Research on the Compound early Strength Agent to the Performance of Super High early Strength Grouting Material

2013 ◽  
Vol 477-478 ◽  
pp. 996-1001 ◽  
Author(s):  
Xiao Ping Zhang ◽  
Chang Zheng Sun ◽  
Tong Feng Zhao
Keyword(s):  
Compressive Strength ◽  
Sodium Sulfate ◽  
Setting Time ◽  
Cementitious Material ◽  
Final Setting Time ◽  
Grouting Material ◽  
Reinforcement Material ◽  
Reasonable Proportion ◽  
Strength Material ◽  
Early Strength

The effect of sodium sulfate, triethanolamine and early strength agent A on the early strength reinforcement material final setting time, flexural strength and compressive strength and structure were investigated. The results show that the composite of sodium sulfate, triethanolamine and early strength agent according to a reasonable proportion, the dosage of 0.35% -0.40% (in cementitious material quality), the final setting time of early strength material for 50 to 60 min, Initial fluidity over 320mm, 0.5h flow degree greater than 280mm, 1d bending greater than 12MPa and 28d compressive strength greater than 80MPa, meet the requirements.

Early Strength Agent on the Properties of Reinforcement Materials Research

2013 ◽  
Vol 477-478 ◽  
pp. 936-940
Author(s):  
Chang Zheng Sun ◽  
Xiao Ping Zhang ◽  
Hai Nan Zhao ◽  
Qiang Gao
Keyword(s):  
Compressive Strength ◽  
Flexural Strength ◽  
Sodium Nitrite ◽  
Setting Time ◽  
Initial Flow ◽  
Final Setting Time ◽  
Reinforcement Material ◽  
Materials Research ◽  
Early Strength ◽  
Nitrite Content

In the trial, the author explores sodium nitrite, triethanolamine and sodium on fluidity initial and final setting time, flexural strength and compressive strength and other properties, of early strength reinforcement material. The results showed that, when sodium nitrite content is 0.2%, triethanolamine content is 0.05%, the dosage of sodium sulfate is 0.8%, final setting time for 58min, the initial flow greater than 320[mm], 30min flow greater than 280[mm], 2h compressive strength of 30[MPa], 1d bending greater than 10[MPa], 28d compressive strength greater than 90[MPa], on the early strength reinforcement, meet construction requirements.

Research on Sand Gradation to Ultra Strength Grouting Material Properties

2014 ◽  
Vol 507 ◽  
pp. 300-305
Author(s):  
Chang Zheng Sun ◽  
Xiao Ping Zhang ◽  
Hai Nan Zhao ◽  
Qiang Gao
Keyword(s):  
Compressive Strength ◽  
Flexural Strength ◽  
Material Properties ◽  
Setting Time ◽  
Fine Sand ◽  
Coarse Sand ◽  
Medium Sand ◽  
Final Setting Time ◽  
Grouting Material ◽  
Early Strength

The gradation of coarse sand, medium sand and fine sand on fluidity initial, final setting time, flexural strength, compressive strength, and other properties and structure, of ultra early strength grouting material, was explored. The quartz sand gradation of cement sand ratio 1.0 was systematically studied. The results showed that, the coarse sand, medium sand and fine sand mixed according to the reasonable distribution, when glue sand ratio was 1.0-1.5, ultra-early-strength grouting material, with final setting time for 50-60(min), the initial fluidity greater than 320(mm), 0.5h fluidity greater than 280(mm), 2h compressive strength of 35.6(MPa), 1d flexural strength greater than 13(MPa), 28d compressive strength over 93(MPa), achieved the free vibration.

Several Common Retarders on Performance of Ultra-Early-Strength Grouting Material

2013 ◽  
Vol 477-478 ◽  
pp. 931-935
Author(s):  
Chang Zheng Sun ◽  
Xiao Ping Zhang ◽  
Hai Nan Zhao ◽  
Qiang Gao
Keyword(s):  
Mechanical Strength ◽  
Setting Time ◽  
Strength Properties ◽  
Preliminary Screening ◽  
Final Setting Time ◽  
Grouting Material ◽  
Early Strength

To explore retarders on performance of ultra-early strength grouting material, Retarder, which are commonly used in the market after a preliminary screening, are further tested and analyzed for initial fluidity, setting time and mechanical strength properties of super early strength grouting material. The results show that: When borax content is 0.4%, the initial fluidity, final setting time, workability, mechanical strength are the best.

scholarly journals Effect of Calcium Nitrate on the Properties of Portland–Limestone Cement-Based Concrete Cured at Low Temperature

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1611
Author(s):  
Gintautas Skripkiūnas ◽  
Asta Kičaitė ◽  
Harald Justnes ◽  
Ina Pundienė
Keyword(s):  
Compressive Strength ◽  
Cement Paste ◽  
Setting Time ◽  
Calcium Nitrate ◽  
Curing Temperature ◽  
Hardened Concrete ◽  
Cement Pastes ◽  
Initial Setting Time ◽  
Initial Setting ◽  
Early Strength

