC-W composite sintered at optimized temperature of 1800°C are 438 MPa and 3.99 MPa·m1/2, respectively.

scholarly journals Effect of Fe on the Microstructure and Mechanical Properties of Fe/FeAl2O4 Cermet Prepared by Hot Press Sintering

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 204
Author(s):  
Kuai Zhang ◽  
Yungang Li ◽  
Chuang Wang ◽  
Hongyan Yan ◽  
Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Raw Materials ◽  
Diffusion Reaction ◽  
Mass Ratio ◽  
Hot Press ◽  
Ceramic Phase ◽  
Microstructure And Mechanical Properties ◽  
Hot Press Sintering

The Fe/FeAl2O4 cermet was prepared with Fe-Fe2O3-Al2O3 powder by a hot press sintering method at 1400 °C. The raw materials for the powder particles were respectively 2 µm (Fe), 0.5 µm (Fe2O3), and 0.5 µm (Al2O3) in diameter, the sintering pressure was 30 MPa, and the holding time was 120 min. The effects of different Fe mass ratios on the microstructure and mechanical properties of Fe/FeAl2O4 cermet were studied. The results showed that a new ceramic phase FeAl2O4 could be formed by an in situ reaction during the hot press sintering. When the Fe mass ratio was increased, the microstructure and mechanical properties of the Fe/FeAl2O4 cermet showed a change law that initially became better and then became worse. The best microstructure and mechanical properties were obtained in the S2 sample, where the mass ratio of Fe-Fe2O3-Al2O3 was 6:1:2. In this Fe mass ratio, the relative density was about 94%, and the Vickers hardness and bending strength were 1.21 GPa and 210.0 MPa, respectively. The reaction mechanism of Fe in the preparation process was the in situ synthesis reaction of FeAl2O4 and the diffusion reaction of Fe to FeAl2O4 grains. The increase of the Fe mass ratio improved the wettability of Fe and FeAl2O4, which increased the diffusion rate of Fe to FeAl2O4 grains, which increased the influence on the structure of FeAl2O4.

scholarly journals Microstructural Evolution of H-BN Matrix Composite Ceramics With Amorphous La2O3-Al2O3-SiO2 Glass Phase During Hot Pressing

2020 ◽  
Author(s):  
Baofu Qiu ◽  
Xiaoming Duan ◽  
Zhuo Zhang ◽  
Chen Zhao ◽  
Bo Niu ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Microstructural Evolution ◽  
Glass Phase ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Sintering Process ◽  
Hot Press ◽  
Composite Ceramics ◽  
Phase Precipitation ◽  
Hot Press Sintering

Abstract BN-La2O3-Al2O3-SiO2 composite ceramics were fabricated by hot press sintering using h-BN, La2O3, Al2O3 and amorphous SiO2 as the raw materials. The effects of sintering temperature on the microstructural evolution, bulk density, apparent porosity, and mechanical properties of h-BN composite ceramics were investigated. The results indicated that ternary La2O3-Al2O3-SiO2 liquid phase was formed during sintering process, which provided an environment for the growth of h-BN grains. With increasing sintering temperature, the cristobalite phase precipitation and h-BN grain growth occurred at the same time, which had the significant influence on the densification and mechanical properties of h-BN composite ceramics. The best mechanical properties of BN-La2O3-Al2O3-SiO2 composite ceramics were obtained under sintering temperature of 1700 °C, and the elastic modulus, flexural strength, and fracture toughness were 80.5 GPa, 266.4 MPa and 3.25 MPa·m1/2, respectively.

Effects of MgO and Y2O3 on the Microstructure and Mechanical Properties of Al2O3 Ceramics

2013 ◽  
Vol 589-590 ◽  
pp. 572-577 ◽  
Author(s):  
Hua He Liu ◽  
Han Lian Liu ◽  
Chuan Zhen Huang ◽  
Bin Zou ◽  
Ya Cong Chai
Keyword(s):  
Mechanical Properties ◽  
Sintering Temperature ◽  
Hot Press ◽  
Composite Ceramics ◽  
Microstructure And Mechanical Properties ◽  
Suitable Amount ◽  
Hot Press Sintering ◽  
Grains Refinement ◽  
Better Than

Al2O3-MgO, Al2O3-Y2O3 and Al2O3-MgO-Y2O3 composite ceramics were fabricated respectively by hot-press sintering technique. With the analysis of the mechanical properties and microstructure, it was found that single additive MgO could be more favorable to the grains’ refinement and densification than Y2O3; the composite additive including both MgO and Y2O3 was better than single additive MgO or Y2O3, because their interactions could improve the mechanical properties of the Al2O3 ceramics; The sintering temperature could be reduced by adding the suitable amount of composite additives.

