Preparation of Sodium Diacetate
2014 ◽
Vol 508
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pp. 79-82
Keyword(s):
The sodium diacetate using acetic acid and sodium hydroxide as materials was prepared in which one-step liquid-phase method and microwave method were adopted in the paper. By single factor experiment, the regularities of the influence of various factors including reaction temperature, reaction time and acetic acid-sodium hydroxide ratio on the yield of sodium diacetate were studied. Through the orthogonal experiment the optimum synthesis conditions of sodium diacetate were confirmed that the reaction temperature was 70°C, the reaction time was 60min and the acetic acid-sodium hydroxide ratio was 2.1:1. The product yield was 96.2% under the optimal reaction conditions.
2013 ◽
Vol 634-638
◽
pp. 628-631
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2012 ◽
Vol 554-556
◽
pp. 1178-1182
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2013 ◽
Vol 781-784
◽
pp. 276-279
Keyword(s):
1999 ◽
Vol 14
(11)
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pp. 4437-4442
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2011 ◽
Vol 295-297
◽
pp. 2088-2091
Keyword(s):
Keyword(s):