The effect of calcium nitrate (CN) dosages from 0 to 3% (of cement mass) on the properties of fresh cement paste rheology and hardening processes and on the strength of hardened concrete with two types of limestone-blended composite cements (CEM II A-LL 42.5 R and 42.5 N) at different initial (two-day) curing temperatures (−10 °C to +20 °C) is presented. The rheology results showed that a CN dosage up to 1.5% works as a plasticizing admixture, while higher amounts demonstrate the effect of increasing viscosity. At higher CN content, the viscosity growth in normal early strength (N type) cement pastes is much slower than in high early strength (R type) cement pastes. For both cement-type pastes, shortening the initial and final setting times is more effective when using 3% at +5 °C and 0 °C. At these temperatures, the use of 3% CN reduces the initial setting time for high early strength paste by 7.4 and 5.4 times and for normal early strength cement paste by 3.5 and 3.4 times when compared to a CN-free cement paste. The most efficient use of CN is achieved at −5 °C for compressive strength enlargement; a 1% CN dosage ensures the compressive strength of samples at a −5 °C initial curing temperature, with high early strength cement exceeding 3.5 MPa but being less than the required 3.5 MPa in samples with normal early strength cement.

Behaviour of Calcium Alkali Orthophosphate Cements under Simulated Implantation Conditions

2008 ◽  
Vol 396-398 ◽  
pp. 213-216 ◽  
Author(s):  
Daniela Jörn ◽  
Renate Gildenhaar ◽  
Georg Berger ◽  
Michael Stiller ◽  
Christine Knabe
Keyword(s):  
Compressive Strength ◽  
Simulated Body Fluid ◽  
Clinical Application ◽  
Body Fluid ◽  
Setting Time ◽  
Great Decrease ◽  
Final Setting Time ◽  
Laboratory Conditions ◽  
Setting Times

The setting behaviour, the compressive strength and the porosity of four calcium alkali orthophosphate cements were examined under laboratory conditions (dry) and under conditions similar to those during clinical application (37°C, contact with body fluid). The results showed an increase of the setting times when specimens were covered with simulated body fluid. Especially, the final setting time (FHZ) was significantly higher for three of the four cements. Furthermore, when specimens were stored in SBF for 16h, an extensive decrease of the compressive strength was noted. The porosity was more than twice as high after 16h in SBF and this may be the cause for the great decrease of the compressive strength.

scholarly journals Optimization and Hydration Mechanism of Composite Cementing Material for Paste Filling in Coal Mines

2019 ◽  
Vol 2019 ◽  
pp. 1-13
Author(s):  
Jinxiao Liu ◽  
Wenxin Li ◽  
Feng Zhang ◽  
Xinguo Zhang ◽  
Lianjun Chen ◽  
...  
Keyword(s):  
Early Stage ◽  
Uniform Design ◽  
Setting Time ◽  
Coal Mines ◽  
Hydration Products ◽  
Hydrated Calcium Silicate ◽  
Sulphoaluminate Cement ◽  
Final Setting Time ◽  
Early Strength ◽  
Cementing Material

The low early strength of materials for paste filling in mines caused by low early strength of composite cementing material has been a severe issue. In this study, the effects of sulphoaluminate cement and gypsum on strengths of composite cementing material were investigated experimentally by employing the constrained formulation uniform design. With the content of the sulphoaluminate cement below 14% and the content of the gypsum below 16%, the compressive strengths of composite cementing materials increased, especially early strength. However, the initial and final setting time does not meet the engineering requirements in this case. Optimization tests of composite additives demonstrated that H2BO3(0.3%) + Na2SO4(0.1%) and H2BO3(0.3%) + NaNO2(0.1%) were ideal setting retarding and early strengthening composite additives as they can both reduce the initial and final setting time and enhance compressive strengths of composite cementing material. Investigations by XRD and SEM revealed that the hydration products of composite cementing material were dominated by AFt (ettringite) at the early stage and by C-S-H (hydrated calcium silicate) gel + CH (calcium hydroxide) gel at the middle and late stages. The hydration products of ratio-optimized composite cementing material do not restrain each other due to the generation sequence. Instead, they grew interactively and were coupled, thus facilitating the growth of the hardened body. This study can provide references for optimization of composite cementing material for paste filling in coal mines.