Fabrication of TiAl Intermetallic by Spark Plasma Sintering

2007 ◽  
Vol 336-338 ◽  
pp. 1050-1052 ◽  
Author(s):  
Hai Tao Wu ◽  
Yun Long Yue ◽  
Wei Bing Wu ◽  
Hai Yan Yin
Keyword(s):  
Mechanical Properties ◽  
Intermetallic Compounds ◽  
Spark Plasma Sintering ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Three Point Bending ◽  
The Poor ◽  
High Relative Density ◽  
Plasma Sintering ◽  
Spark Plasma

The γ-TiAl intermetallic compounds were produced at the temperature ranging from 850°C to 1050°C by the Spark Plasma Sintering (SPS) process. The effects of sintering temperature and holding time on the mechanical properties of γ-TiAl intermetallic compounds were investigated. The γ-TiAl intermetallic compounds sintered at 1050°C for 10 min showed a high relative density more than 98%, and had the best three-point bending strength of 643MPa, fracture toughness of 12 MPa·m1/2 and microhardness of 560MPa. The microstructural observations indicated typical characteristics of intergranular fracture, which meant the poor ductility of γ-TiAl intermetallic compounds.

Hot-Press Sintering of Tic0.5N0.5-Based Cermets: Addition Effect of AlN Nano-Powder on Microstructure and Mechanical Properties

2017 ◽  
Vol 726 ◽  
pp. 297-302
Author(s):  
Chang Chun Lv ◽  
Yu Jia Zhai ◽  
Cheng Biao Wang ◽  
Zhi Jian Peng
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Vickers Hardness ◽  
Bending Strength ◽  
Hot Press ◽  
Nano Powder ◽  
Microstructure And Mechanical Properties ◽  
Hot Press Sintering

TiCN-based cermets were prepared by hot-press sintering through adding various amounts of AlN nanopowder (0-20 wt.%) into a 64 wt.% TiC0.5N0.5-10 wt.% WC-8.5 wt.% Mo-12.5 wt.% Ni-5 wt.% Co system. The microstructure and mechanical properties of the prepared cermets were investigated. For the prepared cermets, samples with 5 wt.% AlN nanopowder exhibited optimum mechanical properties of Vickers hardness 2191 HV10, bending strength 601 MPa, and fracture toughness 6.03 MPa.m1/2, respectively.

Preparation and Characterization of WC Matrix Nanocomposite Cermet

2009 ◽  
Vol 628-629 ◽  
pp. 459-464 ◽  
Author(s):  
Fa Zhan Yang ◽  
Xing Ai ◽  
Jun Zhao
Keyword(s):  
Mechanical Properties ◽  
Particle Size ◽  
Sintering Temperature ◽  
Fracture Morphology ◽  
Particle Sizes ◽  
Growth Inhibitors ◽  
Hot Press ◽  
Hot Press Sintering ◽  
Matrix Nanocomposite

A new WC matrix nanocomposite cermet was prepared by hot-press sintering. In the composite, certain amounts of VC is added to the composite as grain growth inhibitors. The consolidation is carried out under pressure 30～35Mpa and sintering temperature 1610°C for soaking 30min sintering. Microstructure of the nanocomposite cermet is scanned by SEM and mechanical properties are measured. It is detected that microstructure and fracture morphology is dissimilar to different particle sizes. Experimental results show that particle size of WC is important to the composite. Results show that relative density and hardness have the similar trend in growth. Meanwhile, the function of Al2O3 addition is also investigated in this paper.

Fabrication Processes and Properties of Highly Pure MgAlON Materials

2007 ◽  
Vol 561-565 ◽  
pp. 543-546 ◽  
Author(s):  
Qing Huang ◽  
Yong Huang ◽  
Chang An Wang ◽  
Hou Xing Zhang
Keyword(s):  
Spark Plasma Sintering ◽  
Open Porosity ◽  
Single Phase ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Hot Press ◽  
Plasma Sintering ◽  
Short Period ◽  
Spark Plasma ◽  
Hot Press Sintering

In this paper, the MgAlON ceramic was fabricated by Spark Plasma Sintering (SPS) and hot press sintering respectively. The results showed that highly pure and single-phase MgAlON could be fabricated at lower sintering temperature in a short period through SPS process, compared with the conventional Hot Press sintering (HP) process. The bending strength of MgAlON specimens prepared by SPS process was higher than 500MPa while bending strength of HP specimens was much lower. The open porosity was almost eliminated in SPS MgAlON specimens. Spark Plasma Sintered MgAlON had a single phase of MgAlON while Hot Press Sintered MgAlON had major MgAlON and minor AlN and Al2O3.

Sign in / Sign up

Export Citation Format

Share Document