Research on Multivariate Composite Super early Strength Grouting Materials

2013 ◽  
Vol 477-478 ◽  
pp. 990-995
Author(s):  
Xiao Ping Zhang ◽  
Chang Zheng Sun ◽  
Tong Feng Zhao
Keyword(s):  
Compressive Strength ◽  
High Performance ◽  
Ordinary Portland Cement ◽  
High Alumina ◽  
Flow Ratio ◽  
Initial Flow ◽  
Growth Structure ◽  
Grouting Material ◽  
Early Strength ◽  
Grouting Materials

Super early strength high performance grouting material was produced using high alumina cement, ordinary portland cement, gypsum and silica fume. The different glue sand ratio and the cement sand ratio 1.0 mix microstructure were studied systematically. The results showed that the system with a variety of admixture using hingh mortar ratio can be prepared for the initial flow ratio greater than 325{mm},, 30min flow greater than 280{mm}, 2h compressive strength 34.80{MPa}, 24h bending over 13.82{MPa}, 28d compressive strength greater than 99.90{MPa}, 28d compressive strength greater than 56d compressive strength. The system of early SEM microstructures showed good crystal growth, structure compact.

scholarly journals Experimental Study on the Influence of PVA Content on the Performance of Grouting Material in Deep Stope

Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-11
Author(s):  
Bin Liu ◽  
Liming Yin ◽  
Juntao Chen ◽  
Ming Li ◽  
Daozeng Tang ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Flexural Strength ◽  
Setting Time ◽  
Practical Significance ◽  
Peak Period ◽  
Grouting Material ◽  
Coupling Characteristics ◽  
Grouting Materials ◽  
And Control ◽  
Water Hazards

Based on laboratory experiments, the paper researches the effect of polyvinyl alcohol (PVA) content on the performance of fly ash-based cement grouting materials. The test results show that the addition of PVA has limited effect on the initial and final setting time and brings a certain but minor delay on the appearance of the hydration peak period. It enhances cement hydration during the hydration slow down period. The impermeability of PVA to the grouting material is obviously improved, and it increases with the growing amount of PVA content. PVA improves the flexural strength and compressive strength of the sample block to varying degrees, and the improvement on flexural strength is more obvious than that on the compressive strength. It has a significant effect on the mechanical properties of the grouting material and can effectively improve the rock mass’s hydraulic coupling characteristics. It also has great application value and practical significance for the prevention and control of water hazards in deep coal stopes.

Experimental Research on Si-Mn Slag Cementitious Material

2013 ◽  
Vol 438-439 ◽  
pp. 98-101
Author(s):  
Xu Fang Zhang ◽  
Jun Yu Wu
Keyword(s):  
Experimental Research ◽  
Sodium Sulfate ◽  
Anhydrous Sodium Sulfate ◽  
Setting Time ◽  
Cementitious Material ◽  
Additive Effect ◽  
Raw Material

A Si-Mn Slag Cementitious Material was prepared by mixing Si-Mn slag, circulating fluidization bed slag as raw material. The results shows that circulating fluidization bed slag and Si-Mn slag has a preferably additive effect in a certain range by combination of lime, anhydrite and anhydrous sodium sulfate as activator, and the strength of samples reach the peak at circulating fluidization bed slag of 8%, Si-Mn slag of 70%, anhydrous sodium sulfate of 2%, anhydrite of 10%, lime of 10%. The strength, setting time and soundness were also tested and the results can meet most of the requirements of OPC standard (42.5) GB/T 175-2007.

scholarly journals A Feasibility Study on HPMC-Improved Sulphoaluminate Cement for 3D Printing

Materials ◽  
2018 ◽  
Vol 11 (12) ◽  
pp. 2415 ◽  
Author(s):  
Zhu Ding ◽  
Xiaodong Wang ◽  
Jay Sanjayan ◽  
Patrick Zou ◽  
Zhi-Kun Ding
Keyword(s):  
Compressive Strength ◽  
3D Printing ◽  
Feasibility Study ◽  
Setting Time ◽  
Hydroxypropyl Methylcellulose ◽  
Hydration Heat ◽  
Heat Setting ◽  
Sulphoaluminate Cement ◽  
Final Setting Time ◽  
Experimental Parameters

A novel 3D printing material based on hydroxypropyl methylcellulose (HPMC)—improved sulphoaluminate cement (SAC) for rapid 3D construction printing application is reported. The hydration heat, setting time, fluidity of paste and mortar, shape retainability, and compressive strength of extruded SAC mortar were investigated. HPMC dosage, water-to-cement (W/C) ratio, and sand-to-cement (S/C) ratio were studied as the experimental parameters. Hydration heat results reveal HPMC could delay the hydration of SAC. The initial and final setting time measured using Vicat needle would be shortened in the case of W/C ratio of 0.3 and 0.35 with HPMC dosage from 0.5% to 1.5%, W/C ratio of 0.40 with HPMC dosage of 0.5%, 0.75%, and 1.5%, and W/C ratio of 0.45 with HPMC dosage of 0.45, or be extended in the case of W/C ratio of 0.4 with HPMC dosage of 1.0% and W/C ratio of 0.45 with HPMC dosage from 0.75% to 1.5%. Fluidity measurement shows HPMC significantly improves the shape retainability. Furthermore, the addition of HPMC remarkably increased the compressive strength of extruded mortar. The results showed that HPMC could be used to prepare 3D printing SAC having satisfactory shape retainability, setting time and compressive strength.

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